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Metallurgical and Materials Transactions A
Published in: Metallurgical and Materials Transactions A 4/2019

14-01-2019

Evolution and Growth Kinetics of θ Precipitates in Naturally Aged MgLiAlZn Alloy Studied by In Situ Small-Angle X-ray Scattering

Authors: Yung-Chien Huang, Cheng-Si Tsao, Shyi-Kaan Wu

Published in: Metallurgical and Materials Transactions A | Issue 4/2019

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Abstract

The MgLiAlZn (LAZ1110) magnesium alloy was studied by in situ small-angle X-ray scattering (SAXS) to reveal the evolution of MgLi2Al θ precipitates (ppts) in the early aging stage at room temperature (RT). DSC and XRD measurements reveal θ ppts in naturally aged alloy. During 0 to 22 hours of early aging at RT, the growth and coarsening of plate-like θ nano-ppts are quantitatively resolved using SAXS in terms of the temporal evolution of the radius, thickness, and relative volume fraction. In this early aging period, the radius of θ ppts grows gradually from 3.1 to 6.9 nm with a nearly constant thickness of 3.7 nm. The relative volume fraction of θ ppts increases rapidly in the early aging stage and then more slowly in the peak aging stage at ~ 17 hours. The growth behavior of θ ppts after the peak aging stage follows the coarsening kinetics and causes hardness softening. It is supposed that the corresponding increase and decrease in hardness can be attributed to the coherency strengthening and coherency loss of the θ ppts, respectively.
previous article Rationalizing the Grain Size Dependence of Strength and Strain-Rate Sensitivity of Nanocrystalline fcc Metals
next article Quench Sensitivity in a Dispersoid-Containing Al-Mg-Si Alloy

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Literature
1.
2.
3.
3. H. Haferkamp, R. Boehm, U. Holzkamp, C. Jaschik, V. Kaese, M. Niemeyer: Mater. Trans., 2001, vol. 42, pp. 1160-1166.CrossRef
4.
5.
5. M. Kawasaki, K. Kubota, K.I. Higashi, T.G. Langdon: Mat. Sci. Eng. A, 2006, vol. 429, pp. 334-340.CrossRef
6.
6. P. Metenier, G. Gonzalezdoncel, O.A. Ruano, J. Wolfenstine, O.D. Sherby: Mat. Sci. Eng. A, 1990, vol. 125, pp. 195-202.CrossRef
7.
ASM Handbook: Alloy Phase Diagrams, ASM International, Ohio, 1992, vol. 3, pp. 2–276.
8.
8. F.H. Herbstein, B.L. Averbach: Acta Metall. Mater., 1956, vol. 4, pp. 407-413.CrossRef
9.
9. C.T. Chiang, S. Lee, C.L. Chu: Trans. Nonferrous Met. Soc. China, 2010, vol. 20, pp. 1374-1379.CrossRef
10.
10. Z.X. Kang, K. Lin, J.Y. Zhang: Mater. Sci. Tech., 2016, vol. 32, pp. 498-506.CrossRef
11.
11. X.R. Meng, R.Z. Wu, M.L. Zhang, L.B. Wu, C.L. Cui: J. Alloys Compd., 2009, vol. 486, pp. 722-725.CrossRef
12.
G. Sheng, M. Staiger, M. Kral: Magnesium Technology, TMS, 2003, pp. 77–79.
13.
13. G.S. Song, M. Staiger, M. Kral: Mat. Sci. Eng. A, 2004, vol. 371, pp. 371-376.CrossRef
14.
14. H.Y. Wu, Z.W. Gao, J.Y. Lin, C.H. Chiu: J. Alloys Compd., 2009, vol. 474, pp. 158-163.CrossRef
15.
15. L.B. Wu, C.L. Cui, R.Z. Wu, J.Q. Li, H.B. Zhan, M.L. Zhang: Mat. Sci. Eng. A, 2011, vol. 528, pp. 2174-2179.CrossRef
16.
17.
18.
18. C.Q. Li, D.K. Xu, B.J. Wang, L.Y. Sheng, Y.X. Qiao, E.H. Han: Sci. Rep., 2017, vol. 7, 40078.CrossRef
19.
19. Z.K. Qu, R.Z. Wu, H.B. Zhan, M.L. Zhang: J. Alloys Compd., 2012, vol. 536, pp. 145-149.CrossRef
20.
20. H.Y. Wu, J.Y. Lin, Z.W. Gao, H.W. Chen: Mat. Sci. Eng. A, 2009, vol. 523, pp. 7-12.CrossRef
21.
21. C.C. Hsu, J.Y. Wang, S. Lee: Mater. Trans., 2008, vol. 49, pp. 2728-2731.CrossRef
22.
22. J.C. McDonald: ASM Trans., 1968, vol. 61, pp. 505.
23.
23. C.J. Ma, D. Zhang, J.N. Qin: Trans. Nonferrous Met. Soc. China, 1999, vol. 9, pp. 772-777.
24.
24. Z. Drozd, Z. Trojanova, S. Kudela: J. Alloys Compd., 2004, vol. 378, pp. 192-195.CrossRef
25.
25. P. Crawford, R. Barrosa, J. Mendez, J. Foyos, O.S. EsSaid: J. Mater. Process. Tech., 1996, vol. 56, pp. 108-118.CrossRef
26.
26.A. Yamamoto, T. Ashida, Y. Kouta, K.B. Kim, S. Fukumoto, H. Tsubakino: Mater. Trans., 2003, vol. 44, pp. 619-624.CrossRef
27.
27. X.Y. Guo, R.Z. Wu, J.H. Zhang, B. Liu, M.L. Zhang: Mater. Design, 2014, vol. 53, pp. 528-533.CrossRef
28.
28. H.Y. Lin, R.Z. Wu, P.F. Fei, Z. Leng, X.Y. Guo, J.H. Zhang, B. Liu, M.L. Zhang: Kovove Mater., 2014, vol. 52, pp. 47-55.
29.
29. R.Z. Wu, X.Y. Guo, D.Y. Li: J. Alloys Compd., 2014, vol. 616, pp. 408-412.CrossRef
30.
31.
32.
32. T. Liu, S.D. Wu, S.X. Li, P.J. Li: Mat. Sci. Eng. A, 2007, vol. 460, pp. 499-503.CrossRef
33.
33. Z.J. Li, X.Y. Jing, Y. Yuan, M.L. Zhang: Corros. Sci., 2012, vol. 63, pp. 358-366.CrossRef
34.
34. L.L. Shi, Y.J. Xu, K. Li, Z.P. Yao, S.Q. Wu: Curr. Appl. Phys., 2010, vol. 10, pp. 719-723.CrossRef
35.
35. H. Zhang, G.C. Yao, S.L. Wang, Y.H. Liu, H.J. Luo: Surf. Coat. Tech., 2008, vol. 202, pp. 1825-1830.CrossRef
36.
36. S.K. Wu, Y.H. Li, K.T. Chien, C. Chien, C.S. Yang: J. Alloys Compd., 2013, vol. 563, pp. 234-241.CrossRef
37.
37. C. Antion, P. Donnadieu, F. Perrard, A. Deschamps, C. Tassin, A. Pisch: Acta Mater., 2003, vol. 51, pp. 5335-5348.CrossRef
38.
38. R. Ferragut, F. Moia, F. Fiori, D. Lussana, G. Riontino: J. Alloys Compd., 2010, vol. 495, pp. 408-411.CrossRef
39.
39. G. Barucca, R. Ferragut, F. Fiori, D. Lussana, P. Mengucci, F. Moia, G. Riontino: Acta Mater., 2011, vol. 59, pp. 4151-4158.CrossRef
40.
40. W. Liu, W.L. Johnson, S. Schneider, U. Geyer, P. Thiyagarajan: Phys. Rev. B, 1999, vol. 59, pp. 11755-11759.CrossRef
41.
41. B. Rashkova, W. Prantl, R. Goergl, J. Keckes, S. Cohen, M. Bamberger, G. Dehm: Mat. Sci. Eng. A, 2008, vol. 494, pp. 158-165.CrossRef
42.
42. A. Deschamps, M. Garcia, J. Chevy, B. Davo, F. De Geuser: Acta Mater., 2017, vol. 122, pp. 32-46.CrossRef
43.
43. A. Deschamps, L. Lae, P. Guyot: Acta Mater., 2007, vol. 55, pp. 2775-2783.CrossRef
44.
44. E. Gumbmann, F. De Geuser, C. Sigli, A. Deschamps: Acta Mater., 2017, vol. 133, pp. 172-185.CrossRef
45.
45. F. De Geuser, F. Bley, A. Deschamps: J. Appl. Crystallogr., 2012, vol. 45, pp. 1208-1218.CrossRef
46.
46. P. Fratzl, F. Langmayr, O. Paris: J. Appl. Crystallogr., 1993, vol. 26, pp. 820-826.CrossRef
47.
47. A. Deschamps, F. De Geuser: Metall. Mater. Trans. A, 2013, vol. 44A, pp. 77-86.CrossRef
48.
O. Glatter, O. Kratky: Small Angle X-ray Scattering, Academic Press: New York, 1982, p. 222.
49.
49. C. Genevois, A. Deschamps, A. Denquin, B. Doisneau-cottignies: Acta Mater., 2005, vol. 53, pp. 2447-2458.CrossRef
50.
51.
51. C.S. Tsao, E.W. Huang, M.H. Wen, T.Y. Kuo, S.L. Jeng, U.S. Jeng, Y.S. Sun: J. Alloys Compd., 2013, vol. 579, pp. 138-146.CrossRef
52.
52. E.W. Huang, C.S. Tsao, M.H. Wen, T.Y. Kuo, S.Y. Tu, B.W. Wu, C.J. Su, U.S. Jeng: J. Mater. Res., 2014, vol. 29, pp. 874-879.CrossRef
53.
54.
55.
55. S. Esmaeili, D.J. Lloyd, W.J. Poole: Acta Mater., 2003, vol. 51, pp. 3467-3481.CrossRef
56.
56. W.A. Johnson, R.F. Mehl: T. Am. I. Min. Met. Eng., 1939, vol. 135, pp. 416-442.
57.
57. A. Kolmogoroff: Izv. Akad. Nauk SSSR Ser. Mat., 1937, vol. 1, pp. 355-359.
58.
58. R.E. Smallman, R.J. Bishop: Modern Physical Metallurgy and Materials Engineering: Chapter 8 - Strengthening and toughening, Butterworth-Heinemann, Oxford, 1999, pp. 259-296.CrossRef
59.
M.N. Shetty: Dislocations and mechanical behaviour of materials: 4.12-Precipitation Hardening, PHI Learning Private Limited, Delhi, Indian, 2013, pp. 419–31.
60.
T.H. Courtney: Mechanical behavior of materials: 5.6 Particle Hardening, McGraw Hill, New York, USA, 2000, pp. 196–209.
61.
61. H.H. J. Roesler, M. Baeker: Mechanical Behaviour of Engineering Materials, Springer-Verlag, Berlin/Heidelberg, Germany, 2007, pp. 165-225.CrossRef
62.
63.
63. A. Vattre, B. Devincre, A. Roos: Intermetallics, 2009, vol. 17, pp. 988-994.CrossRef
64.
64. C.R. Barrett, W.D. Nix, A.S. Tetelman: The Principles of Engineering Materials, Prentice-Hall, New Jersey, USA, 1973, p. 263.
65.
65. J.W. Martin: Precipitation Hardening: 2 - The strength of aged alloy, Butterworth-Heinemann, Oxford, 1998, pp. 79-125.CrossRef
66.
67.
H.S. M.F. Ashby, D. Cebon: Materials: Engineering, Science, Processing and Design: 6. Beyond elasticity: plasticity, yielding and ductility, Butterworth-Heinemann, Oxford, 2018, p. 129.
68.
68. M. Yamasaki, T. Anan, S. Yoshimoto, Y. Kawamura: Scripta Mater., 2005, vol. 53, pp. 799-803.CrossRef
Metadata
Title
Evolution and Growth Kinetics of θ Precipitates in Naturally Aged MgLiAlZn Alloy Studied by In Situ Small-Angle X-ray Scattering
Authors
Yung-Chien Huang
Cheng-Si Tsao
Shyi-Kaan Wu
Publication date
14-01-2019
Publisher
Springer US
Published in
Metallurgical and Materials Transactions A / Issue 4/2019
Print ISSN: 1073-5623
Electronic ISSN: 1543-1940
DOI
https://doi.org/10.1007/s11661-019-05119-x

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