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Erschienen in: Cellulose 4/2014

01.08.2014 | Original Paper

Vibrational sum-frequency-generation (SFG) spectroscopy study of the structural assembly of cellulose microfibrils in reaction woods

verfasst von: Kabindra Kafle, Rui Shi, Christopher M. Lee, Ashutosh Mittal, Yong Bum Park, Ying-Hsuan Sun, Sunkyu Park, Vincent Chiang, Seong H. Kim

Erschienen in: Cellulose | Ausgabe 4/2014

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Abstract

The cellulose microfibril assemblies in secondary cell walls of tension wood and compression wood were studied with vibrational sum frequency generation (SFG) spectroscopy. The tension wood contains the gelatinous layer with highly-crystalline and highly-aligned cellulose microfibrils. The SFG spectral features of tension wood changed depending on the azimuth angle between the polarization of the incident IR beam and the preferential alignment axis of the cellulose microfibrils. The SFG spectra of the compression wood did not show any dependence on the azimuth angle, implying that the overall orientation of cellulose microfibrils in compression wood is not highly aligned. Instead, the decrease of cellulose content in compression wood brought about larger separation between cellulose microfibrils, which was manifested as changes in CH2/OH intensity ratio in SFG spectra. These results implied that SFG spectral features are sensitive to cellulose microfibril alignments and inter-fibrillar separations.

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Metadaten
Titel
Vibrational sum-frequency-generation (SFG) spectroscopy study of the structural assembly of cellulose microfibrils in reaction woods
verfasst von
Kabindra Kafle
Rui Shi
Christopher M. Lee
Ashutosh Mittal
Yong Bum Park
Ying-Hsuan Sun
Sunkyu Park
Vincent Chiang
Seong H. Kim
Publikationsdatum
01.08.2014
Verlag
Springer Netherlands
Erschienen in
Cellulose / Ausgabe 4/2014
Print ISSN: 0969-0239
Elektronische ISSN: 1572-882X
DOI
https://doi.org/10.1007/s10570-014-0322-3

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