Skip to main content
Top
Published in: Journal of Materials Science 11/2007

01-06-2007

Processing of sucrose to low density carbon foams

Authors: K. Prabhakaran, P. K. Singh, N. M. Gokhale, S. C. Sharma

Published in: Journal of Materials Science | Issue 11/2007

Log in

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

A novel process for preparation low density carbon foams from sucrose has been demonstrated. A resin prepared by heating aqueous acidic sucrose solution when heated in an open Teflon mould at 120 °C undergoes foaming and then setting in to a solid organic foam. The solid organic foam undergoes carbonization in air by dehydration at 250 °C under isothermal condition. Carbon foams thus obtained sintered at temperature in the range 600–1,400 °C showed density in the range 115–145 mg/cc and electrical conductivity in the range 1.5 × 10−5 to 0.2 ohm−1 cm−1, respectively. The carbon foams contain spherical cells of size in the range 450–850 μm and the cells are interconnected through circular or oval shape windows of size in the range 80–300 μm. The carbon foam samples sintered at 1,400 °C showed compressive strength of 0.89 MPa.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literature
2.
go back to reference Knippenberg WF, Dersmacher B (1976) Philips Tech Rev 36:93 Knippenberg WF, Dersmacher B (1976) Philips Tech Rev 36:93
4.
go back to reference Klett RD (1975) High temperature insulating carbonaceous materials. US Patent 3,914,392 Klett RD (1975) High temperature insulating carbonaceous materials. US Patent 3,914,392
5.
go back to reference Bonzom A, Crepaux AP, Montard AMEJ (1981) Process for preparing pitch foams and products so produced. US Patent, 4,276,246 Bonzom A, Crepaux AP, Montard AMEJ (1981) Process for preparing pitch foams and products so produced. US Patent, 4,276,246
6.
go back to reference Marek R, Udichak W (1975) Foam carbonization and resulting structure. US Patent 3,922,334 Marek R, Udichak W (1975) Foam carbonization and resulting structure. US Patent 3,922,334
7.
go back to reference Vinton C, Franklin C (1975) Method for the preparation of carbon structure. US Patent 3,927,186 Vinton C, Franklin C (1975) Method for the preparation of carbon structure. US Patent 3,927,186
8.
go back to reference Spradling DM, Andrew Guth R (2003) Adv Mater Process 11:29 Spradling DM, Andrew Guth R (2003) Adv Mater Process 11:29
9.
10.
go back to reference Raley CF Jr, Asher DR (1976) Process for preparing macroporous open cell carbon foam from normally crystalline vinylidene chloride polymer. US Patent 3,960,770 Raley CF Jr, Asher DR (1976) Process for preparing macroporous open cell carbon foam from normally crystalline vinylidene chloride polymer. US Patent 3,960,770
11.
go back to reference Droege MW (1999) Low density open cell organic foam, low density carbon foams, and method for preparing the same. US Patent 5,945,084 Droege MW (1999) Low density open cell organic foam, low density carbon foams, and method for preparing the same. US Patent 5,945,084
12.
go back to reference Stankiewicz EP (2000) Method for producing controlled aspect ratio reticulated carbon foam and the resultant foam. US Patent 6,103,149 Stankiewicz EP (2000) Method for producing controlled aspect ratio reticulated carbon foam and the resultant foam. US Patent 6,103,149
13.
go back to reference Vinton CS, Franklin CH (1979) Activated reticulated or unreticulated carbon structures. US Patent 4,154,704 Vinton CS, Franklin CH (1979) Activated reticulated or unreticulated carbon structures. US Patent 4,154,704
14.
go back to reference Pekala RW (1989) Low density, resorcinol – formaldehyde aerogels. US Patent 4,873,218 Pekala RW (1989) Low density, resorcinol – formaldehyde aerogels. US Patent 4,873,218
15.
17.
go back to reference Inagaki M, Morishita T, Kuno A, Kito T, Hirano M, Suwa T, Kusakawa K (2004) Carbon 42:497CrossRef Inagaki M, Morishita T, Kuno A, Kito T, Hirano M, Suwa T, Kusakawa K (2004) Carbon 42:497CrossRef
18.
19.
go back to reference Klett RD (1975) High temperature insulating carbonaceous material. US Patent 3,914,392 Klett RD (1975) High temperature insulating carbonaceous material. US Patent 3,914,392
20.
go back to reference Nagle DC, Byrne CE (2003) Carbonized wood and materials formed therefrom. US Patent 6,670,039 Nagle DC, Byrne CE (2003) Carbonized wood and materials formed therefrom. US Patent 6,670,039
21.
go back to reference Stiller AH, Plucinski J, Yocum A (2003) Method of making carbon foam. US Patent 6,544,491 Stiller AH, Plucinski J, Yocum A (2003) Method of making carbon foam. US Patent 6,544,491
22.
go back to reference Fujii M, Minohata M (1990) Method for producing elastic graphite structures. US Patent 4,908,200 Fujii M, Minohata M (1990) Method for producing elastic graphite structures. US Patent 4,908,200
23.
go back to reference Hardcastle LA, Sheppard RG, Dingus DF (2003) Process for making carbon foam induced by process depressurization. US Patent 6,576,168 Hardcastle LA, Sheppard RG, Dingus DF (2003) Process for making carbon foam induced by process depressurization. US Patent 6,576,168
24.
go back to reference Klett JW (2003) Pitch-based carbon foam and composites. US Patent 6,663,842 Klett JW (2003) Pitch-based carbon foam and composites. US Patent 6,663,842
25.
go back to reference Yamada Y, Imamura T, Honda H, Fujii M, Minohata M (1989) Graphite structures and method for production thereof. US Patent 4,873,071 Yamada Y, Imamura T, Honda H, Fujii M, Minohata M (1989) Graphite structures and method for production thereof. US Patent 4,873,071
27.
go back to reference Klett JW, Mcmillan AD, Gallego NC, Burchell TD, Walls CA (2004) Carbon 42:1849CrossRef Klett JW, Mcmillan AD, Gallego NC, Burchell TD, Walls CA (2004) Carbon 42:1849CrossRef
29.
go back to reference Finar IL (1973) Organic chemistry volume. I. The fundamental principles. Longman, London, pp 503–530 Finar IL (1973) Organic chemistry volume. I. The fundamental principles. Longman, London, pp 503–530
30.
go back to reference Kinoshita K (1988) Carbon electrochemical and physical properties. Wiley & Sons, USA, pp 22–75 Kinoshita K (1988) Carbon electrochemical and physical properties. Wiley & Sons, USA, pp 22–75
32.
go back to reference Jenkins GM, Kawamura K (1976) Polymeric carbons, carbon fibers, glass and char. Cambridge University press, New York Jenkins GM, Kawamura K (1976) Polymeric carbons, carbon fibers, glass and char. Cambridge University press, New York
33.
go back to reference Long JC (1978) In: Grayson M (ed) Encyclopedia of chemical technology, vol 4. John Wiley and Sons, New York, pp 556–560 Long JC (1978) In: Grayson M (ed) Encyclopedia of chemical technology, vol 4. John Wiley and Sons, New York, pp 556–560
Metadata
Title
Processing of sucrose to low density carbon foams
Authors
K. Prabhakaran
P. K. Singh
N. M. Gokhale
S. C. Sharma
Publication date
01-06-2007
Published in
Journal of Materials Science / Issue 11/2007
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-006-0481-1

Other articles of this Issue 11/2007

Journal of Materials Science 11/2007 Go to the issue

Premium Partners