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Journal of Materials Engineering and Performance

Published in:

01-07-2013

Grain Size Control of the Magnetic Nanoparticles by Solid State Route Modification

Authors: A. C. H. Barreto, V. R. Santiago, R. M. Freire, S. E. Mazzetto, J. M. Sasaki, I. F. Vasconcelos, J. C. Denardin, Giuseppe Mele, Luigi Carbone, P. B. A. Fechine

Published in: Journal of Materials Engineering and Performance | Issue 7/2013

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Abstract

The CoFe₂O₄ and NiFe₂O₄ nanoparticles were synthesized exploiting a co-precipitation method and afterward calcinated at 400 °C through two different experimental apparatus: a conventional muffle and rotatory oven. X-ray diffraction (XRD) analysis revealed that nanocrystalline ferrites grew with a face center cubic structure (fcc) and Fd3m symmetry space group. XRD, transmission electron microscopy, and magnetic measurements confirmed the compositional homogeneity and the narrow size particle distribution (6-8 nm) of the sample thermally treated in a rotary oven, in all likelihood due to the sample’s constant turning movement. The size of the magnetic particles is extremely important and influences the choice of a potential technological application. For this reason, our study emerges as a new and simple innovating procedure to control the size of magnetic nanoparticles.

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Title: Grain Size Control of the Magnetic Nanoparticles by Solid State Route Modification
Authors: A. C. H. Barreto
V. R. Santiago
R. M. Freire
S. E. Mazzetto
J. M. Sasaki
I. F. Vasconcelos
J. C. Denardin
Giuseppe Mele
Luigi Carbone
P. B. A. Fechine
Publication date: 01-07-2013
Publisher: Springer US
Published in: Journal of Materials Engineering and Performance / Issue 7/2013
Print ISSN: 1059-9495
Electronic ISSN: 1544-1024
DOI: https://doi.org/10.1007/s11665-013-0480-8

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