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Journal of Materials Science

Published in:

01-01-2010

A novel chemical reduction route toward fabrication of Fe₃O₄ octahedrons and Fe tubes

Authors: DongEn Zhang, Wei Wu, ShanZhong Li, XiaoBo Zhang, GuiQuan Han, Ailing Ying, JunYan Gong, ZhiWei Tong

Published in: Journal of Materials Science | Issue 1/2010

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Abstract

Novel Fe₃O₄ octahedrons and Fe microtubes were successfully prepared in different alkaline concentration solutions by the reduction of hematite (α-Fe₂O₃) with hydrazine hydrate. The as-prepared powders were characterized in detail by conventional techniques such as X-ray diffraction and field emission scanning electron microscopy. The role of alkaline concentration during the reaction process is discussed in detail. Compared to the reaction in a water system, the reaction in ethanol required less sodium hydroxide and smaller particles were obtained. In addition, the magnetic properties of the samples were characterized using a vibrating sample magnetometer.

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Title: A novel chemical reduction route toward fabrication of Fe3O4 octahedrons and Fe tubes
Authors: DongEn Zhang
Wei Wu
ShanZhong Li
XiaoBo Zhang
GuiQuan Han
Ailing Ying
JunYan Gong
ZhiWei Tong
Publication date: 01-01-2010
Publisher: Springer US
Published in: Journal of Materials Science / Issue 1/2010
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI: https://doi.org/10.1007/s10853-009-3866-0

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