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Journal of Sol-Gel Science and Technology
Published in: Journal of Sol-Gel Science and Technology 1/2011

01-04-2011 | Original Paper

Preparation and characterization of diphasic sol-gel derived unsupported mullite membranes

Authors: Berna Topuz, Muhsin Çiftçioğlu

Published in: Journal of Sol-Gel Science and Technology | Issue 1/2011

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Abstract

Diphasic gels prepared by mixing freshly prepared polymeric silica and polymeric boehmite sols through a modified Al-alkoxide route in mullite compositions led to the crystallization of mullite upon heat treatment at 775 °C. Mullite formation was observed at a 100 °C higher temperature when diphasic gels were formed by mixing aged polymeric sols containing about 2 nm in diameter boehmite species. These relatively low mullite formation temperatures were attributed to the nanoscale sizes of the polymeric species of the two amorphous phases present in the diphasic gels.
previous article Preparation, dielectric and ferroelectric properties of (Na0.5Bi0.5)0.94Ba0.06TiO3 thin films by a sol–gel process
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Metadata
Title
Preparation and characterization of diphasic sol-gel derived unsupported mullite membranes
Authors
Berna Topuz
Muhsin Çiftçioğlu
Publication date
01-04-2011
Publisher
Springer US
Published in
Journal of Sol-Gel Science and Technology / Issue 1/2011
Print ISSN: 0928-0707
Electronic ISSN: 1573-4846
DOI
https://doi.org/10.1007/s10971-010-2347-x

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