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Journal of Polymer Research
Erschienen in: Journal of Polymer Research 8/2023

01.08.2023 | Original Paper

Preparation and characterization of morphological and mechanical properties of cellulose cryogel nanofibers reinforced by different polyamide resins

verfasst von: Benyamin Yousefi, Mohammad Dinari, Mehdi Karevan, Mostafa Jamshidian

Erschienen in: Journal of Polymer Research | Ausgabe 8/2023

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Abstract

As environmentally friendly materials, cellulose cryogels are good choices due to their biodegradability and ease of use. However, the most crucial issue concerning cellulose cryogels is their weakness in terms of mechanical properties. In this study, two types of Polyamide-Epichlorohydrine resins, named PAE1 and PAE2, and Polyamide-Glutaraldehide-Epichlorohydrine resin (PGE) were synthesized; they were utilized to reinforce cellulose nanofiber gel (CNFG), and this was followed by the freeze-drying process. The density and porosity of the cryogels were improved and evaluated using mathematical equations. The mechanical behavior of the fabricated specimens was examined to obtain the optimized values of processing time and temperature, as well as the resin weight fraction, which yielded the improvement of compressive modulus, yield strength, and the stress at 60% strain (S60) to 2 (MPa), 50 (kPa), and 1.8 (MPa) respectively. Also, attenuated total reflection (ATR) analysis was conducted to study the effect of resins on the cross-linking of cellulose nanofibers (CNF)s; further, nitrogen adsorption–desorption analysis was performed to investigate the specific surface area and mesopore diameter distribution of cryogels using Brunauer–Emmett–Teller (BET) and Barrett-Joyner-Halenda (BJH) methods, respectively.
Vorheriger Artikel Exploring ordered structures by varying symmetric interaction parameters of non-frustrated ABCBA linear pentablock terpolymers in the melt
Nächster Artikel Preparation of stereocomplex powder from polycondensation poly(L-lactic acid) and poly(D-lactic acid) for use as a nucleating agent of high-molecular-weight poly(L-lactide)

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Metadaten
Titel
Preparation and characterization of morphological and mechanical properties of cellulose cryogel nanofibers reinforced by different polyamide resins
verfasst von
Benyamin Yousefi
Mohammad Dinari
Mehdi Karevan
Mostafa Jamshidian
Publikationsdatum
01.08.2023
Verlag
Springer Netherlands
Erschienen in
Journal of Polymer Research / Ausgabe 8/2023
Print ISSN: 1022-9760
Elektronische ISSN: 1572-8935
DOI
https://doi.org/10.1007/s10965-023-03697-4

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