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Erschienen in: Journal of Nanoparticle Research 9/2018

01.09.2018 | Brief Communication

Time-dependent non-linear size change of C60-ethylenediamine adduct particles in formation process

verfasst von: Tsuyoshi Akiyama, Yuji Ono, Hiroshi Miyamura, Jo Saito, Kento Kimura, Suguru Higashida, Takeo Oku

Erschienen in: Journal of Nanoparticle Research | Ausgabe 9/2018

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Abstract

Addition reaction between C60 and ethylenediamine occurred at room temperature in an ambient condition. C60-ethylenediamine adduct particles were prepared by mixing toluene solutions of C60 and ethyelenediamine. Average diameter of the C60-ethylenediamine adduct particles was changed non-linearly according to the reaction time, which were observed using transmission electron microscopy. Early stage of the reaction, the diameter of the adduct particles was changed from about 250 to about 430 nm. Then, the size of the adduct particles was converged to about 300 nm. During this addition reaction, the crystalline sizes of adduct particles were constant about 2–3 nm, regardless of the sizes of the adduct particles, which were determined by X-ray diffraction measurement.

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Metadaten
Titel
Time-dependent non-linear size change of C60-ethylenediamine adduct particles in formation process
verfasst von
Tsuyoshi Akiyama
Yuji Ono
Hiroshi Miyamura
Jo Saito
Kento Kimura
Suguru Higashida
Takeo Oku
Publikationsdatum
01.09.2018
Verlag
Springer Netherlands
Erschienen in
Journal of Nanoparticle Research / Ausgabe 9/2018
Print ISSN: 1388-0764
Elektronische ISSN: 1572-896X
DOI
https://doi.org/10.1007/s11051-018-4353-9

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