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Published in: Journal of Polymer Research 2/2021

01-02-2021 | ORIGINAL PAPER

Effect of mandrel rotation speed on morphology and mechanical properties of polypropylene pipes produced by rotational shear

Authors: Junjun Wu, Zexiang Xie, Hao Yang, Minghao Yang, Kaizhi Shen, Qiang Fu, Xueqin Gao

Published in: Journal of Polymer Research | Issue 2/2021

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Abstract

To research the role of mandrel rotation speed on the morphology and mechanical properties of polypropylene (PP) pipes, a self-made rotational shear system (RSS) was applied in this study to manufacture plastic pipes with improved hoop tensile strength through applying hoop shear on the pipes using a rotational mandrel. Morphology study results indicated that different morphologies of the PP pipes were produced when the mandrel rotated at 0 rpm, 2 rpm, 4 rpm, 6 rpm, 8 rpm and 10 rpm. The tensile strength and elongation at break of the pipes were found to increase rapidly with the rotation speed and the properties peaked at 6 rpm. At this speed, the tensile strength and elongation at break increased by 4.1% and 727%, respectively. The high mechanical and thermal performance of the pipe produced at 6 rpm was attributed to the grains begin to refine and the thickness of amorphous region increases throughout the pipe wall.

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Appendix
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Literature
1.
go back to reference Yesil Y, Bhat GS et al (2016) Technology Structure and mechanical properties of polyethylene melt blown nonwovens. INT J CLOTH SCI TECH 28:780–793CrossRef Yesil Y, Bhat GS et al (2016) Technology Structure and mechanical properties of polyethylene melt blown nonwovens. INT J CLOTH SCI TECH 28:780–793CrossRef
2.
go back to reference Xu H, Zhong GJ, Fu Q, Lei J, Li ZM et al (2012) Interfaces Formation of Shish-Kebabs in Injection-Molded Poly(L-lactic acid) by Application of an Intense Flow Field. Acs Applied Materials & Interfaces, 4(12):6774–6784CrossRef Xu H, Zhong GJ, Fu Q, Lei J, Li ZM et al (2012) Interfaces Formation of Shish-Kebabs in Injection-Molded Poly(L-lactic acid) by Application of an Intense Flow Field. Acs Applied Materials & Interfaces, 4(12):6774–6784CrossRef
3.
go back to reference Wang K, Chen F, Li Z, Fu Q et al (2014) Control of the hierarchical structure of polymer articles via “structuring” processing. Progress in Polymer ence 39(5):891–920CrossRef Wang K, Chen F, Li Z, Fu Q et al (2014) Control of the hierarchical structure of polymer articles via “structuring” processing. Progress in Polymer ence 39(5):891–920CrossRef
4.
go back to reference Ning N, Luo F, Pan B, Zhang Q, Wang K, Fu Q et al (2007) Observation of Shear-Induced Hybrid Shish Kebab in the Injection Molded Bars of Linear Polyethylene Containing Inorganic Whiskers. Macromolecules 40(24):8533–8536CrossRef Ning N, Luo F, Pan B, Zhang Q, Wang K, Fu Q et al (2007) Observation of Shear-Induced Hybrid Shish Kebab in the Injection Molded Bars of Linear Polyethylene Containing Inorganic Whiskers. Macromolecules 40(24):8533–8536CrossRef
5.
go back to reference Zhou SY, Niu B, Xie XL et al (2017) Interfacial Shish-Kebabs Lengthened by Coupling Effect of In Situ Flexible Nanofibrils and Intense Shear Flow: Achieving Hierarchy To Conquer the Conflicts between Strength and Toughness of Polylactide. ACS Appl Mater Interfaces 9(11):10148–10159CrossRef Zhou SY, Niu B, Xie XL et al (2017) Interfacial Shish-Kebabs Lengthened by Coupling Effect of In Situ Flexible Nanofibrils and Intense Shear Flow: Achieving Hierarchy To Conquer the Conflicts between Strength and Toughness of Polylactide. ACS Appl Mater Interfaces 9(11):10148–10159CrossRef
6.
go back to reference Gu X, Zhou M, Wang Y et al (2019) Influence of annealing on the morphology and mechanical properties of iPP/HDPE blend with tailored oriented crystalline structures. Journal of Polymer Research 26(8):194CrossRef Gu X, Zhou M, Wang Y et al (2019) Influence of annealing on the morphology and mechanical properties of iPP/HDPE blend with tailored oriented crystalline structures. Journal of Polymer Research 26(8):194CrossRef
7.
go back to reference Coates PD, Ward IM et al (1981) Science Die drawing: Solid phase drawing of polymers through a converging die. Polymer Engineering & ence 21:612–618CrossRef Coates PD, Ward IM et al (1981) Science Die drawing: Solid phase drawing of polymers through a converging die. Polymer Engineering & ence 21:612–618CrossRef
8.
go back to reference Pingping, Yang, Qi et al (2018) Structure evolution and orientation mechanism of isotactic polypropylene during the two-stage solid die drawing process. Journal of Applied Polymer Science 135:46581CrossRef Pingping, Yang, Qi et al (2018) Structure evolution and orientation mechanism of isotactic polypropylene during the two-stage solid die drawing process. Journal of Applied Polymer Science 135:46581CrossRef
9.
go back to reference Ruizhang X, Sheng Z, Jiantao W et al (2018) Impact of different die draw ratio on crystalline and oriented properties of polypropylene cast films and annealed films. J Polym Res 25(6):1–10 Ruizhang X, Sheng Z, Jiantao W et al (2018) Impact of different die draw ratio on crystalline and oriented properties of polypropylene cast films and annealed films. J Polym Res 25(6):1–10
10.
go back to reference An FZ, Gao XQ, Lei J et al (2015) Vibration Assisted Extrusion of Polypropylene. Chinese Journal of Polymer ence 33(5):688–696CrossRef An FZ, Gao XQ, Lei J et al (2015) Vibration Assisted Extrusion of Polypropylene. Chinese Journal of Polymer ence 33(5):688–696CrossRef
11.
go back to reference Nie M, Wang Q et al (2013) Control of rotation extrusion over shish-kebab crystal alignment in polyethylene pipe and its effect on the pipes crack resistance. Journal of Applied Polymer Science 135:46581. Nie M, Wang Q et al (2013) Control of rotation extrusion over shish-kebab crystal alignment in polyethylene pipe and its effect on the pipes crack resistance. Journal of Applied Polymer Science 135:46581.
12.
go back to reference Nie M, Li X, Hu X et al (2014) Effect of Die Temperature on Morphology and Performance of Polyethylene Pipe Prepared via Mandrel Rotation Extrusion. Journal of Macromolecular ence Part B 53(8):1442–1452CrossRef Nie M, Li X, Hu X et al (2014) Effect of Die Temperature on Morphology and Performance of Polyethylene Pipe Prepared via Mandrel Rotation Extrusion. Journal of Macromolecular ence Part B 53(8):1442–1452CrossRef
13.
go back to reference Nie M, Bai SB, Wang Q et al (2010) High-density polyethylene pipe with high resistance to slow crack growth prepared via rotation extrusion. Polym Bull 65(6):609–621CrossRef Nie M, Bai SB, Wang Q et al (2010) High-density polyethylene pipe with high resistance to slow crack growth prepared via rotation extrusion. Polym Bull 65(6):609–621CrossRef
14.
go back to reference Han R, Nie M, Wang Q et al (2015) Control over β-form hybrid shish-kebab crystals in polypropylene pipe via coupled effect of self-assembly β nucleating agent and rotation extrusion. Journal of the Taiwan Institute of Chemical Engineers 52:158–164CrossRef Han R, Nie M, Wang Q et al (2015) Control over β-form hybrid shish-kebab crystals in polypropylene pipe via coupled effect of self-assembly β nucleating agent and rotation extrusion. Journal of the Taiwan Institute of Chemical Engineers 52:158–164CrossRef
15.
go back to reference Kalay G, Bevis MJ et al (1997) Processing and physical property relationships in injection olded isotactic polypropylene. 2. Morphology and crystallinity. Journal of Polymer ence Part B: Polymer Physics 35(2):265-291 Kalay G, Bevis MJ et al (1997) Processing and physical property relationships in injection olded isotactic polypropylene. 2. Morphology and crystallinity. Journal of Polymer ence Part B: Polymer Physics 35(2):265-291
16.
go back to reference Kalay G, Bevis MJ et al (2015) The effect of shear controlled orientation in injection moulding on the mechanical properties of an aliphatic polyketone. Journal of Polymer ence Part B Polymer Physics 35(3):415–430CrossRef Kalay G, Bevis MJ et al (2015) The effect of shear controlled orientation in injection moulding on the mechanical properties of an aliphatic polyketone. Journal of Polymer ence Part B Polymer Physics 35(3):415–430CrossRef
17.
go back to reference Han R, Nie M, Wang Q et al (2017) Continuously enhanced hoop strength of rotation-extruded polypropylene pipe via self-assembly β nucleating agent with different aspect ratio. J Polym Res 24(11):204CrossRef Han R, Nie M, Wang Q et al (2017) Continuously enhanced hoop strength of rotation-extruded polypropylene pipe via self-assembly β nucleating agent with different aspect ratio. J Polym Res 24(11):204CrossRef
18.
go back to reference Xie Z, Gao N, Du Z, Yang H, Shen K, Fu Q, Gao X et al (2020) Role of Melt Plasticizing Temperature in Morphology and Properties of PE100 Pipes Prepared by a Rotational Shear System. ACS Omega 5:12660–12671CrossRef Xie Z, Gao N, Du Z, Yang H, Shen K, Fu Q, Gao X et al (2020) Role of Melt Plasticizing Temperature in Morphology and Properties of PE100 Pipes Prepared by a Rotational Shear System. ACS Omega 5:12660–12671CrossRef
19.
go back to reference Na B, Li Z, Lv R et al (2011) Oriented re-crystallization of polypropylene through partial melting and its dramatic influence on mechanical properties. J Polym Res 18(6):2103–2108CrossRef Na B, Li Z, Lv R et al (2011) Oriented re-crystallization of polypropylene through partial melting and its dramatic influence on mechanical properties. J Polym Res 18(6):2103–2108CrossRef
20.
go back to reference Worth RA (1979) The effect of mandrel rotation on power consumption in polypropylene extrusion. Polymer Engineering & ence 19(3):198–202CrossRef Worth RA (1979) The effect of mandrel rotation on power consumption in polypropylene extrusion. Polymer Engineering & ence 19(3):198–202CrossRef
21.
go back to reference Deberdeev RY, Zuev BM, Bezruk LI et al (1974) The Properties of Pipes Produced under the Conditions of Spiral Flow. Int J Polym Mater 3(3):177–191CrossRef Deberdeev RY, Zuev BM, Bezruk LI et al (1974) The Properties of Pipes Produced under the Conditions of Spiral Flow. Int J Polym Mater 3(3):177–191CrossRef
22.
go back to reference Han R, Nie M, Bai SB et al (2013) Control over crystalline form in polypropylene pipe via mandrel rotation extrusion. Polym Bull 70(7):2083–2096CrossRef Han R, Nie M, Bai SB et al (2013) Control over crystalline form in polypropylene pipe via mandrel rotation extrusion. Polym Bull 70(7):2083–2096CrossRef
23.
go back to reference Nie M, Bai S, Wang Q et al (2010) Effect of the inner wall cooling rate on the structure and properties of a polyethylene pipe extruded at a high rotation speed. Journal of Applied Polymer ence 119(3):1659–1666CrossRef Nie M, Bai S, Wang Q et al (2010) Effect of the inner wall cooling rate on the structure and properties of a polyethylene pipe extruded at a high rotation speed. Journal of Applied Polymer ence 119(3):1659–1666CrossRef
24.
go back to reference Nie M, Wang Q, Bai SB et al (2010) Morphology and property of polyethylene pipe extruded at the low mandrel rotation. Polymer Engineering & ence 50(9):1743–1750CrossRef Nie M, Wang Q, Bai SB et al (2010) Morphology and property of polyethylene pipe extruded at the low mandrel rotation. Polymer Engineering & ence 50(9):1743–1750CrossRef
25.
go back to reference Guo Y, Wang Q, Bai S et al (2010) The Effect of Rotational Extrusion on the Structure and Properties of HDPE Pipes. Polymer-Plastics Technology and Engineering 49(9):908–915CrossRef Guo Y, Wang Q, Bai S et al (2010) The Effect of Rotational Extrusion on the Structure and Properties of HDPE Pipes. Polymer-Plastics Technology and Engineering 49(9):908–915CrossRef
26.
go back to reference Samuels RJ, Yee RY et al (1972)Characterization of the structure and organization of β-form crystals in type III and type IV isotactic polypropylene spherulites.Journal of Polymer ence Part A-2 Polymer Physics 10, 385–432 Samuels RJ, Yee RY et al (1972)Characterization of the structure and organization of β-form crystals in type III and type IV isotactic polypropylene spherulites.Journal of Polymer ence Part A-2 Polymer Physics 10, 385–432
27.
go back to reference Meille V, Stefano Brückner, Sergio et al (1989) Non-parallel chains in crystalline γ-isotactic polypropylene. Nature 340(6233):455–457CrossRef Meille V, Stefano Brückner, Sergio et al (1989) Non-parallel chains in crystalline γ-isotactic polypropylene. Nature 340(6233):455–457CrossRef
28.
go back to reference Natta G, Corradini P et al (1960) Structure and properties of isotactic polypropylene. Il Nuovo Cimento 15(1):40–51CrossRef Natta G, Corradini P et al (1960) Structure and properties of isotactic polypropylene. Il Nuovo Cimento 15(1):40–51CrossRef
29.
go back to reference Wu CM, Chen M, Karger-Kocsis J et al (1999) The role of metastability in the micromorphologic features of sheared isotactic polypropylene melts. Polymer 40(15):4195–4203CrossRef Wu CM, Chen M, Karger-Kocsis J et al (1999) The role of metastability in the micromorphologic features of sheared isotactic polypropylene melts. Polymer 40(15):4195–4203CrossRef
30.
go back to reference Wenig W, Herzog F et al (1993) Injection molding of polypropylene: X-ray investigation of the skin–core morphology. Journal of Applied Polymer ence 50(12):2163–2171CrossRef Wenig W, Herzog F et al (1993) Injection molding of polypropylene: X-ray investigation of the skin–core morphology. Journal of Applied Polymer ence 50(12):2163–2171CrossRef
31.
go back to reference Chu F, Yamaoka T, Kimura Y et al (1995)Crystal transformation and micropore formation during uniaxial drawing of β-form polypropylene film. Polymer 2523-2530 Chu F, Yamaoka T, Kimura Y et al (1995)Crystal transformation and micropore formation during uniaxial drawing of β-form polypropylene film. Polymer 2523-2530
32.
go back to reference Nie M, Han R, Wang Q et al (2014) Formation and Alignment of Hybrid Shish-Kebab Morphology with Rich Beta Crystals in an Isotactic Polypropylene Pipe. Ind Eng Chem Res 53(10):4142–4146CrossRef Nie M, Han R, Wang Q et al (2014) Formation and Alignment of Hybrid Shish-Kebab Morphology with Rich Beta Crystals in an Isotactic Polypropylene Pipe. Ind Eng Chem Res 53(10):4142–4146CrossRef
33.
go back to reference Leugering VHJ, Kirsch G et al (1973) Beeinflussung der Kristallstruktur von isotaktischem Polypropylen durch Kristallisation aus orientierter Schmelze. Angew Makromol Chem 33(1):17–23CrossRef Leugering VHJ, Kirsch G et al (1973) Beeinflussung der Kristallstruktur von isotaktischem Polypropylen durch Kristallisation aus orientierter Schmelze. Angew Makromol Chem 33(1):17–23CrossRef
34.
go back to reference Zebarjad SM, Tahani M, Sajjadi SA et al (2004) Influence of filler particles on deformation and fracture mechanism of isotactic polypropylene. Journal of Materials Processing Tech, 155–156:1459–1464CrossRef Zebarjad SM, Tahani M, Sajjadi SA et al (2004) Influence of filler particles on deformation and fracture mechanism of isotactic polypropylene. Journal of Materials Processing Tech, 155–156:1459–1464CrossRef
35.
go back to reference Acierno S, Coppola S, Grizzuti N et al (2008) Effects of molecular weight distribution on the flow-enhanced crystallization of poly(1-butene). J Rheol 52(2):551–566CrossRef Acierno S, Coppola S, Grizzuti N et al (2008) Effects of molecular weight distribution on the flow-enhanced crystallization of poly(1-butene). J Rheol 52(2):551–566CrossRef
36.
go back to reference Huo H, Meng Y, Li H et al (2004) Influence of shear on polypropylene crystallization kinetics. European Physical Journal E Soft Matter 15(2):167CrossRef Huo H, Meng Y, Li H et al (2004) Influence of shear on polypropylene crystallization kinetics. European Physical Journal E Soft Matter 15(2):167CrossRef
37.
go back to reference Yang H, Luo X, Shen K, Yuan Y, Fu Q, Gao X, Jiang L et al (2019) The role of mandrel rotation speed on morphology and mechanical properties of polyethylene pipes produced by rotational shear. Polymer 184:121915CrossRef Yang H, Luo X, Shen K, Yuan Y, Fu Q, Gao X, Jiang L et al (2019) The role of mandrel rotation speed on morphology and mechanical properties of polyethylene pipes produced by rotational shear. Polymer 184:121915CrossRef
38.
go back to reference Jiang ZY, Tang YJ, Men YF et al (2007) Structural Evolution of Tensile-Deformed High-Density Polyethylene during Annealing: Scanning Synchrotron Small-Angle X-ray Scattering Study. Macromolecules 40(20):7263–7269CrossRef Jiang ZY, Tang YJ, Men YF et al (2007) Structural Evolution of Tensile-Deformed High-Density Polyethylene during Annealing: Scanning Synchrotron Small-Angle X-ray Scattering Study. Macromolecules 40(20):7263–7269CrossRef
39.
go back to reference Somani RH, Hsiao BS, Nogales A et al (2013) Structure development during shear flow induced crystallization of i-PP: In situ wide-angle X-ray diffraction study. Macromolecules 33:9385–9394CrossRef Somani RH, Hsiao BS, Nogales A et al (2013) Structure development during shear flow induced crystallization of i-PP: In situ wide-angle X-ray diffraction study. Macromolecules 33:9385–9394CrossRef
40.
go back to reference Larin B, Avila-Orta CA, Somani RH et al (2008) Combined effect of shear and fibrous fillers on orientation-induced crystallization in discontinuous aramid fiber/isotactic polypropylene composites. Polymer 49(1):295–302CrossRef Larin B, Avila-Orta CA, Somani RH et al (2008) Combined effect of shear and fibrous fillers on orientation-induced crystallization in discontinuous aramid fiber/isotactic polypropylene composites. Polymer 49(1):295–302CrossRef
41.
go back to reference Campbell D, Qayyum MM et al (1977) Enhanced fracture strain of polypropylene by incorporation of thermoplastic fibres. J Mater Sci 12(12):2427–2434CrossRef Campbell D, Qayyum MM et al (1977) Enhanced fracture strain of polypropylene by incorporation of thermoplastic fibres. J Mater Sci 12(12):2427–2434CrossRef
42.
go back to reference Chan CM, Wu J, Li JX et al (2003) Polypropylene/calcium carbonate nanocomposites Polymer 43(10):2981-2992 Chan CM, Wu J, Li JX et al (2003) Polypropylene/calcium carbonate nanocomposites Polymer 43(10):2981-2992
43.
go back to reference Pan Y, Gao X, Lei J et al (2016) Effect of different morphologies on the creep behavior of high-density polyethylene. RSC Advances 6(5):3470–3479CrossRef Pan Y, Gao X, Lei J et al (2016) Effect of different morphologies on the creep behavior of high-density polyethylene. RSC Advances 6(5):3470–3479CrossRef
Metadata
Title
Effect of mandrel rotation speed on morphology and mechanical properties of polypropylene pipes produced by rotational shear
Authors
Junjun Wu
Zexiang Xie
Hao Yang
Minghao Yang
Kaizhi Shen
Qiang Fu
Xueqin Gao
Publication date
01-02-2021
Publisher
Springer Netherlands
Published in
Journal of Polymer Research / Issue 2/2021
Print ISSN: 1022-9760
Electronic ISSN: 1572-8935
DOI
https://doi.org/10.1007/s10965-020-02366-0

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