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Polymer Bulletin
Published in: Polymer Bulletin 4/2024

27-05-2023 | ORIGINAL PAPER

Interfacial synthesis, characterization and thermal studies of PANI/MAl2O4 (M = Mg, Zn) nanocomposites

Authors: Arunkumar Lagashetty, M. Ameena, P. Anjalidevi, K. S. Darshan, K. Reshma, Shreeharsha, B. Manjunatha, Sangshetty Kalyani, V. Veena, Sangappa K. Ganiger

Published in: Polymer Bulletin | Issue 4/2024

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Abstract

Science and technology of nanoscale materials is enriched by developing new synthetic technology and its applications in various fields. Recent development reviews the combustion method which is an efficient and simple method for the preparation of different materials and their composites. Metal oxide-based polymer nanocomposites have gained much importance due to their special applications. In addition, interfacial polymerization method has gained its importance in the synthesis of composites by eco-friendly system. Nanosized metal aluminates such as MgAl2O4 and ZnAl2O4 were prepared by a combustion route using poly(vinyl alcohol) as a fuel. Interfacial polymerization method was used for the preparation of polyaniline–MAl2O4 (PANI/MgAl2O4, PANI/ZnAl2O4) nanocomposites. These composites were well characterized for their structures by employing X-ray diffraction tool and morphology by scanning electron micrograph tool, respectively. In-depth morphology of the sample was well studied by transmission electron micrograph tool. The bonding nature of the sample was studied by Fourier transform infrared (FT-IR) study, and the presence of metals in the composites was confirmed by EDX pattern. Electrical and thermal studies of the PANI/MAl2O4 composites were conducted to understand their electrical and thermal behaviors, respectively. UV–visible and DLS studies of the prepared nanocomposite were also conducted to understand the absorbance and particle distribution, respectively.
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Metadata
Title
Interfacial synthesis, characterization and thermal studies of PANI/MAl2O4 (M = Mg, Zn) nanocomposites
Authors
Arunkumar Lagashetty
M. Ameena
P. Anjalidevi
K. S. Darshan
K. Reshma
Shreeharsha
B. Manjunatha
Sangshetty Kalyani
V. Veena
Sangappa K. Ganiger
Publication date
27-05-2023
Publisher
Springer Berlin Heidelberg
Published in
Polymer Bulletin / Issue 4/2024
Print ISSN: 0170-0839
Electronic ISSN: 1436-2449
DOI
https://doi.org/10.1007/s00289-023-04834-1

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