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Journal of Materials Science

Published in:

01-04-2007

Preparation and phase formation of perovskite Pb(Ni_1/3Nb_2/3)O₃ by a reaction-sintering process

Authors: Yi-Cheng Liou, Yi-Chen Huang, Chi-Ting Wu

Published in: Journal of Materials Science | Issue 8/2007

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Abstract

Pyrochlore-free Pb(Ni_1/3Nb_2/3)O₃ perovskite ceramics produced by a simple and effective reaction-sintering process were investigated. Without any calcination, the mixture of PbO, Ni(NO₃)₂ and Nb₂O₅ was pressed and sintered directly into PNN ceramics. Density of 98.5% of theoretical value was obtained after sintered at 1230 °C for 2 h in air. 99.3% of theoretical density was obtained after sintered at 1,200 °C for 2 h in PbO compensated atmosphere. PNN ceramic with dielectric constant 1,680 at 25 °C and 1 kHz has been obtained.

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Title: Preparation and phase formation of perovskite Pb(Ni1/3Nb2/3)O3 by a reaction-sintering process
Authors: Yi-Cheng Liou
Yi-Chen Huang
Chi-Ting Wu
Publication date: 01-04-2007
Publisher: Kluwer Academic Publishers-Plenum Publishers
Published in: Journal of Materials Science / Issue 8/2007
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI: https://doi.org/10.1007/s10853-006-1344-5

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