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Journal of Materials Science
Published in: Journal of Materials Science 6/2014

01-03-2014

Colloidal particles with various glass transition temperatures: preparation, assembly, and the properties of stop bands under heat treatment

Authors: Chunmei Li, Baoliang Zhang, Jiaojun Tan, Xinlong Fan, Yali Liu, Hepeng Zhang, Qiuyu Zhang

Published in: Journal of Materials Science | Issue 6/2014

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Abstract

Monodisperse P(St-co-nBA-co-AA) colloidal microspheres with various glass transition temperatures (T gs), whose average particle sizes were about 300 nm, were prepared using soap-free emulsion polymerization by adjusting the ratio of styrene and n-butyl acrylate. Colloidal photonic crystals were assembled with these microspheres by vertical deposition method. Stop bands of colloidal crystals under different temperatures have been characterized. The relationship between the stop band and temperature was indicated. The microstructure and reflectance spectra of photonic crystals were characterized by SEM and fiber spectrometer, respectively. Results showed that as the temperature increased, only a little red shift of stop band appeared in the vicinity of T g and the intensity of the maximum reflection peak decreased until the stop bands disappeared. Furthermore, enough heating time at the T g ±2 °C could also lead to the disappearance of stop bands. What’s more, colloidal crystal films with certain connection strength were obtained by simple heating.
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Metadata
Title
Colloidal particles with various glass transition temperatures: preparation, assembly, and the properties of stop bands under heat treatment
Authors
Chunmei Li
Baoliang Zhang
Jiaojun Tan
Xinlong Fan
Yali Liu
Hepeng Zhang
Qiuyu Zhang
Publication date
01-03-2014
Publisher
Springer US
Published in
Journal of Materials Science / Issue 6/2014
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-013-7970-9

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