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Journal of Materials Science: Materials in Electronics
Published in: Journal of Materials Science: Materials in Electronics 9/2018

07-02-2018

Photoreduction of 4-Nitrophenol in the presence of carboxylic acid using CdS nanofibers

Authors: Agileo Hernández-Gordillo, Próspero Acevedo-Peña, Monserrat Bizarro, Sandra E. Rodil, Ricardo Gómez

Published in: Journal of Materials Science: Materials in Electronics | Issue 9/2018

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Abstract

The photocatalytic reduction of 4-Nitrophenol was assisted with blue light irradiation using CdS semiconductor nanofiber. The kinetic study of the blue-photoreduction of 4-Nitrophenol to 4-Aminophenol was performed by using Na2SO3 as “hole scavenger” in the presence of middle carboxylic acids (acetic, oxalic and citric acid). The effect of photocatalyst load, the carboxylic acid concentration and of the pH solution (acid, neutral and alkaline media) were investigated. The maximum 4-Nitrophenol photoreduction rate was reached in neutral media and it is related to the enhanced “hole scavenging” effect caused by the SO32− or HSO32− ions in the presence of carboxylic acid. Electrochemical characterization of CdS nanofiber was made in the presence of 4-NP and citric acid. The 4-NP photoreduction reaction follows a zero order reaction and a possible mechanism to explain the fast electron transfer process is discussed as a consequence of the carboxylic acid adsorbed on the CdS surface.
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Metadata
Title
Photoreduction of 4-Nitrophenol in the presence of carboxylic acid using CdS nanofibers
Authors
Agileo Hernández-Gordillo
Próspero Acevedo-Peña
Monserrat Bizarro
Sandra E. Rodil
Ricardo Gómez
Publication date
07-02-2018
Publisher
Springer US
Published in
Journal of Materials Science: Materials in Electronics / Issue 9/2018
Print ISSN: 0957-4522
Electronic ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-018-8724-x

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