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Journal of Materials Science

Published in:

01-01-2008

Splitting behavior and structural transformation process of K₂Ti₆O₁₃ whiskers under hydrothermal conditions

Authors: Yaxin Zhou, Chang Liu, Ming He, Xiaohua Lu, Xin Feng, Zhuhong Yang

Published in: Journal of Materials Science | Issue 1/2008

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Abstract

The splitting behavior and structural transformation process of K₂Ti₆O₁₃ whiskers in various hydrothermal solutions were investigated by the X-ray diffraction technique, scanning electron microscopy, transmission electron microscopy, and atomic force microscopy. TiO₂ (B) particle aggregates and rutile twinned crystals were produced respectively in diluted and concentrated HCl solutions via “dissolution-precipitation” mechanism, while no changes were observed in deionized water. In contrary to the chemical inertia of K₂Ti₆O₁₃ whiskers in KOH solution, trititanate nanowires were synthesized by splitting the bulk K₂Ti₆O₁₃ whiskers in NaOH solution. The driving force for the formation of nanowires originated from the intrinsic strain induced by the phase transition from K₂Ti₆O₁₃with a tunnel structure to layered trititanate.

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Title: Splitting behavior and structural transformation process of K2Ti6O13 whiskers under hydrothermal conditions
Authors: Yaxin Zhou
Chang Liu
Ming He
Xiaohua Lu
Xin Feng
Zhuhong Yang
Publication date: 01-01-2008
Publisher: Springer US
Published in: Journal of Materials Science / Issue 1/2008
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI: https://doi.org/10.1007/s10853-007-2140-6

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