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Journal of Nanoparticle Research

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01-11-2012 | Research Paper

Size-controlled synthesis of Fe₂O₃ and Fe₃O₄ nanoparticles onto zeolite by means of a modified activated-coprecipitation method: effect of the HCl concentration during the activation

Authors: S. Mendoza-Bello, Raúl A. Morales-Luckie, L. Flores-Santos, Juan P. Hinestroza, Víctor Sanchez-Mendieta

Published in: Journal of Nanoparticle Research | Issue 11/2012

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Abstract

Synthetic sodium type A zeolite bearing Fe₂O₃ and Fe₃O₄ nanoparticles composites have been prepared by means of a coprecipitation method with two different activation methodologies, one using Sn and the other using Sn/Pd nanoparticles as activators. Sn activation generates hematite nanoparticles while Sn/Pd produces magnetite nanoparticles. Amount of HCl used during the activation of the zeolite with SnCl₂ showed a correlation between the stannous activating species and the particle size. Both Sn and Sn–Pd activated nanocomposites show nearly narrow size distributions but only those iron oxides obtained with Sn–Pd showed supermagnetism.

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Title: Size-controlled synthesis of Fe2O3 and Fe3O4 nanoparticles onto zeolite by means of a modified activated-coprecipitation method: effect of the HCl concentration during the activation
Authors: S. Mendoza-Bello
Raúl A. Morales-Luckie
L. Flores-Santos
Juan P. Hinestroza
Víctor Sanchez-Mendieta
Publication date: 01-11-2012
Publisher: Springer Netherlands
Published in: Journal of Nanoparticle Research / Issue 11/2012
Print ISSN: 1388-0764
Electronic ISSN: 1572-896X
DOI: https://doi.org/10.1007/s11051-012-1242-5

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