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Journal of Polymer Research
Published in: Journal of Polymer Research 4/2016

01-04-2016 | Original Paper

Preparation, characterization of nano-silica/fluoroacrylate material and the application in stone surface conservation

Authors: Xiaoying Zhang, Wenya Wen, Hanqiang Yu, Fengxian Qiu, Qian Chen, Dongya Yang

Published in: Journal of Polymer Research | Issue 4/2016

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Abstract

A series of fluoroacrylate (FPA) and nano-silica/fluoroacrylate were prepared. The properties including physical properties, mechanical behavior and contact angle of FPA were investigated. According to the results, the optimal fluoride content can be screened. The nano-silica/fluoroacrylate (SiO2/FPA) materials were characterized by fourier transform infrared (FT-IR), thermogravimetric analysis (TGA) and transmission electron microscope (TEM). The surface morphology and mineralogical analysis of the stone samples were characterized by scanning electron microscope (SEM) and X-ray diffraction (XRD), respectively. The prepared coating was selected to protect on the stone surface. Aimed at evaluating the coating performance, the protective performances were also evaluated by artificial aging test. The results indicated that when the content of hexafluoro-butyl methacrylate (HFMA) was 8.0 wt% and the content of SiO2 was 4.0 wt%, the prepared material has good compatibility and appearance with stone relics. The protective coating material for protection of chosen Jiaoshan Steles Grove (China) is noticeable and it can be widely applied to the protection of stone relics.
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Metadata
Title
Preparation, characterization of nano-silica/fluoroacrylate material and the application in stone surface conservation
Authors
Xiaoying Zhang
Wenya Wen
Hanqiang Yu
Fengxian Qiu
Qian Chen
Dongya Yang
Publication date
01-04-2016
Publisher
Springer Netherlands
Published in
Journal of Polymer Research / Issue 4/2016
Print ISSN: 1022-9760
Electronic ISSN: 1572-8935
DOI
https://doi.org/10.1007/s10965-016-0967-8

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