Skip to main content
Top
Published in: Journal of Materials Science 8/2017

30-12-2016 | Original Paper

Physical properties of Fe films electrodeposited on porous Al substrates

Authors: M. Mebarki, A. Layadi, M. R. Khelladi, A. Azizi, N. Tiercelin, V. Preobrazhensky, P. Pernod

Published in: Journal of Materials Science | Issue 8/2017

Log in

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

Two series of Fe thin films have been electrodeposited onto polycrystalline porous Al substrates using two baths: iron chloride (FeCl2) and iron sulfate (FeSO4). The texture, strain, and grain size values have been derived from X-ray diffraction experiments. Scanning electron microscopy has been employed for surface morphology. The magnetic properties were inferred from hysteresis curves that were obtained from a vibrating sample magnetometer; the external magnetic field was applied in different directions of the film plane and also perpendicular to the film. Hysteresis curves have been obtained at low temperatures (120 K (−153 °C) to room temperature). We investigate the effects of Al porosity, bath type, and deposition rate on physical properties of these Fe films. A correlation between the structural and magnetic properties is made. Different mechanisms responsible for the coercive field (H C) behavior have also been investigated.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literature
1.
go back to reference Díaz SL, Calderón JA, Barcia OE, Mattos OR (2008) Electrodeposition of iron in sulphate solutions. Electrochim Acta 53:7426–7435CrossRef Díaz SL, Calderón JA, Barcia OE, Mattos OR (2008) Electrodeposition of iron in sulphate solutions. Electrochim Acta 53:7426–7435CrossRef
2.
go back to reference Su C, He F, Ju H, Zhang Y, Wang E (2009) Electrodeposition of Ni, Fe and Ni–Fe alloys on a 316 stainless steel surface in a fluorborate bath. Electrochim Acta 54:6257–6263CrossRef Su C, He F, Ju H, Zhang Y, Wang E (2009) Electrodeposition of Ni, Fe and Ni–Fe alloys on a 316 stainless steel surface in a fluorborate bath. Electrochim Acta 54:6257–6263CrossRef
3.
go back to reference Allongue P, Maroun F (2010) Electrodeposited magnetic layers in the ultrathin limit. MRS Bull 35:761CrossRef Allongue P, Maroun F (2010) Electrodeposited magnetic layers in the ultrathin limit. MRS Bull 35:761CrossRef
4.
go back to reference Izaki M (2010) Electrodeposition of iron and iron alloys. In: Schlesinger M, Paunovic M (eds) Modern electroplating, 5th edn. Wiley, Hoboken, pp 309–326 Izaki M (2010) Electrodeposition of iron and iron alloys. In: Schlesinger M, Paunovic M (eds) Modern electroplating, 5th edn. Wiley, Hoboken, pp 309–326
5.
go back to reference Park D-Y, Yoo BY, Kelcher S, Myung NV (2006) Electrodeposition of low-stress high magnetic moment Fe-rich FeCoNi thin films. Electrochim Acta 51:2523–2530CrossRef Park D-Y, Yoo BY, Kelcher S, Myung NV (2006) Electrodeposition of low-stress high magnetic moment Fe-rich FeCoNi thin films. Electrochim Acta 51:2523–2530CrossRef
6.
go back to reference Heinrich B, Purcell ST, Dutcher JR, Urquhart KB, Cochran JF, Arrott AS (1988) Structural and magnetic properties of ultrathin Ni/Fe bilayers grown epitaxiaiiy on Ag(001). Phys Rev 38:12879CrossRef Heinrich B, Purcell ST, Dutcher JR, Urquhart KB, Cochran JF, Arrott AS (1988) Structural and magnetic properties of ultrathin Ni/Fe bilayers grown epitaxiaiiy on Ag(001). Phys Rev 38:12879CrossRef
7.
go back to reference Layadi A, Artman JO, Hall BO, Hoffman RA, Jensen CL, Chakrabarti DJ, Saunders DA (1988) FMR in evaporated single and multilayer thin Fe films. J Appl Phys 64(10):5760–5762CrossRef Layadi A, Artman JO, Hall BO, Hoffman RA, Jensen CL, Chakrabarti DJ, Saunders DA (1988) FMR in evaporated single and multilayer thin Fe films. J Appl Phys 64(10):5760–5762CrossRef
8.
go back to reference Celinski Z, Uquhart KB, Heinrich B (1997) Using ferromagnetic resonance to measure the magnetic moments of ultrathin films. J Magn Magn Mater 166:6–26CrossRef Celinski Z, Uquhart KB, Heinrich B (1997) Using ferromagnetic resonance to measure the magnetic moments of ultrathin films. J Magn Magn Mater 166:6–26CrossRef
9.
go back to reference Rezende SM, Chesman C, Lucena MA, de Moura MC, Azevedo A, de Aguir FM (1999) Biquadratic coupling in sputtered Fe/Cr/Fe still in need of a new mechanism. J Appl Phys 85:5892–5894CrossRef Rezende SM, Chesman C, Lucena MA, de Moura MC, Azevedo A, de Aguir FM (1999) Biquadratic coupling in sputtered Fe/Cr/Fe still in need of a new mechanism. J Appl Phys 85:5892–5894CrossRef
10.
go back to reference Sadashivaiah PJ, Sankarappa T, Sujatha T, Santoshkumar R, Rawat P Sarvanan, Bhatnagar AK (2010) Structural, magnetic and electrical properties of Fe/Cu/Fe films. Vacuum 85(3):466–473CrossRef Sadashivaiah PJ, Sankarappa T, Sujatha T, Santoshkumar R, Rawat P Sarvanan, Bhatnagar AK (2010) Structural, magnetic and electrical properties of Fe/Cu/Fe films. Vacuum 85(3):466–473CrossRef
11.
go back to reference D’Orazio F, Gubbiotti G, Lucari F, Tassoni E (2002) Magnetic and structural properties of Fe/Al multilayers. J Magn Magn Mater 242–245:535–537CrossRef D’Orazio F, Gubbiotti G, Lucari F, Tassoni E (2002) Magnetic and structural properties of Fe/Al multilayers. J Magn Magn Mater 242–245:535–537CrossRef
12.
go back to reference Ghebouli B, Chérif S-M, Layadi A, Helifa B, Boudissa M (2007) Structural and magnetic properties of evaporated Fe thin films on Si(111), Si(100) and glass substrates. J Magn Magn Mater 312:194–199CrossRef Ghebouli B, Chérif S-M, Layadi A, Helifa B, Boudissa M (2007) Structural and magnetic properties of evaporated Fe thin films on Si(111), Si(100) and glass substrates. J Magn Magn Mater 312:194–199CrossRef
13.
go back to reference Mebarki M, Layadi A, Guittoum A, Benabbas A, Ghebouli B, Saad M, Menni N (2011) Structural and electrical properties of evaporated Fe thin films. Appl Surf Sci 257:7025–7029CrossRef Mebarki M, Layadi A, Guittoum A, Benabbas A, Ghebouli B, Saad M, Menni N (2011) Structural and electrical properties of evaporated Fe thin films. Appl Surf Sci 257:7025–7029CrossRef
14.
go back to reference Mebarki M, Layadi A, Kerkache L, Benabbas A, Tiercelin N, Preobrazhensky V, Pernod P (2014) Effect of thickness and deposition rate on the structural and magnetic properties of evaporated Fe/Al thin films. J Supercond Nov Magn 27(8):1951–1957CrossRef Mebarki M, Layadi A, Kerkache L, Benabbas A, Tiercelin N, Preobrazhensky V, Pernod P (2014) Effect of thickness and deposition rate on the structural and magnetic properties of evaporated Fe/Al thin films. J Supercond Nov Magn 27(8):1951–1957CrossRef
15.
go back to reference Mebarki M, Layadi A, Kerkache L, Tiercelin N, Preobrazhensky V, Pernod P (2015) Surface morphology and magnetic properties of evaporated Fe/Si and Fe/glass thin films. Appl Phys A 120(1):97–104CrossRef Mebarki M, Layadi A, Kerkache L, Tiercelin N, Preobrazhensky V, Pernod P (2015) Surface morphology and magnetic properties of evaporated Fe/Si and Fe/glass thin films. Appl Phys A 120(1):97–104CrossRef
16.
go back to reference Chen Gang, Cao Peng, He Yuehui, Shen Peizhi, Gao Haiyan (2012) Effect of aluminium evaporation loss on pore characteristics of porous FeAl alloys produced by vacuum sintering. J Mater Sci 47:1244–1250. doi:10.1007/s10853-011-5771-6 CrossRef Chen Gang, Cao Peng, He Yuehui, Shen Peizhi, Gao Haiyan (2012) Effect of aluminium evaporation loss on pore characteristics of porous FeAl alloys produced by vacuum sintering. J Mater Sci 47:1244–1250. doi:10.​1007/​s10853-011-5771-6 CrossRef
17.
go back to reference Osaka T (1999) Recent development of magnetic recording head core materials by plating method. Electrochim Acta 44(21):3885–3890CrossRef Osaka T (1999) Recent development of magnetic recording head core materials by plating method. Electrochim Acta 44(21):3885–3890CrossRef
18.
go back to reference Park D-Y, Myung NV, Schwartz M, Nobe K (2002) Nanostructured magnetic CoNiP electrodeposits: structure-property relationships. Electrochim Acta 47:2893–2900CrossRef Park D-Y, Myung NV, Schwartz M, Nobe K (2002) Nanostructured magnetic CoNiP electrodeposits: structure-property relationships. Electrochim Acta 47:2893–2900CrossRef
19.
go back to reference Chiu A, Croll I, Heim DE, Jones RE Jr, Kasiraj P, Klassen KB, Simmons CDRG (1996) Thin-film inductive heads. IBM J Res Dev 40(3):283–300CrossRef Chiu A, Croll I, Heim DE, Jones RE Jr, Kasiraj P, Klassen KB, Simmons CDRG (1996) Thin-film inductive heads. IBM J Res Dev 40(3):283–300CrossRef
20.
go back to reference Andricacos PC, Robertson N (1998) Future directions in electroplated materials for thin-film recording heads. IBM J Res Dev 42(5):671–680CrossRef Andricacos PC, Robertson N (1998) Future directions in electroplated materials for thin-film recording heads. IBM J Res Dev 42(5):671–680CrossRef
21.
go back to reference Protsenko VS, Vasil’eva EA, Smenova IV, Baskevich AS, Danilenko IA, Konstantinova TE, Danilov FI (2015) Electrodeposition of Fe and composite Fe/ZrO2 coatings from a methanesulfonate electrolyte. Surf Eng Appl Electrochem 51:65–75CrossRef Protsenko VS, Vasil’eva EA, Smenova IV, Baskevich AS, Danilenko IA, Konstantinova TE, Danilov FI (2015) Electrodeposition of Fe and composite Fe/ZrO2 coatings from a methanesulfonate electrolyte. Surf Eng Appl Electrochem 51:65–75CrossRef
22.
go back to reference Abd El Meguid EA, Abd El Rehim SS, Moustafa EM (2003) Electroplating of iron from alkaline gluconate baths. Thin Solid Films 443(1–2):53–59CrossRef Abd El Meguid EA, Abd El Rehim SS, Moustafa EM (2003) Electroplating of iron from alkaline gluconate baths. Thin Solid Films 443(1–2):53–59CrossRef
23.
go back to reference Hou XW, Liu SB, Yang SL, Li JP, Guo B (2013) Electrical and magnetic properties of electrodeposited Fe-based alloys used for thin film transformer. Sci China Technol Sci 56(1):84–88CrossRef Hou XW, Liu SB, Yang SL, Li JP, Guo B (2013) Electrical and magnetic properties of electrodeposited Fe-based alloys used for thin film transformer. Sci China Technol Sci 56(1):84–88CrossRef
24.
go back to reference Svedberg EB, Mallett JJ, Bendersky LA, Roy AG, Egelhoff WF Jr, Moffat TP (2006) A structural study of electrodeposited Fe on n-GaAs (001). J Electrochem Soc 153(12):C807–C813CrossRef Svedberg EB, Mallett JJ, Bendersky LA, Roy AG, Egelhoff WF Jr, Moffat TP (2006) A structural study of electrodeposited Fe on n-GaAs (001). J Electrochem Soc 153(12):C807–C813CrossRef
25.
go back to reference Motoyama M, Fukunaka Y, Sakka T, Ogatab YH (2006) Effect of surface pH on electrodeposited Ni films. J Electrochem Soc 153:C502–C508CrossRef Motoyama M, Fukunaka Y, Sakka T, Ogatab YH (2006) Effect of surface pH on electrodeposited Ni films. J Electrochem Soc 153:C502–C508CrossRef
26.
go back to reference Lallemand F, Ricq L, Wery M, Berc¸ot P, Pagetti J (2004) The influence of organic additives on the electrodeposition of iron-group metals and binary alloy from sulfate electrolyte. Appl Surf Sci 228:326–333CrossRef Lallemand F, Ricq L, Wery M, Berc¸ot P, Pagetti J (2004) The influence of organic additives on the electrodeposition of iron-group metals and binary alloy from sulfate electrolyte. Appl Surf Sci 228:326–333CrossRef
27.
29.
go back to reference Kim D, Park D-Y, Yoo BY, Sumodjo PTA, Myung NV (2003) Magnetic properties of nanocrystalline iron group thin film alloys electrodeposited from sulfate and chloride baths. Electrochim Acta 48(7):819–830CrossRef Kim D, Park D-Y, Yoo BY, Sumodjo PTA, Myung NV (2003) Magnetic properties of nanocrystalline iron group thin film alloys electrodeposited from sulfate and chloride baths. Electrochim Acta 48(7):819–830CrossRef
30.
go back to reference Gundel A, Devolder T, Chappert C, Schmidt JE, Cortes R, Allongue P (2004) Electrodeposition of Fe/Au(1 1 1) ultrathin layers with perpendicular magnetic anisotropy. Phys B 354(1–4):282–285CrossRef Gundel A, Devolder T, Chappert C, Schmidt JE, Cortes R, Allongue P (2004) Electrodeposition of Fe/Au(1 1 1) ultrathin layers with perpendicular magnetic anisotropy. Phys B 354(1–4):282–285CrossRef
31.
go back to reference Zarpellon J, Jurca HF, Klein JJ, Schreiner WH, Mattoso N, Mosca DH (2007) Electrodeposition of Fe thin films on Si(1 1 1) surfaces in the presence of sodium saccharin. Electrochim Acta 53:2002–2008CrossRef Zarpellon J, Jurca HF, Klein JJ, Schreiner WH, Mattoso N, Mosca DH (2007) Electrodeposition of Fe thin films on Si(1 1 1) surfaces in the presence of sodium saccharin. Electrochim Acta 53:2002–2008CrossRef
32.
go back to reference Jartych E, Zurawicz JK, Maczka E, Borc J (2001) Preparation of thin iron films by electrodeposition and characterization of their local magnetic properties. Mater Chem Phys 72(3):356–359CrossRef Jartych E, Zurawicz JK, Maczka E, Borc J (2001) Preparation of thin iron films by electrodeposition and characterization of their local magnetic properties. Mater Chem Phys 72(3):356–359CrossRef
33.
go back to reference Jartych E, Chocyk D, Budzynski M, Jalochoski M (2001) Surface morphology and local magnetic properties of electrodeposited thin iron layers. Appl Surf Sci 180(3):246–254CrossRef Jartych E, Chocyk D, Budzynski M, Jalochoski M (2001) Surface morphology and local magnetic properties of electrodeposited thin iron layers. Appl Surf Sci 180(3):246–254CrossRef
34.
go back to reference Mebarki M, Layadi A, Khelladi MR, Azizi A, Tiercelin N, Preobrazhensky V, Pernod P (2016) Structural and magnetic properties of Fe films electrodeposited on Al substrates. Metall Mater Trans A 47:3677–3683CrossRef Mebarki M, Layadi A, Khelladi MR, Azizi A, Tiercelin N, Preobrazhensky V, Pernod P (2016) Structural and magnetic properties of Fe films electrodeposited on Al substrates. Metall Mater Trans A 47:3677–3683CrossRef
35.
go back to reference Qin Xu, Yang Yuhua, Jianjun Gu, Li Ziyue, Sun Huiyuan (2012) Influence of Al substrate on the optical properties of porous anodic alumina films. Mater Lett 74:137–139CrossRef Qin Xu, Yang Yuhua, Jianjun Gu, Li Ziyue, Sun Huiyuan (2012) Influence of Al substrate on the optical properties of porous anodic alumina films. Mater Lett 74:137–139CrossRef
36.
go back to reference Koji H, Furuta H, Sekiya K, Nitta N, Harigai T, Hatta A (2013) Increased CNT growth density with an additional thin Ni layer on the Fe/Al catalyst film. Diam Relat Mater 36:1–7CrossRef Koji H, Furuta H, Sekiya K, Nitta N, Harigai T, Hatta A (2013) Increased CNT growth density with an additional thin Ni layer on the Fe/Al catalyst film. Diam Relat Mater 36:1–7CrossRef
37.
go back to reference Brajpuriya R (2010) Low temperature noncollinear behavior in ultrathin Fe/Al multilayer structures. J Appl Phys 107:083914CrossRef Brajpuriya R (2010) Low temperature noncollinear behavior in ultrathin Fe/Al multilayer structures. J Appl Phys 107:083914CrossRef
38.
go back to reference Budevski E, Staikow G, Lorenz WJ (2000) Electrocrystallization: Nucleation and growth phenomena. Electrochim Acta 45(15–16):2559–2574CrossRef Budevski E, Staikow G, Lorenz WJ (2000) Electrocrystallization: Nucleation and growth phenomena. Electrochim Acta 45(15–16):2559–2574CrossRef
39.
40.
go back to reference Herzer Giselher (2005) Anisotropies in soft magnetic nanocrystalline alloys. J Magn Magn Mater 294(2):99–106CrossRef Herzer Giselher (2005) Anisotropies in soft magnetic nanocrystalline alloys. J Magn Magn Mater 294(2):99–106CrossRef
41.
go back to reference Min H-G, Kim S-H, Li M, Wedding JB, Wang GC (1998) Thickness dependent coercivity of ultrathin co films on rough substrates: Cu buffered Si(111). Surf Sci 400:19–28CrossRef Min H-G, Kim S-H, Li M, Wedding JB, Wang GC (1998) Thickness dependent coercivity of ultrathin co films on rough substrates: Cu buffered Si(111). Surf Sci 400:19–28CrossRef
Metadata
Title
Physical properties of Fe films electrodeposited on porous Al substrates
Authors
M. Mebarki
A. Layadi
M. R. Khelladi
A. Azizi
N. Tiercelin
V. Preobrazhensky
P. Pernod
Publication date
30-12-2016
Publisher
Springer US
Published in
Journal of Materials Science / Issue 8/2017
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-016-0693-y

Other articles of this Issue 8/2017

Journal of Materials Science 8/2017 Go to the issue

Interfaces and Intergranular Boundaries

Structure of -tilt boundaries in cubic zirconia

Premium Partners