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Journal of Materials Science

Published in:

01-06-2009

Preparation and electrochemical behavior of methylene blue intercalated into layered niobate K₄Nb₆O₁₇

Authors: Xiaobo Zhang, Dongsheng Feng, Meifeng Chen, Zhidan Ding, Zhiwei Tong

Published in: Journal of Materials Science | Issue 12/2009

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Abstract

K₄Nb₆O₁₇ nano-layered compound was obtained by solid-phase synthesis and then methylene blue (MB) was intercalated into layered niobate K₄Nb₆O₁₇ interlayer I by a two-step guest-guest exchange method using the intercalation compound, methyl viologen (MV²⁺)–K₄Nb₆O₁₇, as precursor. The optically transparent MB⁺–K₄Nb₆O₁₇ nanocomposite thin film has been characterized by XRD, IR, TGA, elemental analysis, UV, and electrochemical measurements. It was estimated that the intercalated MB⁺ ions are mainly aggregated. The cyclic voltammogram of the MB⁺–K₄Nb₆O₁₇ nanocomposite thin film exhibited a fine diffusion-controlled cathodic process, which hints the possibility of being utilized as an electrode modifying material.

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Title: Preparation and electrochemical behavior of methylene blue intercalated into layered niobate K4Nb6O17
Authors: Xiaobo Zhang
Dongsheng Feng
Meifeng Chen
Zhidan Ding
Zhiwei Tong
Publication date: 01-06-2009
Publisher: Springer US
Published in: Journal of Materials Science / Issue 12/2009
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI: https://doi.org/10.1007/s10853-009-3398-7

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