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Biomass Categories Read chapter Read first chapter

2020 | OriginalPaper | Chapter

9. Sludge

Authors : Patricia Arlabosse, Ange Nzihou, Stewart Oakley, Martial Sauceau, Christelle Tribout, Fei Wang, Yaqian Zhao

Published in: Handbook on Characterization of Biomass, Biowaste and Related By-products

Publisher: Springer International Publishing

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Abstract

Water treatment residuals, sewage sludge and dredged sediments, hereinafter referred to as sludge, share common features, like inherent high moisture content, high organic and mineral pollutant load and above all a pasty consistency. Several recovery opportunities exist. However, sludge composition is closely correlated with human activity and the design of the recovery processes requires knowledge of physical, thermal or biological characteristics of the sludge that will be processed, often even before the specific sludge exists. Therefore, sludge characterization is a key challenge for the process design, control and optimization and further valorization. The present chapter is divided into four parts dedicated to the composition, the material properties, the dynamic processing properties and the environmental assessments, respectively. Standard tests methods for the characterization of solids and water distribution in sludge are introduced first. Then, the fate of organic constituents, inorganic nonmetallic and metallic constituents as well as pathogenic organism. In the second part, standard and state-of-the-art methods for the characterization of chemical, physical and thermal properties of sludge are described. Dynamic tests, required for the selection and design of conventional processes for sludge concentration and conveying, are detailed in the third part. Finally, methods for assessing the environment impacts of sludge and secondary raw materials derived from sludge are addressed.

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Footnotes
1
In this document “release” is used to indicate the transfer of an ion from one environment to another.
 
2
It should be remembered that solubility indicates the tendency of substances to be mobilised by leaching; availability is the release potential in relation to total content.
 
3
The CEAMaS project is an international project promoted and financed by the European Union aiming to encourage knowledge and a consensus to bring forward new solutions for the re-use of marine sediments to be applicable throughout Europe. (http://​www.​ceamas.​eu/​fr).
 
Literature
1.
ISO: Water Quality—Sampling—Part 13: Guidance on Sampling of Sludges. 5667-13:2011 (2011)
2.
ISO: Water Quality—Sampling—Part 15: Guidance on Preservation and Handling of Sludge and Sediment Samples. 5667-15:2009 (2009)
3.
AFNOR: Sludge, Treated Biowaste and Soil—Guidance for Sample Pretreatment. NF EN 16179 (2012)
4.
Tchobanoglous, G., Burton, F.: Wastewater engineering. In: Treatment and Reuse, 4th edn. McGrawHill, New York (2003)
5.
AFNOR: Characterization of Sludges—Determination of Dry Residue and Water Content. FR EN 12880:2000 (2000)
6.
Rice, E.W., Baird, R.B., Eaton, A.D., Clesceri, L.S.: Standard Methods for the Examination of Water and Wastewater—Method 2540.G Total, Fixed, and Volatile Solids in Solid and Semisolid Samples. American Public Health Association, Washington DC (2012)
7.
Spellman, F.R.: Handbook of Water and Wastewater Treatment Plant Operations. CRC Press, Boca Raton (2014)
8.
AFNOR: Water Quality—Determination of Suspended Solids. Method by Filtration Through Glass Fibre Filters. NF EN 872 (2005)
9.
Rice, E.W., Baird, R.B., Eaton, A.D., Clesceri, L.S.: Standard Methods for the Examination of Water and Wastewater—Method 2540.D Total Suspended solids dried at 103–105°C. American Public Health Association, Washington DC (2012)
10.
AFNOR: Water Quality—Determination of Suspended Solids by Filtration Through Glass Filters. ISO 11923:1997 (1997)
11.
AFNOR: Water Quality—Determination of Suspended Solids. Method by Centrifugation. NF T90-105-2 (1997). (in French)
12.
Degrémont: Water Treatment Handbook, 7th edn. Lavoisier SAS, Cachan (2007)
13.
Vesilind, A.: The role of water in sludge dewatering. Water Environ. Res. 66(1), 4–11 (1994)CrossRef
14.
Colin, F., Gazbar, S.: Distribution of water in sludges in relation to their mechanical dewatering. Water Res. 29(8), 2000–2005 (1995)CrossRef
15.
Legrand, V.: Study of deswelling and flocculation of polyelectrolyte gel networks: application to wastewater sludge dewatering. PhD dissertation. Université Paris VI, France (1997). (in French)
16.
Vaxelaire, J., Cezac, P.: Moisture distribution in activated sludges: a review. Water Res. 38(9), 2215–2230 (2004)CrossRef
17.
Vaxelaire, J.: Moisture sorption characteristics of waste activated sludge. J. Chem. Technol. Biotechnol. 76(4), 377–382 (2001)CrossRef
18.
Leung, H.K.: Water Activity and Other Colligate Properties of Foods. ASAE Paper No. 83–6508, Chicago (1983)
19.
Rouquerol, F., Rouquerol, J., Sing, K.S.W., Llewellyn, P., Maurin, G.: Adsorption by Powders and Porous Solids: Principles, Methodology and Applications. Academic Press, Oxford (1999)
20.
Ritzi, S.S.H.: Thermodynamic properties of foods in dehydration. In: Dekker, Marcel (ed.) Engineering Properties of Foods, pp. 359–436. Marcel Dekker, New-York (1986)
21.
Jowitt, R., Wagstaffe, P.J.: The Certification of Water Content of Microcrystalline Cellulose (MCC) at 10 Water Activities: CRM 302. Commission of the European Communities, Luxembourg (1989)
22.
Rahman, S.: Food Properties Handbook. CRC Press, Boca Raton (1995)
23.
Wolf, W., Spiess, W.E.L., Jung, G., Wiesser, H., Bizot, H., Duckworth, R.B.: The water-vapour sorption isotherms of microcrystalline cellulose (MCC) and of purified potato starch. Results of a collaborative study. J. Food Eng. 3(1), 51–73 (1984)CrossRef
24.
Brunauer, S., Emmett, P.H., Teller E.: The adsorption of gases in multimolecular layers. J.A.C.S. 60, 309–319 (1938)CrossRef
25.
26.
Arrêté du 8 janvier 1998 fixant les prescriptions techniques applicables aux épandages de boues sur les sols agricoles pris en application du décret n°97–1133 du 8 décembre 1997 relatif à l’épandage des boues issues du traitement des eaux usées. (in French)
27.
28.
GB: Discharge Standard of Pollutants for Municipal Wastewater Treatment Plant. 18918-2002
29.
Clarke, B., Porter, N., Symons, R., Blackbeard, J., Ades, P., Marriott, P.: Dioxin-like compounds in Australian sewage-sludge—review and national survey. Chemosphere 72, 1215–1228 (2008)CrossRef
30.
Zuloaga, O., Navarro, P., Bizkarguenaga, E., Iparraguirre, A., Vallejo, A., Olivares, M., Prieto, A.: Overview of extraction, clean-up and detection techniques for the determination of organic pollutants in sewage sludge: a review. Anal. Chim. Acta 736, 7–29 (2012)CrossRef
31.
AFNOR: Determination of Polycyclic Aromatic Hydrocarbons (PAHs) in Waste using Gas Chromatography Mass Spectrometry. NF EN 15527:2008 (2008)
32.
33.
ISO: Soil Quality—Determination of Dioxins and Furans and Dioxin-like Polychlorinated Biphenyls by Gas Chromatography with High-Resolution Mass Selective Detection (GC/HRMS). 13914:2013 (2013)
34.
ISO: Soil Quality—Determination of Nonylphenols (NP) and Nonylphenol-mono- and Diethoxylates—Method by Gas Chromatography with Mass Selective Detection (GC-MS). 13907:2012 (2012)
35.
ISO: Soil Quality—Determination of Selected Phthalates Using Capillary Gas Chromatography with Mass Spectrometric Detection (GC/MS). 13913:2014 (2014)
36.
ISO: Soil Quality—Determination of Linear Alkylbenzene Sulfonate (LAS)—Method by HPLC with Fluorescence Detection (LC-FLD) and Mass Selective Detection (LC-MSD). 13896:2012 (2012)
37.
AFNOR: Sludge, Treated Biowaste and Soil—Determination of Adsorbable Organically Bound Halogens (AOX). NF EN 16166:2012 (2012)
38.
39.
Commission of the European Communities: Council Directive 86/278/EEC of 12 June 1986 on the Protection of the Environment, and in Particular of the Soil, When Sewage Sludge is Used in Agriculture (1986)
40.
Us, E.P.A.: Land Application of Sewage Sludge—A Guide for Land Appliers on the Requirements of the Federal Standards for the use or Disposal of Sewage Sludge, 40 CFR Part 503. United States Environmental Protection Agency, Washington DC (1994)
41.
GB: Control Standards for Pollutants in Sludge from Agricultural Use. 4284-84 (1984)
42.
Rice, E.W., Baird, R.B., Eaton, A.D., Clesceri, L.S.: Standard Methods for the Examination of Water and Wastewater—Method 3120.B Inductively Coupled Plasma (ICP) Method. American Public Health Association, Washington DC (2012)
43.
Rice, E.W., Baird, R.B., Eaton, A.D., Clesceri, L.S.: Standard Methods for the Examination of Water and Wastewater—Method 3030.F. Nitric Acid-Hydrochloric Acid Digestion. American Public Health Association, Washington DC (2012)
44.
Rice, E.W., Baird, R.B., Eaton, A.D., Clesceri, L.S.: Standard Methods for the Examination of Water and Wastewater—Method 3030.K. Microwave Assisted Digestion American Public Health Association, Washington DC (2012)
45.
AFNOR: Sludge, Treated Biowaste and Soil—Determination of Elements Using Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES). FR EN 16170:2016 (2016)
46.
AFNOR: Sludge, Treated Biowaste and Soil—Digestion of Nitric Acid Soluble Fractions of Elements. FR EN 16173:2012 (2012)
47.
AFNOR: Sludge, Treated Biowaste and Soil—Digestion of Aqua Regia Soluble Fractions of Elements. FR EN 16174:2012 (2012)
48.
AFNOR: Determination of Elemental Composition by X-ray Fluorescence. FR EN 15309:2009 (2009)
49.
Pathak, A., Dastidar, M.G., Sreekrishnan, T.R.: Bioleaching of heavy metals from sewage sludge: a review. J. Environ. Manage. 90, 2343–2353 (2009)CrossRef
50.
Ahmad, T., Ahmad, K., Alam, M.: Sustainable management of water treatment sludge through 3‘R’ concept. J. Clean. Prod. 124(Supplement C), 1–13 (2016)CrossRef
51.
Babatunde, A.O., Zhao, Y.Q.: Constructive approaches toward water treatment works sludge management: an international review of beneficial reuses. Crit. Rev. Environ. Sci. Technol. 37, 129–164 (2007)CrossRef
52.
Chiang, K.-Y., Chou, P.H., Hua, C.R., Chien, K.L., Cheeseman, C.: Light weight bricks manufactured from water treatment sludge and rice husks. J. Hazard. Mater. 171, 76–82 (2009)CrossRef
53.
Ippolito, J.A., Barbarick, K.A., Elliot, H.A.: Drinking water treatment residuals: a review of recent uses. J. Environ. Qual. 2, 1–12 (2011)CrossRef
54.
Razali, M., Zhao, Y.Q., Bruen, M.: Effectiveness of a drinking water treatment sludge in removing different phosphorus species from aqueous solution. Sep. Purif. Technol. 55, 300–306 (2007)CrossRef
55.
Sales, A., Rodrigues de Souza, F., do Cousto Rosa Almeida, F.: Mechanical properties of concrete produced with a composite of water treatment sludge and sawdust. Constr. Build. Mater. 25(6), 2793–2798 (2011)CrossRef
56.
Sotero-Santos, R.B., Rocha, O., Povinelli, J.: Evaluation of watertreatment sludges toxicity using the Daphnia bioassay. Water Res. 39(16), 3909–3917 (2005)CrossRef
57.
Zou, J.L., Xu, G.R., Li, G.B.: Ceramsite obtained from water and wastewater sludge and its characteristics affected by Fe2O3, CaO, and MgO. J. Hazard. Mater. 165, 995–1001 (2009)CrossRef
58.
Ippolito, J.A., Barbarick, K.A., Redente, E.F.: Co-application effects of water treatment residuals and biosoilds on two range grasses. J. Environ. Qual. 28, 1644–1650 (1999)CrossRef
59.
Heil, D.M., Barbarick, K.A.: Water treatment sludge influence on the growth of Sorghum-Sudangrass. J. Environ. Qual. 19, 292–298 (1989)CrossRef
60.
Elliott, H.A., Singer, L.M.: Effect of water treatment sludge on growth and element composition of tomato shoots. Commun. Soil Sci. Plant Anal. 19, 345–354 (1988)CrossRef
61.
Diquattro, S., Garau, G., Lauro, G.P., Silvetti, M., Deiana, S., Castaldi, P.: Municipal solid waste compost as a novel sorbent for antimony (V): adsorption and release trials at acidic pH. Environ. Sci. Pollut. Res. 25(6), 5603–5615 (2018)CrossRef
62.
Elkhatib, E., Moharem, M., Mahdy, A., Mesalem, M.: Sorption, release and forms of mercury in contaminated soils stabilized with water treatment residual nanoparticles. Land Degrad. Dev. 28, 752–761 (2017)CrossRef
63.
Tay, D.Y.Y., Fujinuma, R., Wendling, L.A.: Drinking water treatment residual use in urban soils: balancing metal immobilization and phosphorus availability. Geoderma 305, 113–121 (2017)CrossRef
64.
Ociński, D., Jacukowicz-Sobala, I., Mazur, P., Raczyk, J., Kociolek-Balawejder, E.: Water treatment residuals containing iron and manganese oxides for arsenic removal from water—characterization of physicochemical properties and adsorption studies. Chem. Eng. J. 294, 210–221 (2016)CrossRef
65.
Elkhatib, E.A., Moharem, M.L.: Immobilization of copper, lead, and nickel in two arid soils amended with biosolids: effect of drinking water treatment residuals. J.S.S. 15,1937–1946 (2015)CrossRef
66.
Ippolito J.A.: Aluminum-based water treatment residual use in a constructed wetland for capturing urban runoff phosphorus: column study. Water Air Soil Pollut. 226, 334 (2015)
67.
Silvetti, M., Castaldi, P., Garau, G., Demurtas, D., Deiana, S.: Sorption of Cadmium (II) and Zinc (II) from aqueous solution by water treatment residuals at different pH values. Water, Air Soil Pollut. 226, 313 (2015)
68.
Wang, C., Pei, Y., Zhao, Y.: Comparison of metal lability in air-dried and fresh dewatered drinking water treatment residuals. J. Environ. Sci. Health A 50, 135–143 (2015)CrossRef
69.
Elliott, H.A., Taylor, M.: Phosphorus partitioning in co-dewatering biosolids and water treatment residuals. Wat. Sci. Technol. 70, 422–430 (2014)CrossRef
70.
Bhatnagar, A., Sillanpää, M.: Removal of natural organic matter (NOM) and its constituents from water by adsorption—a review. Chemosphere 166, 497–510 (2017)CrossRef
71.
Schmidt, S.B., Jensen, P.E., Husted, S.: Manganese deficiency in plants: the impact on photosystem II. Trends Plant Sci. 21, 622–632 (2016)CrossRef
72.
73.
74.
WHO: Guidelines for the Safe use of Wastewater, Excreta, and Greywater, vol. 4. Excreta and greywater use in agriculture. Geneva (2006)
75.
Feachem, R.G., Bradley, D.J., Garelick, H., Mara, D.D.: Sanitation and Disease. Health Aspects of Excreta and Wastewater Management. Wiley, Chichester (1983)
76.
Carrington, E.G.: Evaluation of Sludge Treatments for Pathogen Reduction-Final Report, Report No. CO 5026/1, European Commission (2001)
77.
Andreoli, C.V., Von Sperling, M., Fernandes, F.: Sludge Treatment and Disposal, Biological Wastewater Treatment Series, vol. 4. IWA Publishing, London (2007)
78.
Lepeuple, A.S., Gaval, G., Jovic, M., de Roulin, M.R.: Literature review on levels of pathogens and their abatement in sludges, soil and treated biowaste. Horizontal Project 6 (2004)
79.
80.
ISO Particle Size Analysis—Laser Diffraction Methods. 13320:2009 (2009)
81.
GB/T Particle Size Analysis—Laser diffraction methods. 19077-2016 (2016)
82.
ISO Particle Size Analysis-Laser Diffraction Methods—Part 1: General Principles. 13220:1999-1 (1999)
83.
Bieganowski, A., Lagod, G., Ryzak, M., Montusiewicz, A., Chomczynska, M., Sochan, A.: Measurement of activated sludge particle diameters using laser diffraction method. Ecol. Chem. Eng. S 19(4), 597–608 (2012)
84.
Chaignon, V., Lartiges, B.S., El Samrani, A., Mustin, C.: Evolution of size distribution and transfer of mineral particles between flocs in activated sludges: an insight into floc exchange dynamics. Water Res. 36(3), 676–684 (2002)CrossRef
85.
Charlou, C.: Caractérisation et modéisation de l’écoulement de boues résiduaires dans un sécheur à palettes, PhD dissertation, Université de Toulouse, 200 p. (2014). (in French)
86.
ASTM Standard Test Method for Screening Apparent Specific Gravity and Bulk Density of Waste. D5057-17 (2017)
87.
Sørensen, B.L., Wakeman, R.J.: Filtration characterization and specific surface area measurement of activated sludge by Rhodamine B adsorption. Water Res. 30(1), 115–121 (1996)CrossRef
88.
Smith, P.G., Coackley, P.: A method for determining specific surface area of activated sludge by dye adsorption. Water Res. 17(5), 595–598 (1983)CrossRef
89.
ASTM Standard Test Methods for Screening of pH in Waste. D4980-89 (1989)
90.
Tan, G.D.: Analysis of characteristics of sludge in Beijing wastewater treatment plant. Sci. Technol. Inf. 7, 340 (2011)
91.
Fytili, D., Zabaniotou, A.: Utilization of sewage sludge in EU application of old and new methods—a review. Renew. Sust. Energ. Rev. 12(1), 116–140 (2008)CrossRef
92.
ASTM Standard Test Methods for Acidity or Alkalinity of Water. D1067-16 (2016)
93.
Sun, J.H., Zhang, S.T., Yao, Y.: On the buffering performance of activated sludge. J. Saf. Environ. 1, 199–202 (2015)
94.
Quevauviller, P., Donard, O.F.X., Maier, E.A., Griepink, B.: Improvements of speciation analyses in environmental matrices. Microchim. Acta 109(1–4), 169–190 (1992)CrossRef
95.
Pustišek, N., Milačič, R., Veber, M.: Use of the BCR three-step sequential extraction procedure for the study of the partitioning of Cd, Pb and Zn in various soil samples. J. Soils Sed. 1(1), 25–29 (2001)CrossRef
96.
Liang, X., Ning, X., Chen, G., Lin, M., Liu, J., Wang, Y.: Concentrations and speciation of heavy metals in sludge from nine textile dyeing plants. Ecotoxicol. Environ. Saf. 98, 128–134 (2013)CrossRef
97.
ISO Soil Quality—Parameters for Geochemical Modelling of Leaching and Speciation of Constituents in Soils and Materials. 12782:2012 (2012)
98.
Alonso, E., Villar, P., Santos, A., Aparicio, I.: Fractionation of heavy metals in sludge from anaerobic wastewater stabilization ponds in Southern Spain. Waste Manage. 26, 1270–1276 (2006)CrossRef
99.
Yang, Y., Tomlinson, D., Kennedy, S., Zhao, Y.Q.: Dewatered alum sludge: a potential adsorbent for phosphorus removal. Water Sci. Technol. 54, 207–213 (2006)CrossRef
100.
Yang, Y., Zhao, Y.Q., Babatunde, A.O., Wang, L., Ren, Y.X., Han, Y.: Characteristics and mechanisms of phosphate adsorption on dewatered alum sludge. Sep. Purif. Technol. 51, 193–200 (2006)CrossRef
101.
Yang, Y., Zhao, Y.Q., Kearney, P.: Influence of ageing on the structure and phosphate adsorption capacity of dewatered alum sludge. Chem. Eng. J. 145, 276–284 (2008)CrossRef
102.
103.
Babatunde, A.O., Zhao, Y.Q., Yang, Y., Kearney, P.: Reuse of dewatered aluminium-coagulated water treatment residual to immobilize phosphorus: batch and column trials using a condensed phosphate. Chem. Eng. J. 136, 108–115 (2008)CrossRef
104.
Makris, K.C., Harris, W.G., O’Conno, G.A., Obreza, T.A.: Phosphorus immobilization in micropores of drinking-water treatment residuals: implications for long-term stability. Environ. Sci. Technol. 38, 6590–6596 (2004)CrossRef
105.
Makris, K.C., Harris, W.G., O’Conno, G.A., Obreza, T.A., Helliot, H.A.: Physicochemical properties related to long-term phosphorus retention by drinking water treatment residuals. Environ. Sci. Technol. 39, 4280–4289 (2005)CrossRef
106.
AFNOR Solid Biofuels—Method for the Determination of Calorific Value, CEN/TS 14918:2005 (2005)
107.
AFNOR Solid recovered fuels—Determination of Calorific Value, EN 15400 (2011)
108.
Thipkhunthod, P., Meeyoo, V., Rangsunvigit, P., Kitiyanan, B., Siemanond, K., Rirksomboon, T.: Predicting the heating value of sewage sludges in Thailand from proximate and ultimate analyses. Fuel 84, 849–857 (2005)CrossRef
109.
Demirbas, A.: Calculation of higher heating values of biomass fuels. Fuel 76, 431–434 (1997)CrossRef
110.
Cordero, T., Marquez, F., Rodriguez-Mirasol, J., Rodriguez, J.J.: Predicting heating value of lignocellulosic and carbonaceous materials from proximate analysis. Fuel 80, 1567–1571 (2001)CrossRef
111.
Parikh, J., Channiwala, S.A., Ghosal, G.K.: A correlation for calculating HHV from proximate analysis of solid fuels. Fuel 84, 487–494 (2005)CrossRef
112.
US EPA Process Design Manual Sludge Treatment and Disposal, US Environmental Protection Agency (1979)
113.
Calvo, L.F., Otero, M., Jenkins, B.M., Garcia, A.I., Moran, A.: Heating process characteristics and kinetics of sewage sludge in different atmospheres. Thermochim. Acta 409, 127–135 (2004)CrossRef
114.
ASTM D5334-14 Standard Test Method for Determination of Thermal Conductivity of Soil and Soft Rock by Thermal Needle Probe Procedure. ASTM International, West Conshohocken
115.
Ladevie, B., Fudym, O., Batsale, J.C.: A new simple device to estimate the thermophysical properties of insulating materials. Int. Commun. Heat Mass Transf. 27(4), 473–484 (2000)CrossRef
116.
Ferrasse, J.H.: Développement d’outils expérimentaux pour le dimensionnement de procédés de séchage conductif avec agitation: application à des boues de stations d’épuration urbaines. PhD Dissertation, Université de Toulouse, p. 207 (2000). (in French)
117.
Spinosa, L., Wichmann, K.: Sludge characterization: the role of physical consistency. Water Sci. Technol. 49(10), 59–65 (2004)CrossRef
118.
AFNOR Usefulness of Rheological Characterization in Sludge Management. CEN/TC308 Report CEN/TC308/WG2-N25 (1995)
119.
Spinosa, L., Lotito, V.: Rheological Measurements and Their Application in Biosolids Management. Water 21, 28–29 (1999)
120.
AFNOR: Sols: reconnaissance et essais - Détermination des limites d’Atterberg - Limite de liquidité à la coupelle - Limite de plasticité au rouleau, NF P94-051 (1993)
121.
AFNOR: Geotechnical Investigation and Testing—Laboratory Testing of Soil—Part 12: Determination of Atterberg limits, XP CEN ISO/TS 17892-12 (2006)
122.
ASTM: Standard Test Methods for Liquid Limit, Plastic Limit, and Plasticity Index of Soils, D4318 (2017)
123.
AFNOR: Characterization of Sludges—Physical Consistency—Thixotropic Behaviour and Piling Behavior, CEN/TR 15463 (2007)
124.
AFNOR, Glossary of Wastewater Engineering Terms, EN 16323 (2014)
125.
Eshtiaghi, N., Markis, F., Yap, S.D., Baudez, J.C., Slatter, P.: Rheological characterisation of municipal sludge: a review. Water Res. 47(15), 5493–5510 (2013)CrossRef
126.
Seyssiecq, I., Ferrasse, J.H., Roche, N.: State-of-the-art: rheological characterisation of wastewater treatment sludge. Biochem. Eng. J. 16(1), 41–56 (2003)CrossRef
127.
Coussot, P.: Steady, laminar, flow of concentrated mud suspensions in open-channel. J. Hydraul. Res. 32(4), 535–559 (1994)CrossRef
128.
Baudez, J.C., Chabot, F., Coussot, P.: Rheological interpretation of the slump test. Appl. Rheol. 12(3), 133–141 (2002)CrossRef
129.
ASTM: Standard Test Method for Determining the Viscosity of Emulsified Asphalts Using a Rotational Paddle Viscometer, D7226-13 (2017)
130.
AFNOR: Determination of Dynamic Viscosity of Bituminous Binder Using a Rotating Spindle Apparatus, NF EN 13302 (2010)
131.
AFNOR: Bitumen and Bituminous Binders Determination of Dynamic Viscosity of Modified Bitumen by Cone and Plate Method, NF EN 13702 (2010)
132.
ASTM: Standard Test Method for High-Shear Viscosity Using a Cone/Plate Viscometer, D4287 (2014)
133.
AFNOR: Determination of Viscosity Using Rotary Viscometers. Part 1: Cone-and-Plate Viscometer Operated at a High Rate of Shear, NF EN ISO 2884-1 (2006)
134.
ASTM: Standard Test Method for Yield Stress of Heterogeneous Propellants by Cone Penetration Method, D2884-93 (2002)
135.
AFNOR: Characterization of Sludges—Physical Consistency—Part 1: Determination of Flowability—Method by Extrusion Tube Apparatus, NF EN 16720-1 (2016)
136.
Ratkovich, N., Horn, W., Helmus, F.P., Rosenberger, S., Naessens, W., Nopens, I., Bentzen, T.R.: Activated sludge rheology: a critical review on data collection and modelling. Water Res. 47(2), 463–482 (2013)CrossRef
137.
Spinosa, L., Wichmann, K.: Physical consistency: a useful tool for sludge characterization to the implementation of European standards. Ingénieries Eau-Agriculture-Territoires, Numéro spécial “Les boues résiduaires: quelle caractérisation et quels impacts environnementaux pour l’épandage agricole?”, pp. 9-22 (2008)
138.
Spinosa, L., Lotito, V.: A simple method for evaluating sludge yield stress. Adv. Environ. Res. 7(3), 655–659 (2003)CrossRef
139.
ASTM: Standard Test Methods for Laboratory Miniature Vane Shear Test for Saturated Fine-Grained Clayey Soil, D 4648 (2016)
140.
AFNOR: Sols: reconnaissance et essais - Essai scissométrique en laboratoire, NF P94-072 (1995)
141.
ASTM: Standard Test Methods for Cone Penetration of Lubricating Grease, D217-17 (2017)
142.
AFNOR: Petroleum Products and Lubricants—Determination of Cone Penetration of Lubricating Grease and Petrolatum, NF ISO 2137 (1985)
143.
AFNOR: Adjuvants pour béton, mortier et coulis—Méthodes d’essai—Partie 2: détermination du temps de prise, NF EN 480-2 (2006)
144.
ASTM: Standard Test Methods for Time of Setting of Hydraulic Cement by Vicat Needle, C191 (2013)
145.
AFNOR: Plastiques - Matières thermoplastiques - Détermination de la température de ramollissement Vicat, NF EN ISO 306 (1014)
146.
ASTM: Standard Test Method for Vicat Softening Temperature of Plastics, D1525 (2017)
147.
Hansbo, S.: A new approach to the determination of the shear strength of clays by the fall-cone test. Proc. Roy. SGI 14, 7–48 (1957)
148.
Mouzaoui, M., Baudez, J.C., Sauceau, M., Arlabosse, P.: Experimental rheological procedure adapted to dewatered sludge up to 45% dry matter. Water Res. 133, 1–7 (2018)CrossRef
149.
Liang, F., Sauceau, M., Dusserre, G., Arlabosse, P.: A uniaxial cyclic compression method for characterizing the rheological and textural behaviors of mechanically dewatered sewage sludge. Water Res. 113, 171–180 (2017)CrossRef
150.
Ruiz, T., Wisniewski, C., Kaosol, T., Persin, F.: Influence of organic content in dewatering and shrinkage of urban residual sludge under controlled atmospheric drying. Process Saf. Environ. 85(B1), 104–110 (2007)CrossRef
151.
Ruiz, T., Wisniewski, C.: Correlation between dewatering and hydro-textural characteristics of sewage sludge during drying. Sep. Purif. Technol. 61(2), 204–210 (2008)CrossRef
152.
Ruiz, T., Kaosol, T., Wisniewski, C.: Dewatering of urban residual sludges: filterability and hydro-textural characteristics of conditioned sludge. Sep. Purif. Technol. 72(3), 275–281 (2010)CrossRef
153.
Liang, F.: Caractérisation et modélisation du comportement rhéologique des boues résiduaires. PhD Dissertation, Ecole des Mines d’Albi-Carmaux (2016). (in French)
154.
Kudra, T.: Sticky region in drying—definition and identification. Drying Technol. 21(8), 1457–1469 (2003)CrossRef
155.
Peeters, B., Dewil, R., Van Impe, J.F., Vernimmen, L., Smets, I.Y.: Using a shear test-based lab protocol to map the sticky phase of activated sludge. Environ. Eng. Sci. 28(1), 81–85 (2010)CrossRef
156.
ASTM: Standard Test Method for Shear Testing of Bulk Solids Using the Jenike Shear Tester, ASTM D 6128 (2016)
157.
Li, B., Wang, F., Chi, Y., Yan, J.H.: Adhesion and cohesion characteristics of sewage sludge during drying. Drying Technol. 32(13), 1598–1607 (2014)CrossRef
158.
Liang, F., Chen, X., Mao, H., Sauceau, M., Arlabosse, P., Wang, F., Chi, Y.: The microstructure: a critical factor in characterising the sticky properties of highly concentrated sewage sludge. In: 6th International Conference on Engineering for Waste and Biomass Valorisation, Albi (2016)
159.
Arlabosse, P., Chavez, S., Lecomte, D.: Method for thermal design of paddle dryers: application to municipal sewage sludge. Drying Technol. 22(10), 2375–2393 (2004)CrossRef
160.
161.
162.
AFNOR: Characterization of Waste. Methodology for the Determination of the Leaching Behaviour of Waste Under Specified Conditions, NF EN 12920 + A1 (2008)
163.
Crest, M.: Etude multi-échelle de percolations instationnaires à travers un résidu minéral réactif et modélisations hydrodynamiques associées – Applicabilité de la norme NF EN 12920, PhD thesis, Institut National des Sciences Appliquées de Lyon (2007). (in French)
164.
165.
166.
Council of the European Union: Council Directive 1999/31/EC of 26 April 1999 on the landfill of waste. Official Journal L 182 published on 16/07/1999, 1-19 (1999)
167.
Council of the European Union: Council Decision DC 2003/33/EC of 19 December 2002 establishing criteria and procedures for the acceptance of waste at landfills pursuant to Article 16 of and Annex II to Directive 1999/31/EC. Official Journal L 011 published on 16/01/2003, 27-49 (2003)
168.
EA NEN: Leaching Characteristics—Determination of the Availability of Inorganic Components for Leaching—Solid Earthy and Stony Materials. NEN 7371 (2004)
169.
EA NEN: Leaching Characteristics of Moulded or Monolithic Building and Waste Materials—Determination of Leaching of Inorganic Components with the Diffusion Test—Tank Leaching Test. NEN 7375 (2004)
170.
AFNOR: Characterization of Waste—Leaching Behaviour Test—Up-Flow Percolation Test (under specified conditions). NF EN 14405 (2017)
171.
AFNOR: Characterization of Waste—Leaching Behaviour Test—Influence of pH on Leaching with Initial Acid/Base Addition. NF EN 14429 (2015)
172.
AFNOR: Characterization of Waste—Leaching Behaviour Test—Influence of pH on Leaching with Continuous pH Control. NF EN 14997 (2015)
173.
AFNOR: Characterization of Waste—Leaching Behaviour Test for Basic Characterization—Dynamic Monolithic Leaching Test with Periodic Leachant Renewal, Under Fixed Conditions. NF EN 15863 (2015)
174.
175.
AFNOR: Characterization of Waste—Leaching Behaviour Test for Basic Characterization—Dynamic Monolithic Leaching Test with Continuous Leachant Renewal Under Conditions Relevant for Specified Scenario(s). XP CEN/TS 15864 (2016)
176.
AFNOR: Caractérisation des déchets - Lixiviation - Essai de conformité pour lixiviation des déchets fragmentés et des boues - Partie 1: essai en bâchée unique avec un rapport liquide-solide de 2 l/kg et une granularité inférieure à 4 mm (sans ou avec réduction de la granularité). NF EN 12457-1 (2002)
177.
AFNOR: Caractérisation des déchets - Lixiviation - essai de conformité pour lixiviation des déchets fragmentés et des boues - Partie 2: Essai en bâchée unique avec un rapport L/S de 10L/kg et une granularité inférieure à 4 mm (sans ou avec réduction de la granularité). NF EN 12457-2 (2002)
178.
AFNOR: Caractérisation des déchets - Lixiviation - Essai de conformité pour lixiviation des déchets fragmentés et des boues - Partie 3: essai en bâchée double avec un rapport liquide-solide de 2 l/kg et de 8 l/kg pour des matériaux à forte teneur en solides et une granularité inférieure à 4 mm (sans ou avec réduction de la granularité). NF EN 12457-3 (2002)
179.
AFNOR: Caractérisation des déchets - Lixiviation - Essai de conformité pour lixiviation des déchets fragmentés et des boues - Partie 4: essai en bâchée unique avec un rapport liquide/solide de 10 l/kg et une granularité inférieure à 10 mm (sans ou avec réduction de la granularité). NF EN 12457-4 (2002)
180.
AFNOR: Déchets – Essai de lixiviation d’un déchet solide initialement massif ou généré par un procédé de solidification. NF X 31-211 (2012)
181.
US EPA: Method 1311. Toxicity Characteristic Leaching Procedure, SW-846: Test Methods for Evaluating Solid Waste—Physical/Chemical Methods (1994)
182.
AFNOR: Caractérisation des déchets - Essai de lixiviation de conformité - Essai de lixiviation en bâchée unique pour des monolithes avec un rapport liquide/ surface (L/A) fixe, pour des prises d’essai de dimensions minimales fixes. XP CEN/TS 15862 (2012)
183.
184.
van der Sloot, H.A., Heasman, L., Quevauviller, Ph.: Harmonization of leaching/extraction tests. Stud. Environ. Sci. 70 (1997)
185.
186.
Tiwari, M.K., Bajpai, S., Dewangan, U.K., Tamrakar, R.K.: Suitability of leaching test methods for fly ash ans slag: a review. J. Radiat. Res. Appl. Sci. 8, 523–537 (2015)CrossRef
187.
188.
Waste Extraction Test, California Code Regulations, Sections 208 and 25141, Health and Safety Code
189.
AFNOR: Qualité du sol - Modes opératoires de lixiviation en vue d’essais chimiques et écotoxicologiques ultérieurs des sols et matériaux du sol - Partie 4: essai de dépendance au pH avec ajout initial d’acide/base. XP CEN ISO/TS 21268-4 (2009)
190.
US EPA: Method 1313. Liquid-solid partitioning as a function of extract pH using parallel batch extraction procedure, revision (2017)
191.
AFNOR: Qualité du sol - Modes opératoires de lixiviation en vue d’essais chimiques et écotoxicologiques ultérieurs des sols et matériaux du sol - Partie 3: Essai de percolation à écoulement ascendant. XP CEN ISO/TS 21268-3 (2009)
192.
ASTM: Standard test method for leaching solid material in a column apparatus. ASTM D4874-95 (2001)
193.
van der Sloot, H.A.: Harmonisation of leaching/extraction procedures for sludge, compost, soil and sediment analyses. In: Quevauviller, P. (ed) Methodologies for Soil and Sediment Fractionation Studies, pp. 142–170. Royal Society of Chemistry, Cambridge (2002)
194.
Commission, European: Technical Work in Support of the Network “Harmonisation of Leaching/Extraction Tests”, Contract SMT4-CT96-2066. European Commission, Brussels (2004)
195.
Gupta, S.K., Vollmer, M.K., Krebs, R.: The importance of mobile, mobilisable and pseudo total heavy metal fractions in soil for three-level risk assessment ans risk management. Sci. Total Environ. 178, 11–20 (1996)CrossRef
196.
197.
Kosson, D.S., van der Sloot, H.A., Sanchez, F., Garrabrants, A.C.: An integrated framework for evaluating leaching in waste management and utilization of secondary materials. Environ. Eng. Sci. 19, 159–204 (2002)CrossRef
198.
Hjelmar, O.: Leachate from land disposal of coal fly-ash. Waste Manage. Res. 8, 429–449 (1990)CrossRef
199.
Tribout, C.: Valorisation de sédiments traités en techniques routières: contribution à la mise en place d’un protocole d’acceptabilité, PhD Thesis, Université de Toulouse (2010). (in French)
200.
AFNOR: Soil Quality—Guidance on Leaching Procedures for Subsequent Chemical and Ecotoxicological Testing of Soils and Soil Materials. NF EN ISO 18772 (2014)
201.
Garrabrants A.C.: Development and Application of Fundamental Leaching Property Protocols for Evaluating Inorganic Release from Wastes and Soil, Master Thesis, The State University of New Jersey (1998)
202.
Meza, S.L., Kalbe, U., Berger, W., Simon, F.-G.: Effect of contact time on the release of contaminants from granular waste materials during column leaching experiments. Waste Manage. 30, 565–571 (2010)CrossRef
203.
van der Sloot, H.A.: Developments in evaluating environmental impact from utilization of bulk inert wastes using laboratory leaching tests and field verification. Waste Manage. 16(1–3), 65–81 (1996)
204.
van der Sloot, H.A., Hoede, D., Cresswell, D.J.F., Barton, J.R.: Leaching behaviour of synthetic aggregates. Waste Manage. 21, 221–228 (2001)CrossRef
205.
206.
Quevauviller, P., van der Sloot, H.A., Urec, A., Muntaud, H., Gomeze, A., Rauret, G.: Conclusions of the workshop: harmonization of leaching/extraction tests for environmental risk assessment. Sci. Total Environ. 178, 133–139 (1996)CrossRef
207.
Tribout, C., Husson, B., Nzihou, A.: Use of treated dredged sediments as road base materials: environmental assessment. Waste Biomass Valorization 2(3), 337–346 (2011)CrossRef
208.
Fang, W., Wei, Y., Liu, J.: Comparative characterization of sewage sludge compost and soil: heavy metal leaching characteristics. J. Hazard. Mater. 310, 1–10 (2016)CrossRef
209.
Kribi, S.: Décomposition des matières organiques et stabilisation des métaux lourds dans les sédiments de dragage, PhD Thesis, Institut National des Sciences Appliquées Lyon (2005). (in French)
210.
Dia, M.: Traitement et valorisation de sédiments de dragage phosphatés en technique routière, PhD Thesis, Ecole des Mines de Douai & Université d’Artois (2013). (in French)
211.
Theodoratos, P., Papassiopi, N., Xenidis, A.: Evaluation of monobasic calcium phosphate for the immobilization of heavy metals in contaminated soils from Lavrion. J. Hazard. Mater. 94(2), 135–146 (2002)CrossRef
212.
RECORD: Impacts écologiques de sédiments pollués extraits et déposés en milieux terrestres. Etat des connaissances et évaluation des risques pour les écosystèmes. RECORD, n°14-1023/1A (2017). (in French)
213.
214.
van der Sloot, H.A., van Zomeren, A., Meeussen, J.C.L., Seignette, P., Bleijerveld, R.: Test method selection, validation against field data, and predictive modelling for impact evaluation of stabilised waste disposal. J. Hazard. Mater. 141(2), 354–369 (2007)CrossRef
215.
van der Sloot, H.A., Kosson, D.S.: Use of characterisation leaching tests and associated modelling tools in assessing the hazardous nature of wastes. J. Hazard. Mater. 207, 36–43 (2012)CrossRef
Metadata
Title
Sludge
Authors
Patricia Arlabosse
Ange Nzihou
Stewart Oakley
Martial Sauceau
Christelle Tribout
Fei Wang
Yaqian Zhao
Copyright Year
2020
Book
Handbook on Characterization of Biomass, Biowaste and Related By-products

Print ISBN: 978-3-030-35019-2

Electronic ISBN: 978-3-030-35020-8

Copyright Year: 2020

DOI
https://doi.org/10.1007/978-3-030-35020-8_9

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