Skip to main content
Top
Published in: Metallography, Microstructure, and Analysis 5/2019

25-09-2019 | Technical Article

Optimization of Microstructure and Mechanical Properties of Hipped Inconel 718 by Various Heat Treatment Processes

Authors: Nader El-Bagoury, M. M. Hessien, Mohammed Alsawat, M. H. H. Mahmoud, Abdullah K. Alanazi, Naif Abdulrahman Alshanbari

Published in: Metallography, Microstructure, and Analysis | Issue 5/2019

Log in

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

The influence of heat treatment processes on hardening and harmful phases in microstructure and mechanical properties of hipped Inconel 718 (IN718) alloy was investigated. In comparison with conventional solid solution treatment, modified solid solution one entirely eradicates δ phase from the microstructure of hipped IN718 alloy. However, a thin film of δ phase precipitates at the grain boundaries of γ matrix. Aging at 750 °C for 4 h, another morphology of needle-like δ phase appeared as small colonies in the microstructure of IN718 alloy. Prolonging the aging duration time to 50 h, these colonies enlarge in size and spread in the whole matrix. X-ray diffraction and transmission electron microscope observations were used to identify different phases such as γ, γ′, γ″, and δ in the microstructure of IN718. Hardness property was measured representing the mechanical properties of investigated heat-treated IN718 alloy. Conventional solutionized specimens have higher rate in hardness increasing with aging time compared to modified solutionized ones. The latter specimens need an incubation period of about 24 h to ascent suddenly achieving the same hardness level of the other corresponding specimens. These heat treatment conditions are considered as the best compromise to achieve the optimum mechanical properties.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literature
1.
go back to reference M. Donachie, S. Donachie Jr., Superalloys: A Technical Guide, 2nd edn. (ASM International, USA, 2002) M. Donachie, S. Donachie Jr., Superalloys: A Technical Guide, 2nd edn. (ASM International, USA, 2002)
2.
go back to reference S. Venukumar, P. Sarkar, J. Sai Sashank, P. Sampath, K. Saikiran, Microstructural and mechanical properties of inconel 718 TIG weldments. Mater. Today Proc. 5, 8480–8485 (2018)CrossRef S. Venukumar, P. Sarkar, J. Sai Sashank, P. Sampath, K. Saikiran, Microstructural and mechanical properties of inconel 718 TIG weldments. Mater. Today Proc. 5, 8480–8485 (2018)CrossRef
3.
go back to reference V.I. Petkov, Alloy 718 manufactured by AM selective laser melting: evaluation of microstructure and weldability, PhD Thesis (2018) V.I. Petkov, Alloy 718 manufactured by AM selective laser melting: evaluation of microstructure and weldability, PhD Thesis (2018)
5.
go back to reference D.F. Paulonis, J.M. Oblak, D.S. Duvall, Precipitation in nickel-base alloy 718. Trans. ASM 62, 611–622 (1969) D.F. Paulonis, J.M. Oblak, D.S. Duvall, Precipitation in nickel-base alloy 718. Trans. ASM 62, 611–622 (1969)
7.
go back to reference M. Jambor, O. Bokůvka, F. Nový, L. Trško, J. Belan, Phase transformations in nickel base superalloy Inconel718 during cyclic loading at high temperatures. Prod. Eng. Arch. 15, 15–18 (2017)CrossRef M. Jambor, O. Bokůvka, F. Nový, L. Trško, J. Belan, Phase transformations in nickel base superalloy Inconel718 during cyclic loading at high temperatures. Prod. Eng. Arch. 15, 15–18 (2017)CrossRef
8.
go back to reference P.J.P. Kañetas, L.A.R. Osorio, M.P.G. Mata, M.D.L. Garza, V.P. López, Influence of delta phase in the microstructure of the Inconel 718 subjected to “delta-processing” heat treatment and hot deformed. Procedia Mater. Sci. 8, 1160–1165 (2015)CrossRef P.J.P. Kañetas, L.A.R. Osorio, M.P.G. Mata, M.D.L. Garza, V.P. López, Influence of delta phase in the microstructure of the Inconel 718 subjected to “delta-processing” heat treatment and hot deformed. Procedia Mater. Sci. 8, 1160–1165 (2015)CrossRef
10.
go back to reference S. Azdian, L.Y. Wei, F. Nicklasson, R. Warren, Precipitations in spray-formed IN 718, in Superalloys 718, 625 and Various Derivatives, ed. by E.A. Loria (Minerals, Metals, & Materials Society, Warrendale, PA, 2001), p. 617CrossRef S. Azdian, L.Y. Wei, F. Nicklasson, R. Warren, Precipitations in spray-formed IN 718, in Superalloys 718, 625 and Various Derivatives, ed. by E.A. Loria (Minerals, Metals, & Materials Society, Warrendale, PA, 2001), p. 617CrossRef
11.
go back to reference D. Cai, W. Zhang, P. Nie, W. Liu, M. Yao, Dissolution kinetics of δ phase and its influence on the notch sensitivity of Inconel 718. Mater. Charact. 58, 220–225 (2007)CrossRef D. Cai, W. Zhang, P. Nie, W. Liu, M. Yao, Dissolution kinetics of δ phase and its influence on the notch sensitivity of Inconel 718. Mater. Charact. 58, 220–225 (2007)CrossRef
12.
go back to reference S.C. Lee, S.H. Chang, T.P. Tang, H.H. Ho, J.K. Chen, Influence of γ″ and δ precipitations on the microstructural properties of 718 alloy though HIP, solid-solution, and different aging heat treatments. Mater. Trans. 47, 2877–2881 (2006)CrossRef S.C. Lee, S.H. Chang, T.P. Tang, H.H. Ho, J.K. Chen, Influence of γ″ and δ precipitations on the microstructural properties of 718 alloy though HIP, solid-solution, and different aging heat treatments. Mater. Trans. 47, 2877–2881 (2006)CrossRef
13.
go back to reference S.H. Chang, In situ TEM observation of γ′, γ″ and δ precipitations on Inconel 718 superalloy though HIP treatment. J. Alloys Compd. 486, 716–721 (2009)CrossRef S.H. Chang, In situ TEM observation of γ′, γ″ and δ precipitations on Inconel 718 superalloy though HIP treatment. J. Alloys Compd. 486, 716–721 (2009)CrossRef
14.
go back to reference S.H. Chang, Optimization of pressure and soaking time of HIP treatment on 713LC cast superalloy. Mater. Trans. 50, 909–916 (2009)CrossRef S.H. Chang, Optimization of pressure and soaking time of HIP treatment on 713LC cast superalloy. Mater. Trans. 50, 909–916 (2009)CrossRef
15.
go back to reference S.H. Chang, S.C. Lee, K.T. Huang, Effects of γ′ precipitation on the structure and properties of 713LC superalloy via HIP treatment. Mater. Trans. 51, 1683–1688 (2010)CrossRef S.H. Chang, S.C. Lee, K.T. Huang, Effects of γ′ precipitation on the structure and properties of 713LC superalloy via HIP treatment. Mater. Trans. 51, 1683–1688 (2010)CrossRef
17.
go back to reference S.J. Hong, W.P. Chen, T.W. Wang, A diffraction study of the γ′ phase in Inconel 718 superalloy. Metall. Mater. Trans. A 32, 1887–1901 (2001)CrossRef S.J. Hong, W.P. Chen, T.W. Wang, A diffraction study of the γ′ phase in Inconel 718 superalloy. Metall. Mater. Trans. A 32, 1887–1901 (2001)CrossRef
18.
go back to reference N. Anbarasan, B.K. Gupta, S. Prakash, P. Muthukumar, R. Oyyaravelu, R.J.F. Kumar, S. Jerome, Effect of heat treatment on the microstructure and mechanical properties of Inconel 718. Mater. Today Proc. 5, 7716–7724 (2018)CrossRef N. Anbarasan, B.K. Gupta, S. Prakash, P. Muthukumar, R. Oyyaravelu, R.J.F. Kumar, S. Jerome, Effect of heat treatment on the microstructure and mechanical properties of Inconel 718. Mater. Today Proc. 5, 7716–7724 (2018)CrossRef
20.
go back to reference M. Sundararaman, P. Mukhopadhyay, S. Banerjee, Precipitation and room temperature deformation behavior of Inconel 718. Superalloys 718, 625, 706 and various derivatives, in Proceedings of the International Symposium on Superalloys 718, 625, 706 and Various Derivatives ed by E. A. Loria, held June 26–29, 1994 M. Sundararaman, P. Mukhopadhyay, S. Banerjee, Precipitation and room temperature deformation behavior of Inconel 718. Superalloys 718, 625, 706 and various derivatives, in Proceedings of the International Symposium on Superalloys 718, 625, 706 and Various Derivatives ed by E. A. Loria, held June 26–29, 1994
22.
go back to reference H.Y. Zhang, S.H. Zhang, M. Cheng, Z.X. Li, Deformation characteristics of δ phase in the delta-processed Inconel 718 alloy. Mater. Charact. 61, 49–54 (2010)CrossRef H.Y. Zhang, S.H. Zhang, M. Cheng, Z.X. Li, Deformation characteristics of δ phase in the delta-processed Inconel 718 alloy. Mater. Charact. 61, 49–54 (2010)CrossRef
23.
go back to reference R.G. Thompson, J. Dobbs, D. Mayo, The effect of heat treatment on microfissuring alloy 718. Weld. J. 65, 299–304 (1986) R.G. Thompson, J. Dobbs, D. Mayo, The effect of heat treatment on microfissuring alloy 718. Weld. J. 65, 299–304 (1986)
24.
go back to reference W.C. Liu, F.R. Xiao, M. Yao, Z.L. Chen, Z.O. Jiang, S.G. Wang, Relationship between the lattice constant of γ phase and the content of δ, γ′ and γ″ phases in Inconel 718. Scr. Mater. 37, 59–64 (1997)CrossRef W.C. Liu, F.R. Xiao, M. Yao, Z.L. Chen, Z.O. Jiang, S.G. Wang, Relationship between the lattice constant of γ phase and the content of δ, γ′ and γ″ phases in Inconel 718. Scr. Mater. 37, 59–64 (1997)CrossRef
25.
go back to reference S. Azadian, L.Y. Wei, R. Warren, Delta phase precipitation in Inconel 718. Mater. Charact. 53, 7–16 (2004)CrossRef S. Azadian, L.Y. Wei, R. Warren, Delta phase precipitation in Inconel 718. Mater. Charact. 53, 7–16 (2004)CrossRef
27.
go back to reference D.G. He, Y.C. Lin, L.H. Wang, Q. Wu, Z.H. Zu, H. Cheng, Influences of pre-precipitated δ phase on microstructures and hot compressive deformation features of a nickel-based superalloy. Vacuum 161, 242–250 (2019)CrossRef D.G. He, Y.C. Lin, L.H. Wang, Q. Wu, Z.H. Zu, H. Cheng, Influences of pre-precipitated δ phase on microstructures and hot compressive deformation features of a nickel-based superalloy. Vacuum 161, 242–250 (2019)CrossRef
28.
go back to reference D.G. He, Y.C. Lin, L.H. Wang, Microstructural variations and kinetic behaviors during metadynamic recrystallization in a nickel base superalloy with pre-precipitated δ phase. Mater. Des. 165, 107584 (2019)CrossRef D.G. He, Y.C. Lin, L.H. Wang, Microstructural variations and kinetic behaviors during metadynamic recrystallization in a nickel base superalloy with pre-precipitated δ phase. Mater. Des. 165, 107584 (2019)CrossRef
30.
go back to reference R.M. Nunes, D. Pereira, T. Clarke, T.K. Hirsch, Delta phase characterization in Inconel 718 alloys through X-ray diffraction. ISIJ Int. 55, 2450–2454 (2015)CrossRef R.M. Nunes, D. Pereira, T. Clarke, T.K. Hirsch, Delta phase characterization in Inconel 718 alloys through X-ray diffraction. ISIJ Int. 55, 2450–2454 (2015)CrossRef
31.
go back to reference V. Beaubois, J. Huez, S. Coste, O. Brucelle, J. Lacaze, Short term precipitation kinetics of delta phase in strain free Inconel 718 alloy. Mater. Sci. Technol. 20, 1019–1026 (2004)CrossRef V. Beaubois, J. Huez, S. Coste, O. Brucelle, J. Lacaze, Short term precipitation kinetics of delta phase in strain free Inconel 718 alloy. Mater. Sci. Technol. 20, 1019–1026 (2004)CrossRef
32.
go back to reference L. Wenchang, X. Furen, Y. Mei, C. Zonglin, W. Shaogang, L. Weihong, Quantitative phase analysis of Inconel 718 by X-ray diffraction. J. Mater. Sci. Lett. 16, 769–771 (1997)CrossRef L. Wenchang, X. Furen, Y. Mei, C. Zonglin, W. Shaogang, L. Weihong, Quantitative phase analysis of Inconel 718 by X-ray diffraction. J. Mater. Sci. Lett. 16, 769–771 (1997)CrossRef
33.
go back to reference J. Belan, L. Kucharikova, E. Tillova, A. Vasko, The influence of applied heat treatment on IN718 fatigue life at three point flexural bending. Metalurgija 56, 167–170 (2017) J. Belan, L. Kucharikova, E. Tillova, A. Vasko, The influence of applied heat treatment on IN718 fatigue life at three point flexural bending. Metalurgija 56, 167–170 (2017)
34.
go back to reference S. Fu, J. Dong, M. Zhang, N. Wang, X. Xie, in 7th International Symposium on Superalloy 718 and Derivatives, ed. by E.A. Ott, J.R. Groh, A. Banik, I. Dempster, T.P. Gabb, R. Helmink, X. Liu, A. Wusatowska-Sanek (TMS (The Minerals, Metals & Materials Society), Warrendale, 2010) S. Fu, J. Dong, M. Zhang, N. Wang, X. Xie, in 7th International Symposium on Superalloy 718 and Derivatives, ed. by E.A. Ott, J.R. Groh, A. Banik, I. Dempster, T.P. Gabb, R. Helmink, X. Liu, A. Wusatowska-Sanek (TMS (The Minerals, Metals & Materials Society), Warrendale, 2010)
35.
go back to reference W.M. Tuchoa, P. Cuvilliera, A.S. Kvernelandb, V. Hansen, Microstructure and Hardness studies of Inconel 718 manufactured by selective laser melting before and after solution heat treatment. Mater. Sci. Eng., A 689, 220–232 (2017)CrossRef W.M. Tuchoa, P. Cuvilliera, A.S. Kvernelandb, V. Hansen, Microstructure and Hardness studies of Inconel 718 manufactured by selective laser melting before and after solution heat treatment. Mater. Sci. Eng., A 689, 220–232 (2017)CrossRef
36.
go back to reference O. Lu, HAZ Microstructural evolution in alloy 718 after multiple repair and PWHT cycles, PhD thesis, Ohio State University, Ohio, United States (1999) O. Lu, HAZ Microstructural evolution in alloy 718 after multiple repair and PWHT cycles, PhD thesis, Ohio State University, Ohio, United States (1999)
37.
go back to reference Y.C. Lin, H. Yang, L. Li, Effects of solutionizing cooling processing on γ″ (Ni3Nb) phase and work hardening characteristics of a Ni-Fe-Cr base superalloy. Vacuum 144, 86–93 (2017)CrossRef Y.C. Lin, H. Yang, L. Li, Effects of solutionizing cooling processing on γ″ (Ni3Nb) phase and work hardening characteristics of a Ni-Fe-Cr base superalloy. Vacuum 144, 86–93 (2017)CrossRef
38.
go back to reference D.G. Hea, Y.C. Lina, Y. Tanga, L. Lia, J. Chend, M.S. Chenb, X.-M. Chen, Influence of solution cooling on microstructures, mechanical properties and hot corrosion resistance of a nickel-base superalloy. Mater. Sci. Eng., A 746, 372–383 (2019)CrossRef D.G. Hea, Y.C. Lina, Y. Tanga, L. Lia, J. Chend, M.S. Chenb, X.-M. Chen, Influence of solution cooling on microstructures, mechanical properties and hot corrosion resistance of a nickel-base superalloy. Mater. Sci. Eng., A 746, 372–383 (2019)CrossRef
39.
go back to reference C. Salama, C. Servant, G. Cizeron, Aging of the Inconel 718 alloy between 500 and 750 C. J. Mater. Res. 12, 2298–2316 (1997)CrossRef C. Salama, C. Servant, G. Cizeron, Aging of the Inconel 718 alloy between 500 and 750 C. J. Mater. Res. 12, 2298–2316 (1997)CrossRef
40.
go back to reference Y. Rong, S. Chen, G. Hu, M. Gao, R.P. Wei, Prediction and characterization of variant electron diffraction patterns for γ″ and δ precipitations in an INCONEL 718 alloy. Metall. Mater. Trans. A 30, 2297–2303 (1999)CrossRef Y. Rong, S. Chen, G. Hu, M. Gao, R.P. Wei, Prediction and characterization of variant electron diffraction patterns for γ″ and δ precipitations in an INCONEL 718 alloy. Metall. Mater. Trans. A 30, 2297–2303 (1999)CrossRef
41.
go back to reference M. Sundararaman, P. Mukhopadhayah, S. Banerjee, in Superalloys 718, 625, 706 and Various Derivatives, ed. by E.A. Loria (The Minerals, Metals and Materials Society, Warrendale, 1994) M. Sundararaman, P. Mukhopadhayah, S. Banerjee, in Superalloys 718, 625, 706 and Various Derivatives, ed. by E.A. Loria (The Minerals, Metals and Materials Society, Warrendale, 1994)
42.
go back to reference M.C. Chaturvedi, Y. Han, Effect of particle size on the creep rate of superalloy Inconel 718. Mater. Sci. Eng. 89, L7–L10 (1987)CrossRef M.C. Chaturvedi, Y. Han, Effect of particle size on the creep rate of superalloy Inconel 718. Mater. Sci. Eng. 89, L7–L10 (1987)CrossRef
43.
go back to reference M. Sundararaman, P. Mukhopadhayah, Overlapping of precipitate variants in Inconel 718. Mater. Charact. 31, 191–196 (1993)CrossRef M. Sundararaman, P. Mukhopadhayah, Overlapping of precipitate variants in Inconel 718. Mater. Charact. 31, 191–196 (1993)CrossRef
Metadata
Title
Optimization of Microstructure and Mechanical Properties of Hipped Inconel 718 by Various Heat Treatment Processes
Authors
Nader El-Bagoury
M. M. Hessien
Mohammed Alsawat
M. H. H. Mahmoud
Abdullah K. Alanazi
Naif Abdulrahman Alshanbari
Publication date
25-09-2019
Publisher
Springer US
Published in
Metallography, Microstructure, and Analysis / Issue 5/2019
Print ISSN: 2192-9262
Electronic ISSN: 2192-9270
DOI
https://doi.org/10.1007/s13632-019-00568-7

Other articles of this Issue 5/2019

Metallography, Microstructure, and Analysis 5/2019 Go to the issue

Premium Partners