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Polymer Bulletin
Published in: Polymer Bulletin 6/2017

15-10-2016 | Original Paper

Role of surface modification of SiO2 with bio-safe citric acid on the morphological and thermal properties of nanocomposites based on N-trimellitylimido-l-methionine diacid and 4,4′-diaminodiphenyl ether: using ultrasound irradiation and ionic liquid

Authors: Shadpour Mallakpour, Marziyeh Shahrokhpour

Published in: Polymer Bulletin | Issue 6/2017

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Abstract

In this work, the surface of SiO2 NPs was modified with citric acid (CA) to prevent agglomeration of SiO2 nanoparticles (NP)s in the poly(amide-imide) (PAI) matrix. The PAI was synthesized from polymerization reaction of N-trimellitylimido-l-methionine with 4,4′-diaminodiphenyl ether using molten tetra-n-butylammonium bromide and triphenyl phosphite. PAI–SiO2/CA nanocomposites (PSCN)s were prepared via a fast ultrasonic irradiation process. The PSCNs were characterized by Fourier transform infrared spectroscopy, X-ray diffraction, field emission scanning electron microscopy, transmission electron microscopy and thermogravimetric analysis.
previous article Synthesis and characterization of chitosan/poly (vinylpyrrolidone) biocomposite for biomedical application
next article Thermal, physical, structural, thermomechanical features and single gas permeation comparison of fluorine, phenyl phosphine oxide-based copolyimides with poly(dimethylsiloxane)

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Metadata
Title
Role of surface modification of SiO2 with bio-safe citric acid on the morphological and thermal properties of nanocomposites based on N-trimellitylimido-l-methionine diacid and 4,4′-diaminodiphenyl ether: using ultrasound irradiation and ionic liquid
Authors
Shadpour Mallakpour
Marziyeh Shahrokhpour
Publication date
15-10-2016
Publisher
Springer Berlin Heidelberg
Published in
Polymer Bulletin / Issue 6/2017
Print ISSN: 0170-0839
Electronic ISSN: 1436-2449
DOI
https://doi.org/10.1007/s00289-016-1829-6

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