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2018 | OriginalPaper | Chapter

18. Electrochemical Surface X-Ray Scattering

Author : Toshihiro Kondo

Published in: Compendium of Surface and Interface Analysis

Publisher: Springer Singapore

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Abstract

Electrochemical surface X-ray scattering (EC-SXS) is an application of surface X-ray scattering (SXS) technique, one of the surface analysis methods, to electrochemical interfaces, i.e., electrode/electrolyte solution interfaces.

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Literature
1.
go back to reference Uosaki, K.: In situ real-time monitoring of geometric, electronic, and molecular structures at solid/liquid interfaces. Jpn. J. Appl. Phys. Part1 54, 030102/1–030102/14 (2015)CrossRef Uosaki, K.: In situ real-time monitoring of geometric, electronic, and molecular structures at solid/liquid interfaces. Jpn. J. Appl. Phys. Part1 54, 030102/1–030102/14 (2015)CrossRef
2.
go back to reference Kondo, T., Masuda, M., Uosaki, K.: In situ SXS and XAFS measurements of electrochemical interface. In: Kumar, C.S.S.R. (eds.) X-ray and Neutron Techniques for Nanomaterials Characterization (Chap. 7), pp. 367–450. Springer, Berlin (2016) Kondo, T., Masuda, M., Uosaki, K.: In situ SXS and XAFS measurements of electrochemical interface. In: Kumar, C.S.S.R. (eds.) X-ray and Neutron Techniques for Nanomaterials Characterization (Chap. 7), pp. 367–450. Springer, Berlin (2016)
3.
go back to reference Toney, M.F., McBreen, J.: In situ synchrotron X-ray techniques for determining atomic structure at electrode/electrolyte interfaces. Electrochem. Soc. Interface 2(Spring), 22–31 (1993) Toney, M.F., McBreen, J.: In situ synchrotron X-ray techniques for determining atomic structure at electrode/electrolyte interfaces. Electrochem. Soc. Interface 2(Spring), 22–31 (1993)
4.
go back to reference Feidenhansl, R.: Surface-structure determination by modern X-ray physics. Surf. Sci. Rep. 10, 105–188 (1989)CrossRef Feidenhansl, R.: Surface-structure determination by modern X-ray physics. Surf. Sci. Rep. 10, 105–188 (1989)CrossRef
5.
go back to reference Wang, J., Ocko, B.M., Davenport, A.J., Isaacs, H.S.: In situ X-ray-diffraction and X-ray-reflectivity studies of the Au(111) electrolyte interface—reconstruction and anion adsorption. Phys. Rev. B 46, 10321–10338 (1992)CrossRef Wang, J., Ocko, B.M., Davenport, A.J., Isaacs, H.S.: In situ X-ray-diffraction and X-ray-reflectivity studies of the Au(111) electrolyte interface—reconstruction and anion adsorption. Phys. Rev. B 46, 10321–10338 (1992)CrossRef
6.
go back to reference Scherb, G., Kazimirov, A., Zegenhagen, J., Lee, T.L., Bedzyk, M.J., Noguchi, H., Uosaki, K.: In situ X-ray standing-wave analysis of electrodeposited Cu monolayers on GaAs(001). Phys. Rev. B 58, 10800–10805 (1998)CrossRef Scherb, G., Kazimirov, A., Zegenhagen, J., Lee, T.L., Bedzyk, M.J., Noguchi, H., Uosaki, K.: In situ X-ray standing-wave analysis of electrodeposited Cu monolayers on GaAs(001). Phys. Rev. B 58, 10800–10805 (1998)CrossRef
7.
go back to reference Nagy, Z., You, H.: Applications of surface X-ray scattering to electrochemistry problems. Electrochim. Acta 47, 3037–3055 (2002)CrossRef Nagy, Z., You, H.: Applications of surface X-ray scattering to electrochemistry problems. Electrochim. Acta 47, 3037–3055 (2002)CrossRef
8.
go back to reference Tamura, K., Wang, J.X., Adzic, R.R., Ocko, B.M.: Kinetics of monolayer Bi electrodeposition on Au(111): surface X-ray scattering and current transients. J. Phys. Chem. B 108, 1992–1998 (2004)CrossRef Tamura, K., Wang, J.X., Adzic, R.R., Ocko, B.M.: Kinetics of monolayer Bi electrodeposition on Au(111): surface X-ray scattering and current transients. J. Phys. Chem. B 108, 1992–1998 (2004)CrossRef
9.
go back to reference Ayyad, A.H., Stettner, J., Magnussen, O.M.: Electrocompression of the Au(111) surface layer during Au electrodeposition. Phys. Rev. Lett. 94, 066106/1-066106/4 (2005) Ayyad, A.H., Stettner, J., Magnussen, O.M.: Electrocompression of the Au(111) surface layer during Au electrodeposition. Phys. Rev. Lett. 94, 066106/1-066106/4 (2005)
10.
go back to reference Krug, K., Stettner, J., Magnussen, O.M.: In situ surface X-ray diffraction studies of homoepitaxial electrochemical growth on Au(100). Phys. Rev. Lett. 96, 246101/1–246101/4 Krug, K., Stettner, J., Magnussen, O.M.: In situ surface X-ray diffraction studies of homoepitaxial electrochemical growth on Au(100). Phys. Rev. Lett. 96, 246101/1–246101/4
11.
go back to reference Kondo, T., Zegenhagen, J., Takakusagi, S., Uosaki, K.: In situ real-time study on potential induced structure change at Au(111) and Au(100) single crystal electrode/sulfuric acid solution interfaces by surface X-ray scattering. Surf. Sci. 631, 96–104 (2015)CrossRef Kondo, T., Zegenhagen, J., Takakusagi, S., Uosaki, K.: In situ real-time study on potential induced structure change at Au(111) and Au(100) single crystal electrode/sulfuric acid solution interfaces by surface X-ray scattering. Surf. Sci. 631, 96–104 (2015)CrossRef
12.
go back to reference Kondo, T., Masuda, T., Aoki, N., Uosaki, K.: Potential-dependent structures and potential-induced structure change at Pt(111) single-crystal electrode/sulfuric and perchloric acid interfaces in the potential region between hydrogen underpotential deposition and surface oxide formation by in situ surface X-ray scattering. J. Phys. Chem. C 120, 16118–16131 (2016)CrossRef Kondo, T., Masuda, T., Aoki, N., Uosaki, K.: Potential-dependent structures and potential-induced structure change at Pt(111) single-crystal electrode/sulfuric and perchloric acid interfaces in the potential region between hydrogen underpotential deposition and surface oxide formation by in situ surface X-ray scattering. J. Phys. Chem. C 120, 16118–16131 (2016)CrossRef
13.
go back to reference Lucas, C.A., Cormack, M., Gallagher, M.E., Brownrigg, A., Thompson, P., Fowler, B., Gründer, Y., Roy, J., Stamenković, V., Marković, N.M.: From ultra-high vacuum to the electrochemical interface: x-ray scattering studies of model electrocatalyst. Faraday Discuss. 140, 41–58 (2008)CrossRef Lucas, C.A., Cormack, M., Gallagher, M.E., Brownrigg, A., Thompson, P., Fowler, B., Gründer, Y., Roy, J., Stamenković, V., Marković, N.M.: From ultra-high vacuum to the electrochemical interface: x-ray scattering studies of model electrocatalyst. Faraday Discuss. 140, 41–58 (2008)CrossRef
14.
go back to reference Tripkovic, D.V., Strmcnik, D., van der Vliet, D., Stamenković, V., Marković, N.M.: The role of anions in surface electrochemistry. Faraday Discuss. 140, 25–40 (2008)CrossRef Tripkovic, D.V., Strmcnik, D., van der Vliet, D., Stamenković, V., Marković, N.M.: The role of anions in surface electrochemistry. Faraday Discuss. 140, 25–40 (2008)CrossRef
15.
go back to reference Marković, N.M., Ross Jr., P.N.: Surface science studies of model fuel cell electrocatalysts. Surf. Sci. Rep. 45, 117–229 (2002)CrossRef Marković, N.M., Ross Jr., P.N.: Surface science studies of model fuel cell electrocatalysts. Surf. Sci. Rep. 45, 117–229 (2002)CrossRef
16.
go back to reference Sisson, N., Gründer, Y., Lucas, C.A.: Structure and stability of underpotentially deposited Ag on Au(111) in alkaline electrolyte. J. Phys. Chem. C 120, 16100–16109 (2016)CrossRef Sisson, N., Gründer, Y., Lucas, C.A.: Structure and stability of underpotentially deposited Ag on Au(111) in alkaline electrolyte. J. Phys. Chem. C 120, 16100–16109 (2016)CrossRef
17.
go back to reference Kondo, T., Morita, J., Okamura, M., Saito, T., Uosaki, K.: In situ structural study on underpotential deposition of Ag on Au(111) electrode using surface X-ray scattering technique. J. Electroanal. Chem. 532, 201–205 (2002)CrossRef Kondo, T., Morita, J., Okamura, M., Saito, T., Uosaki, K.: In situ structural study on underpotential deposition of Ag on Au(111) electrode using surface X-ray scattering technique. J. Electroanal. Chem. 532, 201–205 (2002)CrossRef
18.
go back to reference Uosaki, K., Morita, J., Katsuzaki, T., Takakusagi, S., Tamura, K., Takahasi, M., Mizuki, J., Kondo, T.: In situ electrochemical, electrochemical quartz crystal microbalance, scanning tunneling microscopy, and surface X-ray scattering studies on Ag/AgCl reaction at the underpotentially deposited Ag bilayer on the Au(111) electrode surface. J. Phys. Chem. C 115, 12471–12482 (2011)CrossRef Uosaki, K., Morita, J., Katsuzaki, T., Takakusagi, S., Tamura, K., Takahasi, M., Mizuki, J., Kondo, T.: In situ electrochemical, electrochemical quartz crystal microbalance, scanning tunneling microscopy, and surface X-ray scattering studies on Ag/AgCl reaction at the underpotentially deposited Ag bilayer on the Au(111) electrode surface. J. Phys. Chem. C 115, 12471–12482 (2011)CrossRef
Metadata
Title
Electrochemical Surface X-Ray Scattering
Author
Toshihiro Kondo
Copyright Year
2018
Publisher
Springer Singapore
DOI
https://doi.org/10.1007/978-981-10-6156-1_18

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