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Topics in Catalysis
Published in: Topics in Catalysis 7-10/2010

01-06-2010 | Original Paper

Dehydration of Triol Compounds in High-Temperature Liquid Water Under High-Pressure Carbon Dioxide

Authors: Aritomo Yamaguchi, Norihito Hiyoshi, Osamu Sato, Masayuki Shirai

Published in: Topics in Catalysis | Issue 7-10/2010

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Abstract

High-temperature liquid water treatment of triol compounds [1,2,3-propanetriol (glycerol), 1,2,4-butanetriol (1,2,4-BTO), and 1,2,5-pentanetriol (1,2,5-PTO)] was carried out using a batch reactor. Intramolecular dehydration to hydroxyacetone from glycerol, 3-hydroxytetrahydrofuran from 1,2,4-BTO, and both tetrahydrofurfuryl alcohol and 3-hydroxytetrahydropyran from 1,2,5-PTO proceeded in water at 573 K. The dehydration rates were enhanced by the addition of high-pressure carbon dioxide.
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Literature
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Pacific Northwest National Laboratory (PNNL) and National Renewable Energy Laboratory (NREL) (2004) Top value added chemicals from biomass. Volume I: Results of screening for potential candidates from sugars and synthesis gas
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Yamaguchi A, Hiyoshi N, Sato O, Bando KK, Masuda Y, Shirai M (2009) J Chem Eng Data 54:2666CrossRef
Metadata
Title
Dehydration of Triol Compounds in High-Temperature Liquid Water Under High-Pressure Carbon Dioxide
Authors
Aritomo Yamaguchi
Norihito Hiyoshi
Osamu Sato
Masayuki Shirai
Publication date
01-06-2010
Publisher
Springer US
Published in
Topics in Catalysis / Issue 7-10/2010
Print ISSN: 1022-5528
Electronic ISSN: 1572-9028
DOI
https://doi.org/10.1007/s11244-010-9476-x

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