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Measurement Techniques

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08-03-2018

Development of a New Type of Reference Standard for Carbon Isotopic Composition

Authors: Ya. K. Chubchenko, L. A. Konopel’ko

Published in: Measurement Techniques | Issue 12/2018

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Abstract

The development of a new type of reference standard for carbon isotopic composition consisting of ¹²CO₂ + ¹³CO₂ and N₂ gaseous mixtures in tanks under pressure is discussed. These standards are required for measuring the isotope ratio ¹³C/¹²C in gaseous mixtures of CO₂. The procedures for preparing and verifying the reference standards are described and their stability is tested. These standard samples can be used for calibrating (testing) isotopic infrared analyzers and mass spectrometers.

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T. B. Coplen, W. A. Brand, M. Gehre, et al., “New guidelines for δ¹³C,” Measur. Anal. Chem., 78, 2439–2441 (2006).CrossRef

W. A. Brand, T. B. Coplen, J. Vogl, et al., “Assessment of international reference materials for isotope-ratio analysis (IUPAC Technical Report),” Pure Appl. Chem., 86, No. 3, 425–467 (2014).CrossRef

Ya. K. Chubchenko and L. A. Konopel’ko, “Features of determining the isotopic composition of carbon in gaseous, liquid, and solid media,” Metrologiya, No. 2, 45–52 (2017).

GOST R ISO 6142-2001, Gas Analysis. Preparation of Calibration Gas Mixtures. Gravimetric Method.

ISO 6143:2001, Gas Analysis. Comparison Methods for Determining and Checking the Composition of Calibration Gas Mixtures.

GOST 8.578-2014, National Verification Scheme for Means of Measurement of the Amounts of Components in Gaseous Media.

Title: Development of a New Type of Reference Standard for Carbon Isotopic Composition
Authors: Ya. K. Chubchenko
L. A. Konopel’ko
Publication date: 08-03-2018
Publisher: Springer US
Published in: Measurement Techniques / Issue 12/2018
Print ISSN: 0543-1972
Electronic ISSN: 1573-8906
DOI: https://doi.org/10.1007/s11018-018-1344-2

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