Skip to main content
Top
Published in: Journal of Materials Science 5/2007

01-03-2007 | Nano May 2006

Characterization of nanocrystalline materials by X-ray line profile analysis

Author: Tamás Ungár

Published in: Journal of Materials Science | Issue 5/2007

Log in

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

X-ray line profile analysis is shown to be a powerful tool to characterize the microstructure of nanocrystalline materials in terms of grain and subgrain size, dislocation structure and dislocation densities and planar defects, especially stacking faults and twin boundaries. It is shown that the X-ray method can provide valuable complementary information about the microstructure, especially when combined with transmission electron microscopy and differential scanning calorimetry.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literature
1.
go back to reference Hellmig RJ, Baik SC, Bowen JR, Estrin Y, Juul Jensen D, Kim HS, Seo MH, December 2003, In: Zehetbauer MJ, Valiev RZ (eds) Proc. 2nd Int. Conf. Nanomater. Severe Plastic Deformation: Fundamentals – Processing – Applications, Wien, Austria, J.Wiley VCH, Weinheim, 2004 p 420 Hellmig RJ, Baik SC, Bowen JR, Estrin Y, Juul Jensen D, Kim HS, Seo MH, December 2003, In: Zehetbauer MJ, Valiev RZ (eds) Proc. 2nd Int. Conf. Nanomater. Severe Plastic Deformation: Fundamentals – Processing – Applications, Wien, Austria, J.Wiley VCH, Weinheim, 2004 p 420
2.
go back to reference Scherrer P (1918) Göttinger Nachrichten 2:98 Scherrer P (1918) Göttinger Nachrichten 2:98
6.
go back to reference Wilson AJC (1962) In: X-Ray Optics; the Diffraction of X-Rays by Finite and Imperfect Crystals, Methuen, London Wilson AJC (1962) In: X-Ray Optics; the Diffraction of X-Rays by Finite and Imperfect Crystals, Methuen, London
8.
go back to reference Wilkens M Fundamental Aspects of Dislocation Theory, edited by J.A Simmons, R de Wit, R Bullough, Vol. II Nat Bur Stand (US) Spec. Publ. No. 317, Washington, DC. USA, 970 p 1195 Wilkens M Fundamental Aspects of Dislocation Theory, edited by J.A Simmons, R de Wit, R Bullough, Vol. II Nat Bur Stand (US) Spec. Publ. No. 317, Washington, DC. USA, 970 p 1195
10.
go back to reference Krill CE, Birringer R (1998) Phil Mag A 77:621 Krill CE, Birringer R (1998) Phil Mag A 77:621
12.
go back to reference Ungár T, Borbély A, Goren-Muginstein G R, Bergerand S, Rosen A R (1999) Nanostructured Mater 11:103CrossRef Ungár T, Borbély A, Goren-Muginstein G R, Bergerand S, Rosen A R (1999) Nanostructured Mater 11:103CrossRef
14.
go back to reference Valiev RZ, Kozlov EV, Ivanov Yu F, Lian J, Nazarov AA, Baudelet B (1994) Acta Met Mater 42:2467CrossRef Valiev RZ, Kozlov EV, Ivanov Yu F, Lian J, Nazarov AA, Baudelet B (1994) Acta Met Mater 42:2467CrossRef
15.
go back to reference Terwilliger ChD, Chiang YM (1995) Acta Met Mater 43:319 Terwilliger ChD, Chiang YM (1995) Acta Met Mater 43:319
16.
go back to reference Scardi P, Leoni M (2002) Acta Cryst A58:190 Scardi P, Leoni M (2002) Acta Cryst A58:190
17.
go back to reference Hinds WC In: Aerosol technology. Properties, behavior and measurement of airbone particles, (Wiley, New York, 1982) Hinds WC In: Aerosol technology. Properties, behavior and measurement of airbone particles, (Wiley, New York, 1982)
19.
20.
go back to reference Ribárik G, Gubicza J, Ungár T (2004) Mat Sci Eng A387–389:343 Ribárik G, Gubicza J, Ungár T (2004) Mat Sci Eng A387–389:343
23.
go back to reference Ungár T, Ott S, Sanders PG, Borbély A, Weertman JR (1998) Acta Mater 46:3693CrossRef Ungár T, Ott S, Sanders PG, Borbély A, Weertman JR (1998) Acta Mater 46:3693CrossRef
24.
go back to reference Mitra R, Ungár T, Morita T, Sanders PG, Weertman JR (1999) In: Chung YW, Dunand DC, Liaw PF and Olson GB (eds) Advanced Materials for the 21st Century, Warrendale TMS, USA, p 553 Mitra R, Ungár T, Morita T, Sanders PG, Weertman JR (1999) In: Chung YW, Dunand DC, Liaw PF and Olson GB (eds) Advanced Materials for the 21st Century, Warrendale TMS, USA, p 553
25.
go back to reference Mitra R, Ungár T, Weertman JR (2005) Trans Indian Inst Metals 58:1125–1132 Mitra R, Ungár T, Weertman JR (2005) Trans Indian Inst Metals 58:1125–1132
26.
go back to reference Gubicza J, Balogh L, Hellmig RJ, Estrin Y, Ungár (2005) T Mat Sci Eng A 400–401:334–338CrossRef Gubicza J, Balogh L, Hellmig RJ, Estrin Y, Ungár (2005) T Mat Sci Eng A 400–401:334–338CrossRef
27.
go back to reference Sanders PG (1996) Ph.D. Thesis, Northwestern University, Evanston, IL, USA 60208 Sanders PG (1996) Ph.D. Thesis, Northwestern University, Evanston, IL, USA 60208
28.
go back to reference Zhilyaev AP, Gubicza J, Nurislamova G, Révész Á, Suriñach S, Baró MD, Ungár T (2003) Phys Stat Sol (a) 198:263CrossRef Zhilyaev AP, Gubicza J, Nurislamova G, Révész Á, Suriñach S, Baró MD, Ungár T (2003) Phys Stat Sol (a) 198:263CrossRef
29.
go back to reference Gubicza J, Chinh NQ, Horita Z, Langdon TG (2004) Mater Sci Eng A 387–389:55 Gubicza J, Chinh NQ, Horita Z, Langdon TG (2004) Mater Sci Eng A 387–389:55
30.
go back to reference Zhu YT, Huang JY, Gubicza J, Ungár T, Wang YM, Ma E, Valiev RZ (2003) J Mat Res 18:1908 Zhu YT, Huang JY, Gubicza J, Ungár T, Wang YM, Ma E, Valiev RZ (2003) J Mat Res 18:1908
31.
go back to reference Bolmaro RE, Brokmeier HG, Signorelli JW, Fourtz A, Bertinetti MA (2004) In: Mittemeijer EJ, Scardi P (eds) Diffraction analysis of the microstructure of materials, Springer, Berlin, p 391 Bolmaro RE, Brokmeier HG, Signorelli JW, Fourtz A, Bertinetti MA (2004) In: Mittemeijer EJ, Scardi P (eds) Diffraction analysis of the microstructure of materials, Springer, Berlin, p 391
32.
go back to reference Ungár T, Tichy G, Gubicza J, Hellmig RJ (2005) J Powder Diffraction, 20:366CrossRef Ungár T, Tichy G, Gubicza J, Hellmig RJ (2005) J Powder Diffraction, 20:366CrossRef
33.
go back to reference Krivoglaz M A theory of X-ray and thermal neutron scattering by real crystals Berlin: Springer-Verlag; 1996 Krivoglaz M A theory of X-ray and thermal neutron scattering by real crystals Berlin: Springer-Verlag; 1996
38.
go back to reference Thiele E, Klemm R, Hollang L, Holste C, Schell N, Natter H, Hempelmann R (2005) Mat Sci Eng A 390:42CrossRef Thiele E, Klemm R, Hollang L, Holste C, Schell N, Natter H, Hempelmann R (2005) Mat Sci Eng A 390:42CrossRef
40.
go back to reference Ungár T, Gubicza J, Tichy G, Pantea C, Zerda TW (2005) Composites:Part A 36:431 Ungár T, Gubicza J, Tichy G, Pantea C, Zerda TW (2005) Composites:Part A 36:431
42.
go back to reference Stokes AR, Wilson AJC (1944) Proc Cambridge Phys Soc 40:197 Stokes AR, Wilson AJC (1944) Proc Cambridge Phys Soc 40:197
44.
go back to reference Steeds JW (1973) In introduction to the anisotropic elasticity theory of dislocations. Oxford, Clarendon Steeds JW (1973) In introduction to the anisotropic elasticity theory of dislocations. Oxford, Clarendon
47.
50.
go back to reference Nyilas K, Dupas C, Kruml T, Zsoldos L, Ungár T, Martin JL (2004) Mat Sci Eng A 387:25CrossRef Nyilas K, Dupas C, Kruml T, Zsoldos L, Ungár T, Martin JL (2004) Mat Sci Eng A 387:25CrossRef
51.
52.
go back to reference Fátay D, Bastarash E, Nyilas K, Dobatkin S, Gubicza J, Ungár T (2003) Metallkd Z 94:7 Fátay D, Bastarash E, Nyilas K, Dobatkin S, Gubicza J, Ungár T (2003) Metallkd Z 94:7
53.
go back to reference Balogh L, Gubicza J, Hellmig RJ, Estrin Y, Ungár T (2006) Z Kristallography 23:381CrossRef Balogh L, Gubicza J, Hellmig RJ, Estrin Y, Ungár T (2006) Z Kristallography 23:381CrossRef
54.
go back to reference Gubicza J, Nam NH, Balogh L, Hellmig RJ, Stolyarov VV, Estrin Y, Ungár T (2004) J Alloy Compd 378:248CrossRef Gubicza J, Nam NH, Balogh L, Hellmig RJ, Stolyarov VV, Estrin Y, Ungár T (2004) J Alloy Compd 378:248CrossRef
56.
go back to reference Kuzel R, Cernansky M, Holy V, Kubena J, Simek D, Kub J (2004) In: Mittemeijer EJ, Scardi P (eds) Diffraction analysis of the microstructure of materials, Springer, Berlin, p 229 Kuzel R, Cernansky M, Holy V, Kubena J, Simek D, Kub J (2004) In: Mittemeijer EJ, Scardi P (eds) Diffraction analysis of the microstructure of materials, Springer, Berlin, p 229
58.
go back to reference Dragomir IC, Ungár T, Chen M, Ma E, Hemker KJ, Sheng H, Wang YM, Cheng X (2003) Science 300:1275CrossRef Dragomir IC, Ungár T, Chen M, Ma E, Hemker KJ, Sheng H, Wang YM, Cheng X (2003) Science 300:1275CrossRef
59.
60.
61.
go back to reference Ungár T, Balogh L, Zhu Y T, Horita Z, Xu C, Langdon TG (2006) submitted to Mater Sci Eng A Ungár T, Balogh L, Zhu Y T, Horita Z, Xu C, Langdon TG (2006) submitted to Mater Sci Eng A
62.
go back to reference Zhu YT, Liao XZ, Srinivasan SG, Zhao YH, Baskes MI, Zhou F, Lavernia E (2004) J Appl Phys Lett 85:5049CrossRef Zhu YT, Liao XZ, Srinivasan SG, Zhao YH, Baskes MI, Zhou F, Lavernia E (2004) J Appl Phys Lett 85:5049CrossRef
63.
go back to reference Zhu YT, Liao XZ, Srinivasan SG, Lavernia EJ (2005) J Appl Pys 98:034319/1–8CrossRef Zhu YT, Liao XZ, Srinivasan SG, Lavernia EJ (2005) J Appl Pys 98:034319/1–8CrossRef
64.
go back to reference Zhao YH, Liao XZ, Zhu YT, Horita Z, Langdon TG (2005) Mater Sci Eng A410–411:188 Zhao YH, Liao XZ, Zhu YT, Horita Z, Langdon TG (2005) Mater Sci Eng A410–411:188
Metadata
Title
Characterization of nanocrystalline materials by X-ray line profile analysis
Author
Tamás Ungár
Publication date
01-03-2007
Published in
Journal of Materials Science / Issue 5/2007
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-006-0696-1

Other articles of this Issue 5/2007

Journal of Materials Science 5/2007 Go to the issue

Premium Partners