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Journal of Materials Science
Published in: Journal of Materials Science 11/2007

01-06-2007

Influence of calcination conditions on phase formation and particle size of indium niobate powders synthesized by the solid-state reaction

Authors: S. Wongsaenmai, R. Yimnirun, S. Ananta

Published in: Journal of Materials Science | Issue 11/2007

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Abstract

A wolframite-type phase of indium niobate, InNbO4, has been synthesized by a solid-state reaction via a rapid vibro-milling technique. The formation of the InNbO4 phase in the calcined powders has been investigated as a function of calcination conditions by TG-DTA and XRD techniques. Morphology, particle size and chemical composition have been determined via a combination of SEM and EDX techniques. Single-phase InNbO4 powders have been obtained successfully for calcination condition of 900 °C for 4 h or 950 °C for 2 h with heating/cooling rates of 30 °C/min. Higher temperatures and longer dwell times clearly favoured particle growth and the formation of large and hard agglomerates.
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Metadata
Title
Influence of calcination conditions on phase formation and particle size of indium niobate powders synthesized by the solid-state reaction
Authors
S. Wongsaenmai
R. Yimnirun
S. Ananta
Publication date
01-06-2007
Published in
Journal of Materials Science / Issue 11/2007
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-006-0404-1

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