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Lasers in Manufacturing and Materials Processing

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23-01-2019

Effects of Composition and Post Heat Treatment on Shape Memory Characteristics and Mechanical Properties for Laser Direct Deposited Nitinol

Authors: Jeongwoo Lee, Yung C. Shin

Published in: Lasers in Manufacturing and Materials Processing | Issue 1/2019

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Abstract

Nitinol structures were synthesized in a fully dense form using a laser direct deposition method. The pure elemental metal powders of nickel and titanium were used and powder ratios were controlled to arrive at the prescribed final chemical compositions of Nitinol. The transformation temperatures of synthesized Nitinol samples with different chemical composition and post heat treatment conditions were systematically analyzed and compared with those of conventional Nitinol. Compared to Nitinol parts produced by other techniques, the laser engineered net shaping (LENS) created the least amount of secondary phase, indicating the possibility of high corrosion resistance. Two step post processing of solution heat treatment and aging heat treatment was carried out to improve the homogeneity of the microstructure and to investigate its effects on phase transformation temperatures. The resultant phase transformation temperatures could be controlled by the heat treatment parameters. Compression test results showed mechanical properties of synthesized Nitinol samples are largely affected by its post heat treatment history while the effect of initial chemical composition was negligible.

previous article Laser Alloying of Surface of Ti-5.5Al-2Zr-1Mo-1 V Titanium near-α-Alloy Prepared Via Melted by Pulsed Laser Radiation TiC Particles

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Duerig, T., Pelton, A., Stockel, D.: An overview of nitinol medical applications. Mater. Sci. Eng. A. 273-275, 149–160 (1999)CrossRef

Chen, M., Yang, X., Hu, R., Cui, Z., Man, H.: Bioactive NiTi shape memory alloy used as bone bonding implants. Mater. Sci. Eng. C. 24(4), 497–502 (2004)CrossRef

Bernard, S., Balla, V., Davies, N., Bose, S., Bandyopadhyay, A.: Bone cell-materials interactions and Ni ion release of anodized equiatomic NiTi alloy. Acta Biomater. 7(4), 1902–1912 (2011)CrossRef

Michiardi, A., Aparicio, C., Planell, J., Gil, F.: Electrochemical behaviour of oxidized NiTi shape memory alloys for biomedical applications. Surf. Coat. Technol. 201(14), 6484–6488 (2007)CrossRef

Shabalovskaya, S., Anderegg, J., Van Humbeeck, J.: Critical overview of Nitinol surfaces and their modifications for medical applications. Acta Biomater. 4(3), 447–467 (2008)CrossRef

Wu, M.: H.: fabrication of Nitinol materials and components. Mater. Sci. Forum. 394, 285–292 (2002)CrossRef

Bram, M., Bitzer, M., Buchkremer, H., Stover, D.: Reproducibility study of NiTi parts made by metal injection molding. J. Mater. Eng. Perform. 21(12), 2701–2712 (2012)CrossRef

Mentz, J., Bram, M., Buchkremer, H., Stover, D.: Improvement of mechanical properties of powder metallurgical NiTi shape memory alloys. Adv. Eng. Mater. 8(4), 247–252 (2006)CrossRef

Ismail, M., Goodall, R., Davies, H., Todd, I.: Porous NiTi alloy by metal injection moulding/sintering of elemental powders: effect of sintering temperature. Mater. Lett. 70, 142–145 (2012)CrossRef

10.

Bram, M., Ahmad-Khanlou, A., Heckmann, A., Fuchs, B., Buchkremer, H., Stover, D.: Powder metallurgical fabrication processes for NiTi shape memory alloy parts. Mater. Sci. Eng. A. 337(1-2), 254–263 (2002)CrossRef

11.

Bansiddhi, A., Sargeant, T., Stupp, S., Dunand, D.: Porous NiTi for bone implants: a review. Acta Biomater. 4(4), 773–782 (2008)CrossRef

12.

Malukhin, K., Ehmann, K.: Material characterization of NiTi based memory alloys fabricated by the laser direct metal deposition process. J. Manuf. Sci. Eng. 128(3), 691–696 (2006)CrossRef

13.

Halani, P., Shin, Y.: In situ synthesis and characterization of shape memory alloy Nitinol by laser direct deposition. Metal. Mater. Trans. A. 43A, 650–657 (2012)CrossRef

14.

Khademzadeh, S., Parvin, N., Bariani, P.: Production of NiTi alloy by direct metal deposition of mechanically alloyed powder mixtures. Int. J. Precis. Eng. Manuf. 16(11), 2333–2338 (2015)CrossRef

15.

Shishkovsky, I., Yadroitsev, I., Smurov, I.: Direct selective laser melting of nitinol powder. Phys. Procedia. 39, 447–454 (2012)CrossRef

16.

Bernard, S., Balla, V., Bose, S., Bandyopadhyay, A.: Rotating bending fatigue response of laser processed porous NiTi alloy. Mater. Sci. Eng. C. 31(4), 815–820 (2011)CrossRef

17.

Bernard, S., Balla, V., Bose, S., Bandyopadhyay, A.: Compression fatigue behavior of laser processed porous NiTi alloy. J. Mech. Behav. Biomed. 13, 62–68 (2012)CrossRef

18.

Halani, P., Kaya, I., Shin, Y., Karaca, H.: Phase transformation characteristics and mechanical characterization of nitinol synthesized by laser direct deposition. Mater. Sci. Eng. A. 559, 836–843 (2013)CrossRef

19.

Hamilton, R., Palmer, T., Bimber, B.: Spatial characterization of the thermal-induced phase transformation throughout as-deposited additive manufactured NiTi bulk builds. Scr. Mater. 101, 56–59 (2015)CrossRef

20.

Shiva, S., Palani, I., Mishra, S., Paul, C., Kukreja, L.: Investigations on the influence of composition in the development of Ni-Ti shape memory alloy using laser based additive manufacturing. Opt. Laser Technol. 69, 44–51 (2015)CrossRef

21.

Hamilton, R., Bimber, B., Andani, M., Elahinia, M.: Multi-scale shape memory effect recovery in NiTi alloys additive manufactured by selective laser melting and laser directed energy deposition. J. Mater. Process. Technol. 250, 55–64 (2017)CrossRef

22.

Pelton, A., DiCello, J., Miyazaki, S.: Optimisation of processing and properties of medical grade Nitinol wire. Minim. Invasiv. Ther. 9(2), 107–118 (2000)CrossRef

23.

Sun, B., Fu, M.W., Lin, J., Ning, Y.Q.: Effect of low-temperature aging treatment on thermally-and stress-induced phase transformations of nanocrystalline and coarse-grained NiTi wires. Mater. Des. 131, 49–59 (2017)CrossRef

24.

Fan, Q.C., Zhang, Y.H., Wang, Y.Y., Sun, M.Y., Meng, Y.T., Huang, S.K., Wen, Y.H.: Influences of transformation behavior and precipitates on the deformation behavior of Ni-rich NiTi alloys. Mater. Sci. Eng. A. 700, 269–280 (2017)CrossRef

25.

Adharapurapu, R.R., Vecchio, K.S.: Effects of aging and cooling rate on the transformation of nanostructured Ti-50.8 Ni. Mater. Sci. Eng. A. 693, 150–163 (2017)

26.

Saedi, S., Turabi, A., Andani, M., Haberland, C., Karaca, H., Elahinia, M.: The influence of heat treatment on the thermomechanical response of Ni-rich NiTi alloys manufactured by selective laser melting. J. Alloys Compd. 677, 204–210 (2016)CrossRef

27.

Ahadi, A., Sun, Q.: Stress hysteresis and temperature dependence of phase transition stress in nanostructured NiTi-effects of grain size. Appl. Phys. Lett. 103(2), 021902 (2013)CrossRef

28.

Sun, B., Fu, M.W., Lin, J.P., Ning, Y.Q.: Effect of low-temperature aging treatment on thermally-and stress-induced phase transformations of nanocrystalline and coarse-grained NiTi wires. Mater. Des. 131, 49–59 (2017)CrossRef

29.

Adharapurapu, R.R., Vecchio, K.S.: Effects of aging and cooling rate on the transformation of nanostructured Ti-50.8 Ni. J. Alloys Compd. 693, 150–163 (2017)CrossRef

30.

Bertheville, B., Neudenberger, M., Bidaux, J.E.: Powder sintering and shape-memory behaviour of NiTi compacts synthesized from Ni and TiH2. Mater. Sci. Eng. A. 384, 143–150 (2004)

31.

Tang, W., Sundman, B., Sandstrom, R., Qiu, C.: New modelling of the B2 phase and its associated martensitic transformation in the Ti-Ni system. Acta Mater. 47(12), 3457–3468 (1999)CrossRef

32.

Yeung, K., Cheung, K., Lu, W., Chung, C.: Optimization of thermal treatment parameters to alter austenitic phase transition temperature of NiTi alloy for medical implant. Mater. Sci. and Eng. A 383(2), 213–218 (2004)CrossRef

33.

Krone, L., Mentz, J., Stover, D., Epple, M., "NiTi shape memory alloy parts produced by metal injection molding", Proc. International Conference on Shape Memory and Superelastic Technologies, Baden-Baden, 495–500 (2004)

34.

Mercier, O., Melton, K.N.: Theoretical and experimental efficiency of the conversion of heat into mechanical energy using shape-memeory alloys. J. Appl. Phys. 52(2), 1030–1037 (1981)CrossRef

35.

Mercier, O., Melton, K.N.: Kinetics and thermodynamics of the shape-memory effect in martensitic NiTi and (Ni1− x Cu x) Ti alloys. J. Appl. Phys. 50(9), 5747–5756 (1979)CrossRef

36.

Wasilewski, R.J., Butler, S.R., Hanlon, J.E.: On the martensitic transformation in TiNi. Met. Sci. J. 1(1), 104–110 (1967)CrossRef

37.

Mukherjee, K., Sircar, S., Dahotre, N.B.: Thermal effects associated with stress-induced martensitic transformation in a Ti-Ni alloy. Mater. Sci. Eng. 74(1), 75–84 (1985)CrossRef

38.

Chu, C., Chung, J., Chu, P.: Effects of heat treatment on characteristics of porous Ni-rich NiTiSMA prepared by SHS technique. Trans. Nonferr. Metal. Soc. 16(1), 49–53 (2006)MathSciNetCrossRef

39.

Majkic, G., Chennoufi, N., Chen, Y., Salama, K.: Synthesis of NiTi by low electrothermal loss spark plasma sintering. Metal. Mater. Trans. A. 38A, 2523–2530 (2007)CrossRef

40.

Yuan, B., Chung, C., Zhu, M.: Microstructure and martensitic transformation behavior of porous NiTi shape memory alloy prepared by hot isostatic pressing processing. Mater. Sci. Eng. A. 382(1-2), 181–187 (2004)CrossRef

41.

Shishkovsky, I., Tarasova, E., Zhuravel’, L., Petrov, A.: The synthesis of a biocomposite based on nickel titanium and hydroxyapatite under selective laser sintering conditions. Tech. Phys. Lett. 27, 211–213 (2001), 3

42.

Haberland, C., Meier, H., Frenzel, J.: On the properties of Ni-rich NiTi shape memory parts produced by selective laser melting. ASME 2012 Conference on Smart Materials, Adaptive Structures and Intelligent Systems, 97–104, Georgia, USA, Sept. 19–21 (2012)

43.

Chu, C., Chung, C., Lin, P.: DSC study of the effect of aging temperature on the reverse martensitic transformation in porous Ni-rich NiTi shape memory alloy fabricated by combustion synthesis. Mater. Lett. 59(4), 404–407 (2005)CrossRef

44.

Liang, Y., Jiang, S., Zhang, Y., Yu, J.: Microstructure, mechanical property, and phase transformation of quaternary NiTiFeNb and NiTiFeTa shape memory alloys. Metals-Basel 7(8), 309 (2017)

45.

Grossmann, C., Frenzel, J., Sampath, V., Depka, T., Eggeler, G.: Elementary transformation and deformation processes and the cyclic stability of NiTi and NiTiCu shape memory spring actuators. Metal. Mater. Trans. A 40A, 2530–2544 (2009)CrossRef

46.

Rosner, H., Schlossmacher, P., Shelyakov, A., Glezer, A.: The influence of coherent and semi-coherent TiCu precipitates on the martensitic transformation of melt-spun Ti50Ni25Cu25 shape memory ribbons. Mater. Trans. 42, 1758–1762 (2001)CrossRef

Title: Effects of Composition and Post Heat Treatment on Shape Memory Characteristics and Mechanical Properties for Laser Direct Deposited Nitinol
Authors: Jeongwoo Lee
Yung C. Shin
Publication date: 23-01-2019
Publisher: Springer US
Published in: Lasers in Manufacturing and Materials Processing / Issue 1/2019
Print ISSN: 2196-7229
Electronic ISSN: 2196-7237
DOI: https://doi.org/10.1007/s40516-019-0079-5

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