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Journal of Sol-Gel Science and Technology

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01-02-2015 | Brief Communication

Nd₂O₃: novel synthesis and characterization

Authors: R. Yuvakkumar, S. I. Hong

Published in: Journal of Sol-Gel Science and Technology | Issue 2/2015

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Abstract

The present work was focused on producing sustainable Nd₂O₃ nanoparticles for inhibiting human breast cancer cells. Novel synthesis route was described. Raman, PL, XRD, FTIR, XPS and TEM characterization was explored. Observed Raman F_g and A_g + E_g combination modes confirmed Nd₂O₃. PL emission bands around ∼352–392 nm (UV), ∼429–472 nm (blue), ∼580 nm (green) and ∼650 nm (red) further confirmed Nd₂O₃. Highest incubation period clearly exhibits (100) oriented strong XRD characteristic Nd₂O₃ peak. 413 and 630 cm⁻¹ peaks represent IR characteristic metal–oxygen (Nd–O) vibrations. Nd_3d peak shifted to higher binding energy upon increasing incubation period substantiate the presence of bigger particles due to rich Nd structure. 7 days incubation revealed agglomerated Nd₂O₃ particles (200 nm). 1 day incubated 500 (µg/ml) Nd₂O₃ dosage could be used as an effective biocompatibility material.

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Title: Nd2O3: novel synthesis and characterization
Authors: R. Yuvakkumar
S. I. Hong
Publication date: 01-02-2015
Publisher: Springer US
Published in: Journal of Sol-Gel Science and Technology / Issue 2/2015
Print ISSN: 0928-0707
Electronic ISSN: 1573-4846
DOI: https://doi.org/10.1007/s10971-015-3629-0

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