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Topics in Catalysis
Published in: Topics in Catalysis 9-10/2013

01-06-2013 | Original Paper

Isomerization of α-Pinene Oxide Over Iron-Modified Zeolites

Authors: Narendra Kumar, Päivi Mäki-Arvela, Sara Faten Diáz, Atte Aho, Yulia Demidova, Johan Linden, Anna Shepidchenko, Mikko Tenhu, Jarno Salonen, Pekka Laukkanen, Alexander Lashkul, Johnny Dahl, Iliya Sinev, Anne-Riikka Leino, Krisztian Kordas, Tapio Salmi, Dmitry Yu. Murzin

Published in: Topics in Catalysis | Issue 9-10/2013

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Abstract

Fe-modified mordenite, ferrierite, Y, ZSM-5, ZSM-12 and beta zeolite catalysts were prepared by solid state ion-exchange and conventional liquid phase ion-exchange methods from aqueous solutions. Sn- modified H-beta-300 zeolite catalyst was prepared by the later method. The characterization of proton form, Fe and Sn modified zeolites was carried out using X-ray powder diffraction, scanning electron microscopy, Mössbauer spectroscopy with magnetic measurements, transmission electron microscopy, nitrogen adsorption, X-ray absorption spectroscopy, X-ray photoelectron spectroscopy, inductively coupled plasma spectroscopy, thermo-gravimetric analysis and FTIR spectroscopy using pyridine as a probe molecule. Isomerization of α-pinene oxide over the Fe and Sn modified zeolite catalysts was carried out in the liquid phase using a batch-wise glass reactor. Formation of campholenic aldehyde and fencholenic aldehyde were observed to be influenced by the structure, acidity of zeolite and contents of Fe and Sn, reaction temperature and the catalysts pretreatment.
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Metadata
Title
Isomerization of α-Pinene Oxide Over Iron-Modified Zeolites
Authors
Narendra Kumar
Päivi Mäki-Arvela
Sara Faten Diáz
Atte Aho
Yulia Demidova
Johan Linden
Anna Shepidchenko
Mikko Tenhu
Jarno Salonen
Pekka Laukkanen
Alexander Lashkul
Johnny Dahl
Iliya Sinev
Anne-Riikka Leino
Krisztian Kordas
Tapio Salmi
Dmitry Yu. Murzin
Publication date
01-06-2013
Publisher
Springer US
Published in
Topics in Catalysis / Issue 9-10/2013
Print ISSN: 1022-5528
Electronic ISSN: 1572-9028
DOI
https://doi.org/10.1007/s11244-013-0029-y

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