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Published in: Metallurgical and Materials Transactions A 3/2017

05-01-2017

Pressure- and Additive-Mediated Sintering of B4C at Relatively Low Temperatures

Authors: Ramasis Goswami, Syed B. Qadri, James Wollmershauser, Manoj K. Kolel-Veetil, Boris Feygelson

Published in: Metallurgical and Materials Transactions A | Issue 3/2017

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Abstract

A significant improvement in sinterability of B4C was achieved at a relatively low temperature by applying high pressure (2 GPa) and adding a small amount (5 wt pct) of Ni. The sintered B4C and Ni powder mixture showed improved hardness in the range of 21 to 32 GPa and improved modulus as compared to the sintered B4C powder without additive. This is mostly attributed to the formation of Ni4B3, as characterized by Reitveld refinement method and transmission electron microscopy (TEM), which enhances the bonding between B4C particles. These results provide a new avenue toward the development of sintering of B4C at relatively low temperatures (<0.5T m of B4C).

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Metadata
Title
Pressure- and Additive-Mediated Sintering of B4C at Relatively Low Temperatures
Authors
Ramasis Goswami
Syed B. Qadri
James Wollmershauser
Manoj K. Kolel-Veetil
Boris Feygelson
Publication date
05-01-2017
Publisher
Springer US
Published in
Metallurgical and Materials Transactions A / Issue 3/2017
Print ISSN: 1073-5623
Electronic ISSN: 1543-1940
DOI
https://doi.org/10.1007/s11661-016-3905-9

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