Skip to main content
Top
Published in: Rare Metals 11/2016

01-11-2016

Synthesis of magnetic carrier sub-microparticles with high stability through carbon reduction and solation coating methods

Authors: Qiang Zhang, Li-Bo Gao, Jun-Yang Li, Ze-Bin Guo, Zhen-Yin Hai, Yan-Ting Xing, Chen-Yang Xue

Published in: Rare Metals | Issue 11/2016

Log in

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

This paper presents a novel approach in synthesizing SiO2–Fe3O4 magnetic carrier with high stability. The Fe3O4 magnetic powders were synthesized via one-step method named carbon reduction method. The advantages of the methods are of simple process, none lead-in pollution agent, low cost and adaptation to large-lot production. The stability of the magnetic powders is improved through modifying the Fe3O4 with SiO2 in solation method. The results of the characterizations show that the superparamagnetic SiO2–Fe3O4 sub-microparticles (~600 nm) with saturation intensity of 36.4 mA·m2·g−1 are obtained successfully. Moreover, the quantitating, repeatability and high stability of the carbon reduction method are demonstrated as well.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literature
[1]
go back to reference Salerno M, Diaspro A, Cingolani R, Athanassiou A. Magnetic force microscopy and energy loss imaging of superparamagnetic iron oxide nanoparticles. Sci Rep. 2011;202:1. Salerno M, Diaspro A, Cingolani R, Athanassiou A. Magnetic force microscopy and energy loss imaging of superparamagnetic iron oxide nanoparticles. Sci Rep. 2011;202:1.
[2]
go back to reference Pan T, Zhu J, Su H, Yang CF. Ni segregation and thermal stability of reversed austenite in a Fe–Ni alloy processed by QLT heat treatment. Rare Met. 2015;34(11):776.CrossRef Pan T, Zhu J, Su H, Yang CF. Ni segregation and thermal stability of reversed austenite in a Fe–Ni alloy processed by QLT heat treatment. Rare Met. 2015;34(11):776.CrossRef
[3]
go back to reference He L, Tan YF, Wang XL, Jing QF, Hong X. Tribological properties of laser cladding TiB2 particles reinforced Ni-base alloy composite coatings on aluminum alloy. Rare Met. 2014;34(11):1. He L, Tan YF, Wang XL, Jing QF, Hong X. Tribological properties of laser cladding TiB2 particles reinforced Ni-base alloy composite coatings on aluminum alloy. Rare Met. 2014;34(11):1.
[4]
go back to reference El-Ton AM, Khan A, Labis JP, Ibrahim MA, Al-hoshan M. Synthesis of magnetic core–mesoporous silica shell nanoparticles using anionic surfactant and their application for ketoprofen control release. Chem Lett. 2012;41(10):1357.CrossRef El-Ton AM, Khan A, Labis JP, Ibrahim MA, Al-hoshan M. Synthesis of magnetic core–mesoporous silica shell nanoparticles using anionic surfactant and their application for ketoprofen control release. Chem Lett. 2012;41(10):1357.CrossRef
[5]
go back to reference Chen F, Xie S, Zhang J, Liu R. Synthesis of spherical Fe3O4 magnetic nanoparticles by co-precipitation in choline chloride/urea deep eutectic solvent. Mater Lett. 2013;112:177.CrossRef Chen F, Xie S, Zhang J, Liu R. Synthesis of spherical Fe3O4 magnetic nanoparticles by co-precipitation in choline chloride/urea deep eutectic solvent. Mater Lett. 2013;112:177.CrossRef
[6]
go back to reference Wang C, Wei YJ, Jiang HY, Sun SH. Tug-of-war in nanoparticles: competitive growth of Au on Au–Fe3O4 nanoparticles. Nano Lett. 2009;9(12):4544.CrossRef Wang C, Wei YJ, Jiang HY, Sun SH. Tug-of-war in nanoparticles: competitive growth of Au on Au–Fe3O4 nanoparticles. Nano Lett. 2009;9(12):4544.CrossRef
[7]
go back to reference Yang C, Wu J, Hou YL. Fe3O4 nanostructure: synthesis, growth mechanism, properties and applications. Chem Commun. 2011;47(18):5130.CrossRef Yang C, Wu J, Hou YL. Fe3O4 nanostructure: synthesis, growth mechanism, properties and applications. Chem Commun. 2011;47(18):5130.CrossRef
[8]
go back to reference Mira J, López-Pérez JA, López-Quintela MA, Rivas J. Magnetic iron oxide nanoparticles synthesized via microemulsions. Mater Sci Forum. 1996;235:297. Mira J, López-Pérez JA, López-Quintela MA, Rivas J. Magnetic iron oxide nanoparticles synthesized via microemulsions. Mater Sci Forum. 1996;235:297.
[9]
go back to reference Zhou ZH, Wang J, Liu X, Chan HSO. Synthesis of Fe3O4 nanoparticles from emulsions. J Mater Chem. 2001;11(6):1704.CrossRef Zhou ZH, Wang J, Liu X, Chan HSO. Synthesis of Fe3O4 nanoparticles from emulsions. J Mater Chem. 2001;11(6):1704.CrossRef
[10]
go back to reference Massart R. Preparation of magnetite nanoparticles. IEEE Trans Magn. 1981;17(1):247. Massart R. Preparation of magnetite nanoparticles. IEEE Trans Magn. 1981;17(1):247.
[11]
go back to reference Shen L, Laibinis PE, Hatton TA. Bilayer surfactant stabilized magnetic fluids. Synth Interact Interfaces Langmuir. 1999;15(2):447. Shen L, Laibinis PE, Hatton TA. Bilayer surfactant stabilized magnetic fluids. Synth Interact Interfaces Langmuir. 1999;15(2):447.
[12]
go back to reference Fang LM, Zu XT, Li ZJ, Zhu S, Liu CM, Zhou WL, Wang LM. Synthesis and characteristics of Fe3+-doped SnO2 nanoparticles via sol–gel-calcination or sol–gel-hydrothermal route. J Alloys Compd. 2008;454(1):261.CrossRef Fang LM, Zu XT, Li ZJ, Zhu S, Liu CM, Zhou WL, Wang LM. Synthesis and characteristics of Fe3+-doped SnO2 nanoparticles via sol–gel-calcination or sol–gel-hydrothermal route. J Alloys Compd. 2008;454(1):261.CrossRef
[13]
go back to reference Lee HS, Kim EH, Shao H, Kwak BK. Synthesis of SPIO-chitosan microspheres for MRI-detectable embolotherapy. J Magn Magn Mater. 2005;293(1):102.CrossRef Lee HS, Kim EH, Shao H, Kwak BK. Synthesis of SPIO-chitosan microspheres for MRI-detectable embolotherapy. J Magn Magn Mater. 2005;293(1):102.CrossRef
[14]
go back to reference Oliveira LC, Rios RV, Fabris JD, Garg V, Sapag K, Lago RM. Activated carbon/iron oxide magnetic composites for the adsorption of contaminants in water. Carbon. 2002;40(12):2177.CrossRef Oliveira LC, Rios RV, Fabris JD, Garg V, Sapag K, Lago RM. Activated carbon/iron oxide magnetic composites for the adsorption of contaminants in water. Carbon. 2002;40(12):2177.CrossRef
[15]
go back to reference Vong MSW, Bazin N, Sermon PA. Chemical modification of silica gels. Sol–Gel Sci Technol. 1997;8(1–3):499. Vong MSW, Bazin N, Sermon PA. Chemical modification of silica gels. Sol–Gel Sci Technol. 1997;8(1–3):499.
[16]
go back to reference Bumb A, Brechbiel MW, Choyke PL, Fugger L, Eggeman A, Prabhakaran D, Hutchinson J, Dobson PJ. Synthesis and characterization of ultra-small super paramagnetic iron oxide nanoparticles thinly coated with silica. Nanotechnology. 2008;19(33):335601.CrossRef Bumb A, Brechbiel MW, Choyke PL, Fugger L, Eggeman A, Prabhakaran D, Hutchinson J, Dobson PJ. Synthesis and characterization of ultra-small super paramagnetic iron oxide nanoparticles thinly coated with silica. Nanotechnology. 2008;19(33):335601.CrossRef
[17]
go back to reference Selvan S, Patra PK, Ang CY, Ying JY. Synthesis of silica-coated semiconductor and magnetic quantum dot sand their use in the imaging of live cells. Angew Chem. 2007;119(14):2500.CrossRef Selvan S, Patra PK, Ang CY, Ying JY. Synthesis of silica-coated semiconductor and magnetic quantum dot sand their use in the imaging of live cells. Angew Chem. 2007;119(14):2500.CrossRef
[18]
go back to reference Xiang J, Lu W, Hu YJ, Wu Y, Yan H, Lieber CM. Ge/Si nanowire heterostructures as high-performance field-effect transistors. Nature. 2006;441(7092):489.CrossRef Xiang J, Lu W, Hu YJ, Wu Y, Yan H, Lieber CM. Ge/Si nanowire heterostructures as high-performance field-effect transistors. Nature. 2006;441(7092):489.CrossRef
[19]
go back to reference Yang RG, Chen G, Dresselhaus MS. Thermal conductivity modeling of core–shell and tubular nanowires. Nano Lett. 2005;5(6):1111.CrossRef Yang RG, Chen G, Dresselhaus MS. Thermal conductivity modeling of core–shell and tubular nanowires. Nano Lett. 2005;5(6):1111.CrossRef
Metadata
Title
Synthesis of magnetic carrier sub-microparticles with high stability through carbon reduction and solation coating methods
Authors
Qiang Zhang
Li-Bo Gao
Jun-Yang Li
Ze-Bin Guo
Zhen-Yin Hai
Yan-Ting Xing
Chen-Yang Xue
Publication date
01-11-2016
Publisher
Nonferrous Metals Society of China
Published in
Rare Metals / Issue 11/2016
Print ISSN: 1001-0521
Electronic ISSN: 1867-7185
DOI
https://doi.org/10.1007/s12598-015-0662-7

Other articles of this Issue 11/2016

Rare Metals 11/2016 Go to the issue

Premium Partners