Top

Journal of Sol-Gel Science and Technology

Published in:

01-09-2011 | Original Paper

Synthesis and characterization of titania/MQ silicone resin hybrid nanocomposite via sol–gel process

Authors: Hongping Xiang, Jianfeng Ge, Shaohui Cheng, Hongmei Han, Shaowei Cui

Published in: Journal of Sol-Gel Science and Technology | Issue 3/2011

Activate our intelligent search to find suitable subject content or patents.

search-config

AI-assisted search

Off

Abstract

Inorganic–organic hybrid materials were prepared via an aqueous sol–gel technique from tetra-n-butyl titanate as the precursor of titania, in the presence of MQ silicone resin. The samples were characterized by FT–IR, UV–Vis, DSC, TGA, SEM and XRD. It was illustrated that the Ti–O–Si covalent bonds had formed in the hybrid nanocomposite which were highly transparent in visible light region, and yet had high absorption in UV light range. The thermal stability of the hybrid materials was gradually improved with the increase of titania content. It was concluded that the hybrid material which particle size was around 50 nm were amorphous when the crystallization of titania was retarded by MQ silicone resin.

previous article Synthesis, structural and transport properties of Li-doped molybdenum and vanadium oxide nanocrystalline films

next article Optimization of process variables and corrosion properties of a multi layer silica sol gel coating on AZ91D using the Box–Behnken design

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

über 67.000 Bücher
über 390 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Maschinenbau + Werkstoffe

Jetzt Wissensvorsprung sichern!

inform now

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

über 102.000 Bücher
über 537 Zeitschriften

aus folgenden Fachgebieten:

Automobil + Motoren
Bauwesen + Immobilien
Business IT + Informatik
Elektrotechnik + Elektronik
Energie + Nachhaltigkeit
Finance + Banking
Management + Führung
Marketing + Vertrieb
Maschinenbau + Werkstoffe
Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

inform now

Martinelli M, Luca MA, Bechli DM (2009) Sol–Gel Sci Technol 52:202–209CrossRef

Han ZY, Zhang JC, Yang XY (2011) Polym Lett 5(5):401–408CrossRef

Rubio F, Rubio J, Oteo JL (2000) Sol–Gel Sci Technol 18:105–113CrossRef

Chen Q, Kamitakahara M, Miyata N (2000) Sol–Gel Sci Technol 19:101–105CrossRef

Wei Q, Yu L, Mather RR (2007) Mater Sci 42(19):8001–8005CrossRef

Muller CA, Schneider M, Gisler A (2000) Catal Lett 64(1):9–14CrossRef

Yang QQ, Zhao JF, Li QF (2004) Eng Plas Appl 32(4):71–72

Irena M, Abdurauf P, Toma G (2006) Chem Technol Macedonia 25(1):45–50

Szymom G, Antoni T, Janusz B (2010) the 18th International of Vacuum Congress, Beijing

10.

Yoshinori K, Atsunori M, Masahiro T (2000) Sol–Gel Sci Technol 19:585–588CrossRef

11.

Altıntas Z, Cakmakc E, Kahraman MV (2011) Sol–Gel Sci Technol 58:1–7CrossRef

12.

Di MW, He SY, Li QR (2006) Nucl Inst Meth Phys Res B 248(1):31–36CrossRef

13.

Weidner R, Mautner K, Mautner R (1994) USP: 5548053

14.

Burkus FS, Rub IS, Gul IJ (1999) USP: 6262188

15.

Charles R, Janine C, Kozubal CL (2001) USP: 6287546

16.

Kirubaharan AM, Selvaraj M, Maruthan K (2009) Coat Technol Res 4:139–150

17.

Cannon AS, Morelli A, Pressler W (2005) Sol–Gel Sci Technol 36:157–162CrossRef

18.

Nishide T, Sato M, Hara H (2000) Mater Sci 35(2):465–469CrossRef

19.

Daoud WA, Xin JH (2004) Sol–Gel Sci Technol 29:25–29CrossRef

20.

Luo XS, Zha CJ, Davie BL (2004) Sol–Gel Sci Technol 32:297–301CrossRef

21.

Du WC, Wang HT, Zhong W (2005) Sol–Gel Sci Technol 34:227–231CrossRef

22.

Nakayama N, Hayas T (2007) Appl Polym Sci 105(6):3662–3672CrossRef

23.

Chen Q, Miyaji F, Kokubo T (1999) Biomaterials 20(12):1127–1132CrossRef

24.

Liu YF, Lü CL, Li MJ (2008) Coll Surf A: Physicochem 328(1–3):67–72CrossRef

25.

Huang W, Huang Y, Yu YZ (1998) Appl Polym Sci 70:1753–1757CrossRef

26.

Li SD, Ge JF, Pu X, Guo ZJ, Zhang TF (2009) Chem Indu Guangdong 36(2):35–38

27.

Smitha VS, Manjumol KA, Baiju KV (2010) Sol–Gel Sci Technol 54:203–211CrossRef

28.

Yu J, Feng Z, Xu L (2001) Chem Mater 13(3):994–998CrossRef

29.

Kalele S, Dey R, Hebalkar N (2005) Phys Indian 65(5):787–794

30.

Que W, Zhou Y, Lam YL (2000) Thin Solid Films 358(1–2):16–21CrossRef

31.

Ge JF, Pu X, Li SD (2010) Zhongkai Univ Agri Eng Lett China 23:35–38

32.

Seco AM, Goncalves MC, Almeida RM (2000) Mater Sci Eng B 76:193–199CrossRef

Title: Synthesis and characterization of titania/MQ silicone resin hybrid nanocomposite via sol–gel process
Authors: Hongping Xiang
Jianfeng Ge
Shaohui Cheng
Hongmei Han
Shaowei Cui
Publication date: 01-09-2011
Publisher: Springer US
Published in: Journal of Sol-Gel Science and Technology / Issue 3/2011
Print ISSN: 0928-0707
Electronic ISSN: 1573-4846
DOI: https://doi.org/10.1007/s10971-011-2538-0

Springer Professional

Abstract

Please log in to get access to your license.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Technik"

Springer Professional "Wirtschaft+Technik"

Other articles of this Issue 3/2011

Recent insights into xerogel and aerogel mineral composites for CO2 mineral sequestration

Optimization of process variables and corrosion properties of a multi layer silica sol gel coating on AZ91D using the Box–Behnken design

Synthesis and microwave dielectric properties of Ca0.6La0.267TiO3 nanocrystalline powders by sol–gel method

Influence of pH on the incorporation and growth of Pb2CrO5 crystallites in silica matrix

Manufacturing of ceramic nanomaterials in Ti–Si–C–N system by sol–gel method

Preparation of Li9Cr3(P2O7)3(PO4)2 as cathode material for lithium ion batteries through sol–gel method

Premium Partners