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Published in: Journal of Materials Science 17/2019

28-05-2019 | Materials for life sciences

Microwave-assisted synthesis and simultaneous electrochemical determination of dopamine and paracetamol using ZIF-67-modified electrode

Authors: Nguyen Thi Thanh Tu, Phung Chi Sy, Tran Vinh Thien, Tran Thanh Tam Toan, Nguyen Hai Phong, Hoang Thai Long, Dinh Quang Khieu

Published in: Journal of Materials Science | Issue 17/2019

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Abstract

In the present research, zeolitic imidazolate framework-67 (ZIF-67) was synthesized through a microwave-assisted method and used as an electrode modifier for simultaneous determination of dopamine (DPM) and paracetamol (PRA). The as-prepared materials were characterized by X-ray diffractometry, scanning electron microscopy, nitrogen adsorption/desorption isotherms, and X-ray photoelectron spectroscopy. It was found that the proposed microwave-assisted approach required a short synthesis time and provided the ZIF-67 with excellent textural properties and high yield rate as compared to conventional hydrothermal processes. The as-synthesized ZIF-67 possessed excellent textural properties and manifested a superior electrocatalytic activity toward the oxidation of PRA and DPM. The electrochemical oxidation of DPM and PRA was investigated by both cyclic voltammetry and differential pulse voltammetry. The ZIF-67 modified electrode caused electrocatalytic oxidation of DPM and PRA in a linear response range from 2.0 × 10−6 to 22 × 10−6 M with the detection limits of 1.3 × 10−6 M and 1.4 × 10−6 M, respectively. A proposed method was successfully applied to analyze DMP and PRA in pharmaceutical preparations.

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Appendix
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Metadata
Title
Microwave-assisted synthesis and simultaneous electrochemical determination of dopamine and paracetamol using ZIF-67-modified electrode
Authors
Nguyen Thi Thanh Tu
Phung Chi Sy
Tran Vinh Thien
Tran Thanh Tam Toan
Nguyen Hai Phong
Hoang Thai Long
Dinh Quang Khieu
Publication date
28-05-2019
Publisher
Springer US
Published in
Journal of Materials Science / Issue 17/2019
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-019-03709-z

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