Skip to main content
Erschienen in: Metallurgical and Materials Transactions A 11/2017

23.08.2017

Validation and Analysis of the Parameters for Reconstructing the Austenite Phase from Martensite Electron Backscatter Diffraction Data

verfasst von: L. Sanz, B. Pereda, B. López

Erschienen in: Metallurgical and Materials Transactions A | Ausgabe 11/2017

Einloggen

Aktivieren Sie unsere intelligente Suche um passende Fachinhalte oder Patente zu finden.

search-config
loading …

Abstract

This work focuses on the validation of a method for reconstructing the fcc crystallographic data from martensite orientation electron backscatter diffraction (EBSD) maps based on the “γ nuclei identification” and “γ nuclei spreading strategy.” To that end, an Fe-30Ni alloy was employed. The martensite transformation start temperature (M s ) of this material is close to or below room temperature; therefore, during hot deformation and after water quenching, it presents an fcc austenitic microstructure, while after subzero quenching, austenite-to-martensite transformation takes place. Accordingly, the reconstruction procedure can be applied to the martensitic EBSD crystallographic data, and the morphological and orientation results of the reconstruction can be validated by comparison with the original crystallographic fcc data. Torsion tests were performed to produce recrystallized and deformed austenite microstructures. Although applying the Kurdjumov–Sachs orientation relationship (OR) resulted in reconstructed area fractions larger than 75 pct, the reconstruction quality improved significantly when other ORs closer to the Greninger–Troiano OR were applied. The analysis carried out on the recrystallized microstructure shows that the method is robust against variation in the different parameters involved in the reconstruction. Good angular and morphological reconstruction results were obtained in both recrystallized and deformed microstructures, including the ability to reconstruct twins.

Sie haben noch keine Lizenz? Dann Informieren Sie sich jetzt über unsere Produkte:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literatur
1.
Zurück zum Zitat H.L. Andrade, M.G. Akben, and J.J. Jonas: Metall. Mater. Trans. A, 1983, vol. 14A, pp. 1967–77.CrossRef H.L. Andrade, M.G. Akben, and J.J. Jonas: Metall. Mater. Trans. A, 1983, vol. 14A, pp. 1967–77.CrossRef
2.
Zurück zum Zitat A.I. Fernandez, B. Lopez, and J.M. Rodriguez-Ibabe: Scripta Mater., 1999, vol. 40, pp. 543–49.CrossRef A.I. Fernandez, B. Lopez, and J.M. Rodriguez-Ibabe: Scripta Mater., 1999, vol. 40, pp. 543–49.CrossRef
3.
4.
5.
Zurück zum Zitat A.H. Ücisik, C.J. McMahon, and H.C. Feng: Metall. Trans. A, 1978, vol. 9A, pp. 604–06.CrossRef A.H. Ücisik, C.J. McMahon, and H.C. Feng: Metall. Trans. A, 1978, vol. 9A, pp. 604–06.CrossRef
6.
Zurück zum Zitat N. Bernier, L. Bracke, L. Malet, and S. Godet: Mater. Charact., 2014, vol. 89, pp. 23–32.CrossRef N. Bernier, L. Bracke, L. Malet, and S. Godet: Mater. Charact., 2014, vol. 89, pp. 23–32.CrossRef
7.
Zurück zum Zitat L. Germain, N. Gey, R. Mercier, P. Blaineau, and M. Humbert: Acta Mater., 2012, vol. 60, pp. 4551–62.CrossRef L. Germain, N. Gey, R. Mercier, P. Blaineau, and M. Humbert: Acta Mater., 2012, vol. 60, pp. 4551–62.CrossRef
8.
Zurück zum Zitat M. Humbert, F. Wagner, H. Moustahfid, and C. Esling: J. Appl. Cryst., 1995, vol. 28, pp. 571–76.CrossRef M. Humbert, F. Wagner, H. Moustahfid, and C. Esling: J. Appl. Cryst., 1995, vol. 28, pp. 571–76.CrossRef
9.
10.
11.
Zurück zum Zitat C. Cayron, B. Artaud, and L. Briottet: Mater. Charact., 2006, vol. 57, pp. 386–401.CrossRef C. Cayron, B. Artaud, and L. Briottet: Mater. Charact., 2006, vol. 57, pp. 386–401.CrossRef
12.
Zurück zum Zitat V. Tari, A.D. Rollett, and H. Beladi: J. Appl. Cryst., 2013, vol. 46, pp. 210–15.CrossRef V. Tari, A.D. Rollett, and H. Beladi: J. Appl. Cryst., 2013, vol. 46, pp. 210–15.CrossRef
13.
Zurück zum Zitat G. Miyamoto, N. Iwata, N. Takayama, and T. Furuhara: Acta Mater., 2010, vol. 58, pp. 6393–03.CrossRef G. Miyamoto, N. Iwata, N. Takayama, and T. Furuhara: Acta Mater., 2010, vol. 58, pp. 6393–03.CrossRef
14.
Zurück zum Zitat G. Miyamoto, N. Iwata, N. Takayama, and T. Furuhara: ISIJ Int., 2011, vol. 51, pp. 1174–78.CrossRef G. Miyamoto, N. Iwata, N. Takayama, and T. Furuhara: ISIJ Int., 2011, vol. 51, pp. 1174–78.CrossRef
15.
16.
Zurück zum Zitat D. Poddar, P. Cizek, H. Beladi, and P.D. Hodgson: Acta Mater., 2014, vol. 80, pp. 1–15.CrossRef D. Poddar, P. Cizek, H. Beladi, and P.D. Hodgson: Acta Mater., 2014, vol. 80, pp. 1–15.CrossRef
17.
Zurück zum Zitat D. Poddar, P. Cizek, H. Beladi, and P.D. Hodgson: Acta Mater., 2015, vol. 99, pp. 347–62.CrossRef D. Poddar, P. Cizek, H. Beladi, and P.D. Hodgson: Acta Mater., 2015, vol. 99, pp. 347–62.CrossRef
18.
Zurück zum Zitat E.J. Palmiere, P. Cizek, F. Bai, R.M. Poths, J. Turner, B.P. Wynne, and W.M. Rainforth: Mater. Manuf. Process., 2011, vol. 26, pp. 127–31.CrossRef E.J. Palmiere, P. Cizek, F. Bai, R.M. Poths, J. Turner, B.P. Wynne, and W.M. Rainforth: Mater. Manuf. Process., 2011, vol. 26, pp. 127–31.CrossRef
19.
Zurück zum Zitat F. Ciura, B. Dubiel, and K. Satora: Mater. Charact., 2006, vol. 56, pp. 290–96.CrossRef F. Ciura, B. Dubiel, and K. Satora: Mater. Charact., 2006, vol. 56, pp. 290–96.CrossRef
20.
Zurück zum Zitat TSL OIM Analysis 5.31, Package 7000, EDAX, Mahwah, NJ. TSL OIM Analysis 5.31, Package 7000, EDAX, Mahwah, NJ.
21.
Zurück zum Zitat MATLAB, Release 2013b, The MathWorks, Inc., Natick, MA. MATLAB, Release 2013b, The MathWorks, Inc., Natick, MA.
22.
Zurück zum Zitat M. Humbert, F. Wagner, and C. Esling: J. Appl. Cryst., 1992, vol. 25, pp. 724–30.CrossRef M. Humbert, F. Wagner, and C. Esling: J. Appl. Cryst., 1992, vol. 25, pp. 724–30.CrossRef
23.
Zurück zum Zitat G. Miyamoto, N. Takayama, and T. Furuhara: Scripta Mater., 2009, vol. 60, pp. 1113–16.CrossRef G. Miyamoto, N. Takayama, and T. Furuhara: Scripta Mater., 2009, vol. 60, pp. 1113–16.CrossRef
24.
Zurück zum Zitat M. Humbert, P. Blaineau, L. Germain, and N. Gey: Scripta Mater., 2011, vol. 64, pp. 114–17.CrossRef M. Humbert, P. Blaineau, L. Germain, and N. Gey: Scripta Mater., 2011, vol. 64, pp. 114–17.CrossRef
25.
Zurück zum Zitat M. Humbert, L. Germain, N. Gey, and E. Boucard: Acta Mater., 2015, vol. 82, pp. 137–44.CrossRef M. Humbert, L. Germain, N. Gey, and E. Boucard: Acta Mater., 2015, vol. 82, pp. 137–44.CrossRef
26.
27.
Zurück zum Zitat B.L. Henrie, T.A. Mason, and B.L. Hansen: Metall. Mater. Trans. A, 2004, vol. 35A, pp. 3745–51.CrossRef B.L. Henrie, T.A. Mason, and B.L. Hansen: Metall. Mater. Trans. A, 2004, vol. 35A, pp. 3745–51.CrossRef
28.
Zurück zum Zitat D.P. Field, L.T. Bradford, M.M. Nowell, and T.M. Lillo: Acta Mater., 2007, vol. 55, pp. 4233–41.CrossRef D.P. Field, L.T. Bradford, M.M. Nowell, and T.M. Lillo: Acta Mater., 2007, vol. 55, pp. 4233–41.CrossRef
29.
Zurück zum Zitat W.M. Rainforth, M.P. Black, R.L. Higginson, E.J. Palmiere, C.M. Sellars, I. Prabst, P. Warbichler, and F. Hofer: Acta Mater., 2002, vol. 50, pp. 735–47.CrossRef W.M. Rainforth, M.P. Black, R.L. Higginson, E.J. Palmiere, C.M. Sellars, I. Prabst, P. Warbichler, and F. Hofer: Acta Mater., 2002, vol. 50, pp. 735–47.CrossRef
30.
Zurück zum Zitat H. Beladi, P. Cizek, and P.D. Hodgson: Acta Mater., 2010, vol. 58, pp. 3531–41.CrossRef H. Beladi, P. Cizek, and P.D. Hodgson: Acta Mater., 2010, vol. 58, pp. 3531–41.CrossRef
31.
Zurück zum Zitat H. Beladi, P. Cizek, and P.D. Hodgson, Metall. Mater. Trans. A, 2009, vol. 40A, pp. 1175–89.CrossRef H. Beladi, P. Cizek, and P.D. Hodgson, Metall. Mater. Trans. A, 2009, vol. 40A, pp. 1175–89.CrossRef
32.
Zurück zum Zitat L. Llanos, B. Pereda, and B. López: Metall. Mater. Trans. A, 2015, vol. 46A, pp. 5248–65.CrossRef L. Llanos, B. Pereda, and B. López: Metall. Mater. Trans. A, 2015, vol. 46A, pp. 5248–65.CrossRef
Metadaten
Titel
Validation and Analysis of the Parameters for Reconstructing the Austenite Phase from Martensite Electron Backscatter Diffraction Data
verfasst von
L. Sanz
B. Pereda
B. López
Publikationsdatum
23.08.2017
Verlag
Springer US
Erschienen in
Metallurgical and Materials Transactions A / Ausgabe 11/2017
Print ISSN: 1073-5623
Elektronische ISSN: 1543-1940
DOI
https://doi.org/10.1007/s11661-017-4289-1

Weitere Artikel der Ausgabe 11/2017

Metallurgical and Materials Transactions A 11/2017 Zur Ausgabe

    Marktübersichten

    Die im Laufe eines Jahres in der „adhäsion“ veröffentlichten Marktübersichten helfen Anwendern verschiedenster Branchen, sich einen gezielten Überblick über Lieferantenangebote zu verschaffen.