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Published in: Metallurgical and Materials Transactions A 2/2011

01-02-2011

The Mechanism of Grain Coarsening in Friction-Stir-Welded AA5083 after Heat Treatment

Authors: Ke Chen, Wei Gan, K. Okamoto, Kwansoo Chung, R. H. Wagoner

Published in: Metallurgical and Materials Transactions A | Issue 2/2011

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Abstract

Friction stir welding (FSW) takes place in the solid state, thus providing potential advantages of welds of high strength and ductility because of fine microstructures. However, post-FSW heat treatment can create very coarse grains, potentially reducing mechanical properties. AA5083-H18 sheets were friction-stir butt welded using three sets of welding parameters representing a wide range of heat input. They were then heat treated for 5 minutes at 738 K (465 °C), producing grain sizes exceeding 100 μm near the top weld surfaces, with the coarse grains extending toward the bottom surface to various degrees depending on the welding parameters. Electron backscatter diffraction (EBSD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), optical metallography, inductively coupled plasma–mass spectrometry, and Vickers hardness testing were used to characterize the regions within welds. Particle pinning was determined quantitatively and used with Humphreys’ model of grain growth to interpret the behavior. The mechanism responsible for forming the large grains was identified as abnormal grain growth (AGG), with AGG occurring only for regions with pre-heat-treatment grain sizes smaller than 3 μm. Second-phase particle volume fractions and sizes, textures, and solute concentrations were not significantly different in AGG and non-AGG regions. Ultrafine grain layers with grain diameters of 0.3 mm were characterized and had high densities of pinning particles of MgSi2, Al2O3, and Mg5Al8. Strategies to eliminate AGG by alloy and weld process design were discussed.

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Footnotes
1
The terms nucleation and nuclei are used here to be consistent with most of the literature, but these terms do not imply thermal fluctuation or the formation of atom-by-atom construction.
 
2
Color figures are presented in the on-line version of this article.
 
3
Figures 3 and 4 are taken from Ref. 90 and used with permission of the J. Eng. Mater. Technol.-Trans. ASME.
 
4
OIM is a trademark of TSL, Inc., Draper, UT.
 
5
PHILIPS is a trademark of FEI Company, Hillsboro, OR.
 
6
The hardness measurements closest to the bottom of the sheet were excluded because they differ sharply from the remainder of the region.
 
7
The uncertainty is determined via three adjacent scans on the H1 and H3 middle regions. The standard deviation is calculated for each location.
 
8
The possibility that significant NGG occurs during QPF was eliminated by measuring before-and-after grain sizes for H2-M. These were found to be 3.5 and 3.7 μm, respectively, identical within the 4 pct scatter of the measurement.
 
9
To check if Eq. [8] can be reasonably applied particle by particle, an alternate analysis was carried out by assuming a normal distribution of particle sizes with average and standard deviation corresponding to the measured population. The dispersion was identical, 0.11 μm–1. A simple number average of particle sizes, as sometimes seen in the literature, yielded a value of 0.15 μm–1.
 
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Metadata
Title
The Mechanism of Grain Coarsening in Friction-Stir-Welded AA5083 after Heat Treatment
Authors
Ke Chen
Wei Gan
K. Okamoto
Kwansoo Chung
R. H. Wagoner
Publication date
01-02-2011
Publisher
Springer US
Published in
Metallurgical and Materials Transactions A / Issue 2/2011
Print ISSN: 1073-5623
Electronic ISSN: 1543-1940
DOI
https://doi.org/10.1007/s11661-010-0426-9

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