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Journal of Nanoparticle Research

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01-03-2012 | Brief Communication

One-pot reaction to synthesize superparamagnetic iron oxide nanoparticles by adding phenol as reducing agent and stabilizer

Authors: Yuanfeng Wang, Zhanwang Zhu, Feng Xu, Xinlin Wei

Published in: Journal of Nanoparticle Research | Issue 4/2012

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Abstract

An improved thermal decomposition method was used to directly prepare water-soluble Fe₃O₄ magnetic nanoparticles (MNPs) with relatively higher quality via reductive decomposition of ferric acetylacetonate [Fe(acac)₃], in the presence of benzyl ether and phenol, in which inexpensive phenol acted as reducing agent and stabilizer, produce the semi phenol-benzoquinone coated on the Fe₃O₄ and make the Fe₃O₄·MNPs water-soluble and the colloidal solution stable. By changing the molar ratio of phenol to Fe(acac)₃ and reaction time, the size of Fe₃O₄·MNPs could be varied from 19.3 ± 4.4 nm to 9.7 ± 1.5 nm, with the saturation magnetizations in the range of 51.3–62.9 emu/g.

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Title: One-pot reaction to synthesize superparamagnetic iron oxide nanoparticles by adding phenol as reducing agent and stabilizer
Authors: Yuanfeng Wang
Zhanwang Zhu
Feng Xu
Xinlin Wei
Publication date: 01-03-2012
Publisher: Springer Netherlands
Published in: Journal of Nanoparticle Research / Issue 4/2012
Print ISSN: 1388-0764
Electronic ISSN: 1572-896X
DOI: https://doi.org/10.1007/s11051-012-0755-2

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