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Interceram - International Ceramic Review

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01-09-2018 | Research and Development

Synthesis and characterization of a sol-gel-derived zeolite prototype as a prospective hydrocracking catalyst

Authors: Dr. Sunanda Mukhopadhyay, Dr. Debarati Mitra, S. Kundu, D. Biswas, P. Das, M. SahaPoddar, S. Das

Published in: Interceram - International Ceramic Review | Issue 5/2018

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Abstract

This paper deals with the preparation and evaluation of a zeolite prototype developed from an aluminosilicate precursor for its possible application as a hydrocracking catalyst. Aluminium nitrate and tetraethyl orthosilicate at definite proportions were the primary reagents for the gel synthesis. Nickel loading and stipulated post-synthesis treatment of the material are also addressed in this paper. The characteristics of the calcined aluminosilicate gel were estimated using X-ray diffraction (XRD), scanning electron microscope (SEM) study with energy dispersive spectroscopy (EDS), differential thermal analysis (DTA) with thermogravimetry (TG) and Fourier-transformed infrared spectroscopy (FTIR) at different temperatures. A preliminary laboratory-scale investigation of hydrocracking performance of this zeolite prototype was also conducted.

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Title: Synthesis and characterization of a sol-gel-derived zeolite prototype as a prospective hydrocracking catalyst
Authors: Dr. Sunanda Mukhopadhyay
Dr. Debarati Mitra
S. Kundu
D. Biswas
P. Das
M. SahaPoddar
S. Das
Publication date: 01-09-2018
Publisher: Springer Fachmedien Wiesbaden
Published in: Interceram - International Ceramic Review / Issue 5/2018
Print ISSN: 0020-5214
Electronic ISSN: 2523-8957
DOI: https://doi.org/10.1007/s42411-018-0031-2

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