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Journal of Materials Science

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01-06-2007

Malic acid complex method for preparation of LiNiVO₄ nano-crystallites

Authors: Titipun Thongtem, Sulawan Kaowphong, Somchai Thongtem

Published in: Journal of Materials Science | Issue 11/2007

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Abstract

LiNiVO₄ nano-crystallites were prepared by the polymerized complex method using Li₂CO₃, Ni(CH₃COO)₂·4H₂O and NH₄VO₃ as starting reagents and malic acid as a complexing agent. With the subsequent calcination at 450 °C, the powder analyzed by XRD, FTIR, Raman, electron diffraction, SEM and TEM techniques was found to be inverse spinel LiNiVO₄ with ∼20 nm in diameter. TGA shows continuous weight loss at 40–450 °C due to the evaporation and decomposition processes. Above 450 °C, weight percent tended to be constant. In addition, formation mechanism of the purified LiNiVO₄ was proposed to relate with the experimental results.

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Title: Malic acid complex method for preparation of LiNiVO4 nano-crystallites
Authors: Titipun Thongtem
Sulawan Kaowphong
Somchai Thongtem
Publication date: 01-06-2007
Publisher: Kluwer Academic Publishers-Plenum Publishers
Published in: Journal of Materials Science / Issue 11/2007
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI: https://doi.org/10.1007/s10853-006-0402-3

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