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Journal of Materials Science: Materials in Electronics
Published in: Journal of Materials Science: Materials in Electronics 4/2016

14-12-2015

Simple synthesis and characterization of nickel phosphide nanostructures assisted by different inorganic precursors

Authors: Azam Sobhani, Masoud Salavati-Niasari

Published in: Journal of Materials Science: Materials in Electronics | Issue 4/2016

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Abstract

Nickel phosphide nanostructures were prepared by thermal decomposition method from different inorganic precursors, such as: bis(salicylidene)nickel(II) [Ni(sal)2], bis(salicylate)nickel(II) [Ni(Hsal)2], nickel oxalate [Ni(O4C2)(H2O)4] and nickel-o-phthalate [Ni(pht)(H2O)2]. Nickel(II) acetate tetrahydrate Ni(CH3COO)2·4H2O was used as reference. Nanostructural control of products prepared through the thermolysis of precursors using triphenylphosphine as a surfactant solvent and phosphorus precursor was reported. The SEM and TEM images show the morphology and particle size of the as-synthesized nanostructures. The XRD patterns show mixed-phase hexagonal Ni2P/tetragonal Ni12P5 (represented as NixPy). The FT-IR spectroscopy confirms that the products prepared are NixPy phase, which is in agreement with XRD results.
previous article Study on the properties of Zn–xNi high temperature solder alloys
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Metadata
Title
Simple synthesis and characterization of nickel phosphide nanostructures assisted by different inorganic precursors
Authors
Azam Sobhani
Masoud Salavati-Niasari
Publication date
14-12-2015
Publisher
Springer US
Published in
Journal of Materials Science: Materials in Electronics / Issue 4/2016
Print ISSN: 0957-4522
Electronic ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-015-4199-1

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