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Published in: Journal of Materials Science 21/2015

01-11-2015 | Original Paper

Stress corrosion and droplets formation in calcium phosphate and calcium alumino-phosphate glasses

Authors: Stephanie Etter, Annelise Faivre, Pierre Solignac, Sébastien Clément, Jean-Marc Fromental, Laurent Duffour, Florence Despetis

Published in: Journal of Materials Science | Issue 21/2015

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Abstract

Subcritical crack growth and crack closure are analysed using the double cleavage drilled compression method, in two calcium phosphate-based glasses. The measurements of the crack velocity as a function of temperature, from ambient to 250 °C, are reported for two different relative humidity levels. Studied glasses present unusual trends characterized by a non-gradual shift of VK I curves versus temperature. Moreover, when the load is released and crack closes, expulsion of a “liquid-like” phase is observed forming droplets along the crack path. These droplets are only formed at certain temperatures, but both under high and low water humidity. They evolve towards residues when temperature is decreased.

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Metadata
Title
Stress corrosion and droplets formation in calcium phosphate and calcium alumino-phosphate glasses
Authors
Stephanie Etter
Annelise Faivre
Pierre Solignac
Sébastien Clément
Jean-Marc Fromental
Laurent Duffour
Florence Despetis
Publication date
01-11-2015
Publisher
Springer US
Published in
Journal of Materials Science / Issue 21/2015
Print ISSN: 0022-2461
Electronic ISSN: 1573-4803
DOI
https://doi.org/10.1007/s10853-015-9253-0

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