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Journal of Materials Science: Materials in Electronics

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11-04-2021

One-step synthesis of coated (Gd³⁺, Er³⁺) co-doped Co–Ni ferrite nanoparticles; structural and magnetic properties

Authors: A. Hssaini, M. Belaiche, M. Elansary

Published in: Journal of Materials Science: Materials in Electronics | Issue 9/2021

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Abstract

Coated Ni_0.5Co_0.5Fe_(2−x–y)Gd_xEr_yO₄ (x = 0.3, y = 0.1) nanoparticles were synthesized by the co-precipitation method for the first time. The obtained nanoparticles were characterized by X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), thermogravimetric analysis (TGA), and Magnetic Property Measurement System (MPMS). The analysis of XDR confirms the formation of single-phase spinel with an average crystallinity size value of 18 nm. FTIR showed the formation of octahedral and tetrahedral sites and the formation of bonds between the nanoparticles and oleic acid. TEM showed the formation of quasi-spherical nanoparticles. TGA showed that oleic acid is adsorbed at the surface of the nanoparticles. The analysis of magnetic properties showed a weak ferrimagnetic behavior at 300 K and a hard ferrimagnetic behavior at 80 K and 5 K with a blocking temperature value higher than that of the ambient temperature.

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Title: One-step synthesis of coated (Gd3+, Er3+) co-doped Co–Ni ferrite nanoparticles; structural and magnetic properties
Authors: A. Hssaini
M. Belaiche
M. Elansary
Publication date: 11-04-2021
Publisher: Springer US
Published in: Journal of Materials Science: Materials in Electronics / Issue 9/2021
Print ISSN: 0957-4522
Electronic ISSN: 1573-482X
DOI: https://doi.org/10.1007/s10854-021-05823-8

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