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Journal of Materials Science: Materials in Electronics
Erschienen in: Journal of Materials Science: Materials in Electronics 6/2019

15.02.2019

Thermo-optical correlation for room temperature synthesis: cold-sintered lead halides

verfasst von: Manish Kumar, Vani Pawar, Priyanka A. Jha, S. K. Gupta, A. S. K. Sinha, Pardeep K. Jha, Prabhakar Singh

Erschienen in: Journal of Materials Science: Materials in Electronics | Ausgabe 6/2019

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Abstract

At present, the cost-effective synthesis and stability are major concerns for perovskite halide, which are high-efficient light absorbing solar cell materials. In this work, the cesium lead halides CsPbX3 (where, X = I and Br) were synthesized by simple but unique cold sintering method. The structural (XRD and Raman), microstructural (SEM), electronic (XPS) and optical studies (UV–Visible spectra) revealed that the samples synthesized are in the single phase with Pnma symmetry. The thermal stability of the samples synthesized was explored by estimating ΔG and ΔS. A negligible change in crystal structure and band gap of the samples is observed after 100 days of synthesis showing the stability of samples in the ambient condition. Along with structure–property correlation, the thermo-optical correlation for halide materials has also been established. A comparative of the band gap (on the basis of synthesis technique) suggests the samples synthesised by cold sintering are at par with other synthesis technique.
Vorheriger Artikel High performance humidity sensor based on V0.5Sn0.5Se2 ternary alloy
Nächster Artikel Fabrication and characterization of Au/n-ZnO/p-Si/Al sandwich device with Sol–gel spin coating method

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Metadaten
Titel
Thermo-optical correlation for room temperature synthesis: cold-sintered lead halides
verfasst von
Manish Kumar
Vani Pawar
Priyanka A. Jha
S. K. Gupta
A. S. K. Sinha
Pardeep K. Jha
Prabhakar Singh
Publikationsdatum
15.02.2019
Verlag
Springer US
Erschienen in
Journal of Materials Science: Materials in Electronics / Ausgabe 6/2019
Print ISSN: 0957-4522
Elektronische ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-019-00908-x

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