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Published in: Applied Composite Materials 1/2019

04-05-2018

A Comparison of the Properties of Carbon Fiber Epoxy Composites Produced by Non-autoclave with Vacuum Bag Only Prepreg and Autoclave Process

Authors: Sang Yoon Park, Chi Hoon Choi, Won Jong Choi, Seong Soon Hwang

Published in: Applied Composite Materials | Issue 1/2019

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Abstract

The non-autoclave curing technique with vacuum bag only (VBO) prepreg has been conceived as a cost-effective manufacturing method for producing high-quality composite part. This study demonstrated the feasibility of improving composite part’s performances and established the effective mitigation strategies for manufacturing induced defects, such as internal voids and surface porosity. The experimental results highlighted the fact that voids and surface porosity were clearly dependent on the resin viscosity state at an intermediate dwell stage of the curing process. Thereafter, the enhancement of resin flow could lead to achieving high quality parts with minimal void content (1.3%) and high fiber fraction (53 vol.%). The mechanical testing showed comparable in-plane shear and compressive strength to conventional autoclave. The microscopic observations also supported the evidence of improved interfacial bonding in terms of excellent fiber wet-out and minimal void content for the optimized cure cycle condition.

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Literature
1.
go back to reference Varvani-Farahani, A.: Composite materials: characterization, fabrication and application-research challenges and directions. Appl. Compos. Mater. 17(2), 63–67 (2010)CrossRef Varvani-Farahani, A.: Composite materials: characterization, fabrication and application-research challenges and directions. Appl. Compos. Mater. 17(2), 63–67 (2010)CrossRef
2.
go back to reference Lachaud, F., Espinosa, C., Michel, L., Rahme, P., Piquet, R.: Modelling strategies for predicting the residual strength of impacted composite aircraft fuselages. Appl. Compos. Mater. 22(6), 599–621 (2015)CrossRef Lachaud, F., Espinosa, C., Michel, L., Rahme, P., Piquet, R.: Modelling strategies for predicting the residual strength of impacted composite aircraft fuselages. Appl. Compos. Mater. 22(6), 599–621 (2015)CrossRef
3.
go back to reference Alderliesten, R.C.: Critical review on the assessment of fatigue and fracture in composite materials and structures. Eng. Fail. Anal. 35(15), 370–379 (2013)CrossRef Alderliesten, R.C.: Critical review on the assessment of fatigue and fracture in composite materials and structures. Eng. Fail. Anal. 35(15), 370–379 (2013)CrossRef
4.
go back to reference Grunenfelder, L.K., Dills, A., Centea, T., Nutt, S.R.: Effect of prepreg format on defect control in out-of-autoclave processing. Compos. A: Appl. Sci. Manuf. 93, 88–99 (2017)CrossRef Grunenfelder, L.K., Dills, A., Centea, T., Nutt, S.R.: Effect of prepreg format on defect control in out-of-autoclave processing. Compos. A: Appl. Sci. Manuf. 93, 88–99 (2017)CrossRef
5.
go back to reference Aleksendrić, D., Carlone, P., Ćirović, V.: Optimization of the temperature-time curve for the curing process of thermoset matrix composites. Appl. Compos. Mater. 23(5), 1047–1063 (2016)CrossRef Aleksendrić, D., Carlone, P., Ćirović, V.: Optimization of the temperature-time curve for the curing process of thermoset matrix composites. Appl. Compos. Mater. 23(5), 1047–1063 (2016)CrossRef
6.
go back to reference Bodaghi, M., Cristóvão, C., Gomes, R., Correia, N.C.: Experimental characterization of voids in high fibre volume fraction composites processed by high injection pressure RTM. Compos Part A. Appl. Sci. Manuf. 82, 88–99 (2016)CrossRef Bodaghi, M., Cristóvão, C., Gomes, R., Correia, N.C.: Experimental characterization of voids in high fibre volume fraction composites processed by high injection pressure RTM. Compos Part A. Appl. Sci. Manuf. 82, 88–99 (2016)CrossRef
7.
go back to reference Marsh, G.: De-autoclaving’ prepreg processing. Reinf. Plast. 56(5), 20–25 (2012)CrossRef Marsh, G.: De-autoclaving’ prepreg processing. Reinf. Plast. 56(5), 20–25 (2012)CrossRef
8.
go back to reference Xu, X., Wang, X., Liu, W., Zhang, X., Li, Z., Du, S.: Microwave curing of carbon fiber/bismaleimide composite laminates: material characterization and hot pressing pretreatment. Mater. Des. 97(5), 316–323 (2016)CrossRef Xu, X., Wang, X., Liu, W., Zhang, X., Li, Z., Du, S.: Microwave curing of carbon fiber/bismaleimide composite laminates: material characterization and hot pressing pretreatment. Mater. Des. 97(5), 316–323 (2016)CrossRef
9.
go back to reference Grunenfelder, L.K., Nutt, S.R.: Void formation in composite prepregs – effect of dissolved moisture. Compos. Sci. Technol. 70(16), 2304–2309 (2010)CrossRef Grunenfelder, L.K., Nutt, S.R.: Void formation in composite prepregs – effect of dissolved moisture. Compos. Sci. Technol. 70(16), 2304–2309 (2010)CrossRef
10.
go back to reference Helmus, R., Centea, T., Hubert, P., Hinterhölzl, R.: Out-of-autoclave prepreg consolidation: coupled air evacuation and prepreg impregnation modeling. J. Compos. Mater. 50(10), 1403–1413 (2015)CrossRef Helmus, R., Centea, T., Hubert, P., Hinterhölzl, R.: Out-of-autoclave prepreg consolidation: coupled air evacuation and prepreg impregnation modeling. J. Compos. Mater. 50(10), 1403–1413 (2015)CrossRef
11.
go back to reference Garschke, C., Weimer, C., Parlevliet, P.P., Fox, B.L.: Out-of-autoclave cure cycle study of a resin film infusion process using in situ process monitoring. Compos Part A. Appl. Sci. Manuf. 43(6), 935–944 (2012)CrossRef Garschke, C., Weimer, C., Parlevliet, P.P., Fox, B.L.: Out-of-autoclave cure cycle study of a resin film infusion process using in situ process monitoring. Compos Part A. Appl. Sci. Manuf. 43(6), 935–944 (2012)CrossRef
12.
go back to reference Han, K., Jiang, S., Zhang, C., Wang, B.: Flow modeling and simulation of SCRIMP for composites manufacturing. Compos Part A. Appl. Sci. Manuf. 31(1), 79–86 (2000)CrossRef Han, K., Jiang, S., Zhang, C., Wang, B.: Flow modeling and simulation of SCRIMP for composites manufacturing. Compos Part A. Appl. Sci. Manuf. 31(1), 79–86 (2000)CrossRef
13.
go back to reference Li, W., Krehl, J., Gillespie, J.W., Heider, D., Endrulat, M., Hochrein, K., Dunham, M.G., Dubois, C.J.: Process and performance evaluation of the vacuum-assisted process. J. Compos. Mater. 38(20), 1803–1814 (2004)CrossRef Li, W., Krehl, J., Gillespie, J.W., Heider, D., Endrulat, M., Hochrein, K., Dunham, M.G., Dubois, C.J.: Process and performance evaluation of the vacuum-assisted process. J. Compos. Mater. 38(20), 1803–1814 (2004)CrossRef
14.
go back to reference Centea, T., Nutt, S.R.: Manufacturing cost relationships for vacuum bag-only prepreg processing. J. Compos. Mater. 50(17), 2305–2321 (2015)CrossRef Centea, T., Nutt, S.R.: Manufacturing cost relationships for vacuum bag-only prepreg processing. J. Compos. Mater. 50(17), 2305–2321 (2015)CrossRef
15.
go back to reference Thomas, S., Nutt, S.R.: Temperature dependence of resin flow in a resin film infusion (RFI) process by ultrasound imaging. Appl. Compos. Mater. 16(3), 183–196 (2009)CrossRef Thomas, S., Nutt, S.R.: Temperature dependence of resin flow in a resin film infusion (RFI) process by ultrasound imaging. Appl. Compos. Mater. 16(3), 183–196 (2009)CrossRef
16.
go back to reference Ridgard, C.: Out of autoclave composite technology for aerospace, defense and space structures. In: Proceeding of SAMPE Conference, Baltimore, MD (2009) Ridgard, C.: Out of autoclave composite technology for aerospace, defense and space structures. In: Proceeding of SAMPE Conference, Baltimore, MD (2009)
17.
go back to reference Ridgard, C.: Next generation out of autoclave systems. In: Proceeding of SAMPE Conference, Seattle, WA (2010) Ridgard, C.: Next generation out of autoclave systems. In: Proceeding of SAMPE Conference, Seattle, WA (2010)
18.
go back to reference Kratz, J., Hsiao, K., Fernlund, G., Hubert, P.: Thermal models for MTM45-1 and Cycom 5320 out-of-autoclave prepreg resins. J. Compos. Mater. 47, 341–352 (2012)CrossRef Kratz, J., Hsiao, K., Fernlund, G., Hubert, P.: Thermal models for MTM45-1 and Cycom 5320 out-of-autoclave prepreg resins. J. Compos. Mater. 47, 341–352 (2012)CrossRef
19.
go back to reference Agius, S.L., Magniez, K.J.C., Fox, B.L.: Cure behaviour and void development within rapidly cured out-of-autoclave composites. Compos. Part B. 47, 230–237 (2013)CrossRef Agius, S.L., Magniez, K.J.C., Fox, B.L.: Cure behaviour and void development within rapidly cured out-of-autoclave composites. Compos. Part B. 47, 230–237 (2013)CrossRef
20.
go back to reference Cong, J., Zhang, B.: Methodology for evaluating manufacturability of composite materials. Appl. Compos. Mater. 19(3–4), 189–201 (2012)CrossRef Cong, J., Zhang, B.: Methodology for evaluating manufacturability of composite materials. Appl. Compos. Mater. 19(3–4), 189–201 (2012)CrossRef
21.
go back to reference Guo, Z.S., Liu, L., Zhang, B.M., Du, S.: Critical void content for thermoset composite laminates. J. Compos. Mater. 43(17), 1775–1790 (2006) Guo, Z.S., Liu, L., Zhang, B.M., Du, S.: Critical void content for thermoset composite laminates. J. Compos. Mater. 43(17), 1775–1790 (2006)
22.
go back to reference Hernández, S., Sket, F., González, C., Llorca, J.: Optimization of curing cycle in carbon fiber-reinforced laminates: void distribution and mechanical properties. Compos. Sci. Technol. 85(21), 73–82 (2013)CrossRef Hernández, S., Sket, F., González, C., Llorca, J.: Optimization of curing cycle in carbon fiber-reinforced laminates: void distribution and mechanical properties. Compos. Sci. Technol. 85(21), 73–82 (2013)CrossRef
23.
go back to reference Jeong, H.: Effects of voids on the mechanical strength and ultrasonic attenuation of laminated composites. J. Compos. Mater. 31(3), 276–292 (1997)CrossRef Jeong, H.: Effects of voids on the mechanical strength and ultrasonic attenuation of laminated composites. J. Compos. Mater. 31(3), 276–292 (1997)CrossRef
24.
go back to reference Park, S.Y., Choi, W.J., Choi, H.S.: The effects of void contents on the long-term hygrothermal behaviors of glass/epoxy and GLARE laminates. Compos. Struct. 92(1), 18–24 (2010)CrossRef Park, S.Y., Choi, W.J., Choi, H.S.: The effects of void contents on the long-term hygrothermal behaviors of glass/epoxy and GLARE laminates. Compos. Struct. 92(1), 18–24 (2010)CrossRef
25.
go back to reference Costa, M.L., Rezende, M.C., De Almeida, S.F.M.: Strength of hygrothermally conditioned polymer composites with voids. J. Compos. Mater. 39(21), 1943–1961 (2005)CrossRef Costa, M.L., Rezende, M.C., De Almeida, S.F.M.: Strength of hygrothermally conditioned polymer composites with voids. J. Compos. Mater. 39(21), 1943–1961 (2005)CrossRef
26.
go back to reference Pang, K.P., Gillham, J.K.: Competition between cure and thermal degradation in a high Tg epoxy system: effect of time and temperature of isothermal cure on the glass transition temperature. J. Appl. Polym. Sci. 39(4), 909–933 (1990)CrossRef Pang, K.P., Gillham, J.K.: Competition between cure and thermal degradation in a high Tg epoxy system: effect of time and temperature of isothermal cure on the glass transition temperature. J. Appl. Polym. Sci. 39(4), 909–933 (1990)CrossRef
27.
go back to reference Yenilmez, B., Senan, M., Sozer, E.M.: Variation of part thickness and compaction pressure in vacuum infusion process. Compos. Sci. Technol. 69(11–12), 1710–1719 (2009)CrossRef Yenilmez, B., Senan, M., Sozer, E.M.: Variation of part thickness and compaction pressure in vacuum infusion process. Compos. Sci. Technol. 69(11–12), 1710–1719 (2009)CrossRef
28.
go back to reference Kim, D., Centea, T., Nutt, S.R.: Out-time effects on cure kinetics and viscosity for an out-of-autoclave (OOA) prepreg: modelling and monitoring. Compos. Sci. Technol. 100(21), 63–69 (2014)CrossRef Kim, D., Centea, T., Nutt, S.R.: Out-time effects on cure kinetics and viscosity for an out-of-autoclave (OOA) prepreg: modelling and monitoring. Compos. Sci. Technol. 100(21), 63–69 (2014)CrossRef
29.
go back to reference Kim, D., Centea, T., Nutt, S.R.: Effects of out-time on viscosity, gelation and vitrification. Compos. Sci. Technol. 102(6), 132–138 (2014)CrossRef Kim, D., Centea, T., Nutt, S.R.: Effects of out-time on viscosity, gelation and vitrification. Compos. Sci. Technol. 102(6), 132–138 (2014)CrossRef
30.
go back to reference Garschke, C., Parlevliet, P.P., Weimer, C., Fox, B.L.: Cure kinetics and viscosity modelling of a high-performance epoxy resin film. Polym. Test. 32(1), 150–157 (2013)CrossRef Garschke, C., Parlevliet, P.P., Weimer, C., Fox, B.L.: Cure kinetics and viscosity modelling of a high-performance epoxy resin film. Polym. Test. 32(1), 150–157 (2013)CrossRef
31.
go back to reference AITM 3-0002. Analysis of non metallic materials (uncured) by differential scanning calorimetry. Airbus Industry, France (1997) AITM 3-0002. Analysis of non metallic materials (uncured) by differential scanning calorimetry. Airbus Industry, France (1997)
32.
go back to reference Abouhamzeh, M., Sinke, J., Jansen, K.M.B., Benedictus, R.: Kinetic and thermo-viscoelastic characterisation of the epoxy adhesive in GLARE. Compos. Struct. 124, 19–28 (2015)CrossRef Abouhamzeh, M., Sinke, J., Jansen, K.M.B., Benedictus, R.: Kinetic and thermo-viscoelastic characterisation of the epoxy adhesive in GLARE. Compos. Struct. 124, 19–28 (2015)CrossRef
33.
go back to reference Xie, M., Zhang, Z., Gu, Y., Li, M., Su, Y.: A new method to characterize the cure state of epoxy prepreg by dynamic mechanical analysis. Thermochim. Acta. 487(1–2), 8–17 (2009)CrossRef Xie, M., Zhang, Z., Gu, Y., Li, M., Su, Y.: A new method to characterize the cure state of epoxy prepreg by dynamic mechanical analysis. Thermochim. Acta. 487(1–2), 8–17 (2009)CrossRef
34.
go back to reference Boey, F.Y.C., Qiang, W.: Experimental modeling of the cure kinetics of an epoxy-hexaanhydro-4-methylphthalicanhydride (MHHPA) system. Polymer. 41, 2081–2094 (2000)CrossRef Boey, F.Y.C., Qiang, W.: Experimental modeling of the cure kinetics of an epoxy-hexaanhydro-4-methylphthalicanhydride (MHHPA) system. Polymer. 41, 2081–2094 (2000)CrossRef
35.
go back to reference Alavi-Soltani, S., Sabzevari, S., Koushyar, H., Minaie, B.: Thermal, rheological, and mechanical properties of a polymer composite cured at different isothermal cure temperatures. J. Compos. Mater. 46(5), 575–587 (2011)CrossRef Alavi-Soltani, S., Sabzevari, S., Koushyar, H., Minaie, B.: Thermal, rheological, and mechanical properties of a polymer composite cured at different isothermal cure temperatures. J. Compos. Mater. 46(5), 575–587 (2011)CrossRef
36.
go back to reference ASTM D3529/D3529M-97: Standard test method for matrix solids content and matrix content of composite prepreg. ASTM International, West Conshohocken (1997) ASTM D3529/D3529M-97: Standard test method for matrix solids content and matrix content of composite prepreg. ASTM International, West Conshohocken (1997)
37.
go back to reference ASTM D3530-97: Standard test method for volatiles content of composite material prepreg. ASTM International, West Conshohocken (2015) ASTM D3530-97: Standard test method for volatiles content of composite material prepreg. ASTM International, West Conshohocken (2015)
38.
go back to reference Hamill, L., Centea, T., Nutt, S.R.: Surface porosity during vacuum bag-only prepreg processing: Causes and mitigation strategies. Compos Part A. Appl. Sci. Manuf. 7, 1–10 (2015)CrossRef Hamill, L., Centea, T., Nutt, S.R.: Surface porosity during vacuum bag-only prepreg processing: Causes and mitigation strategies. Compos Part A. Appl. Sci. Manuf. 7, 1–10 (2015)CrossRef
39.
go back to reference Tomblin, J.S., Ng, Y.C., Raju, K.S.: Material qualification and equivalency for polymer matrix composite material systems: updated procedure (report no.: DOT/FAA/AR-03/19). U.S. Department of Transportation, Washington, D.C (2003) Tomblin, J.S., Ng, Y.C., Raju, K.S.: Material qualification and equivalency for polymer matrix composite material systems: updated procedure (report no.: DOT/FAA/AR-03/19). U.S. Department of Transportation, Washington, D.C (2003)
40.
go back to reference ASTM D792-13: Standard test methods for density and specific gravity (relative density) of plastics by displacement. ASTM International, West Conshohocken (2013) ASTM D792-13: Standard test methods for density and specific gravity (relative density) of plastics by displacement. ASTM International, West Conshohocken (2013)
41.
go back to reference ASTM D3171-15: Standard test methods for constituent content of composite materials. ASTM International, West Conshohocken (2015) ASTM D3171-15: Standard test methods for constituent content of composite materials. ASTM International, West Conshohocken (2015)
42.
go back to reference ASTM D2734-16: Standard test methods for void content of reinforced plastics. ASTM International, West Conshohocken (2016) ASTM D2734-16: Standard test methods for void content of reinforced plastics. ASTM International, West Conshohocken (2016)
43.
go back to reference AITM1-0003. Determination of the glass transition temperatures (DMA). Airbus Industry, France (1997) AITM1-0003. Determination of the glass transition temperatures (DMA). Airbus Industry, France (1997)
44.
go back to reference ASTM D3518-13: Standard test methods for in-plane shear response of polymer matrix composite materials by tensile test of a ±45° laminate. ASTM International, West Conshohocken (2013) ASTM D3518-13: Standard test methods for in-plane shear response of polymer matrix composite materials by tensile test of a ±45° laminate. ASTM International, West Conshohocken (2013)
45.
go back to reference ASTM D6641-16: Standard test methods for compressive properties of polymer matrix composite materials using a combined loading compression (CLC) test fixture. ASTM International, West Conshohocken (2016) ASTM D6641-16: Standard test methods for compressive properties of polymer matrix composite materials using a combined loading compression (CLC) test fixture. ASTM International, West Conshohocken (2016)
46.
go back to reference MIL-HDBK-17-1F. Composite materials handbook, Volume 1, polymer matrix composites guidelines for characterization of structural materials. U.S. Department of Defense, Washington, D.C (2002) MIL-HDBK-17-1F. Composite materials handbook, Volume 1, polymer matrix composites guidelines for characterization of structural materials. U.S. Department of Defense, Washington, D.C (2002)
47.
go back to reference Costa, M.L., Rezende, M.C., Almeida, S.F.M.: Effect of void content on the moisture absorption in polymeric composites. Polym. Plast. Technol. Eng. 45(6), 691–698 (2006)CrossRef Costa, M.L., Rezende, M.C., Almeida, S.F.M.: Effect of void content on the moisture absorption in polymeric composites. Polym. Plast. Technol. Eng. 45(6), 691–698 (2006)CrossRef
48.
go back to reference Liu, L., Zhang, B.M., Wang, D.F., Wu, Z.J.: Effects of cure cycles on void content and mechanical properties of composite laminates. Compos. Struct. 73(3), 303–309 (2006)CrossRef Liu, L., Zhang, B.M., Wang, D.F., Wu, Z.J.: Effects of cure cycles on void content and mechanical properties of composite laminates. Compos. Struct. 73(3), 303–309 (2006)CrossRef
49.
go back to reference Choi, H.S., Ahn, K.J., Nam, J.D., Chun, H.J.: Hygroscopic aspects of epoxy/carbon fiber composite laminates in aircraft environments. Compos Part A. Appl. Sci. Manuf. 32(5), 709–720 (2001)CrossRef Choi, H.S., Ahn, K.J., Nam, J.D., Chun, H.J.: Hygroscopic aspects of epoxy/carbon fiber composite laminates in aircraft environments. Compos Part A. Appl. Sci. Manuf. 32(5), 709–720 (2001)CrossRef
Metadata
Title
A Comparison of the Properties of Carbon Fiber Epoxy Composites Produced by Non-autoclave with Vacuum Bag Only Prepreg and Autoclave Process
Authors
Sang Yoon Park
Chi Hoon Choi
Won Jong Choi
Seong Soon Hwang
Publication date
04-05-2018
Publisher
Springer Netherlands
Published in
Applied Composite Materials / Issue 1/2019
Print ISSN: 0929-189X
Electronic ISSN: 1573-4897
DOI
https://doi.org/10.1007/s10443-018-9688-y

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