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Published in: Applied Composite Materials 4/2016

01-08-2016

Tension-Compression Fatigue of a Nextel™720/alumina Composite at 1200 °C in Air and in Steam

Authors: R. L. Lanser, M. B. Ruggles-Wrenn

Published in: Applied Composite Materials | Issue 4/2016

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Abstract

Tension-compression fatigue behavior of an oxide-oxide ceramic-matrix composite was investigated at 1200 °C in air and in steam. The composite is comprised of an alumina matrix reinforced with Nextel™720 alumina-mullite fibers woven in an eight harness satin weave (8HSW). The composite has no interface between the fiber and matrix, and relies on the porous matrix for flaw tolerance. Tension-compression fatigue behavior was studied for cyclical stresses ranging from 60 to 120 MPa at a frequency of 1.0 Hz. The R ratio (minimum stress to maximum stress) was −1.0. Fatigue run-out was defined as 105 cycles and was achieved at 80 MPa in air and at 70 MPa in steam. Steam reduced cyclic lives by an order of magnitude. Specimens that achieved fatigue run-out were subjected to tensile tests to failure to characterize the retained tensile properties. Specimens subjected to prior cyclic loading in air retained 100 % of their tensile strength. The steam environment severely degraded tensile properties. Tension-compression cyclic loading was considerably more damaging than tension-tension cyclic loading. Composite microstructure, as well as damage and failure mechanisms were investigated.

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Literature
1.
go back to reference Szweda, A., Millard, M.L., Harrison, M.G.: Fiber reinforced ceramic composite member and method for making. U. S. Pat 5, 601–674 (1997) Szweda, A., Millard, M.L., Harrison, M.G.: Fiber reinforced ceramic composite member and method for making. U. S. Pat 5, 601–674 (1997)
2.
go back to reference Zok, F.W.: Developments in oxide fiber composites. J. Am. Ceram. Soc. 89, 3309–3324 (2006)CrossRef Zok, F.W.: Developments in oxide fiber composites. J. Am. Ceram. Soc. 89, 3309–3324 (2006)CrossRef
3.
go back to reference Kerans, R.J., Hay, R.S., Parthasarathy, T.A., Cinibulk, M.K.: Interface design for oxidation resistant ceramic composites. J. Am. Ceram. Soc. 85, 2599–2632 (2002)CrossRef Kerans, R.J., Hay, R.S., Parthasarathy, T.A., Cinibulk, M.K.: Interface design for oxidation resistant ceramic composites. J. Am. Ceram. Soc. 85, 2599–2632 (2002)CrossRef
4.
go back to reference Kanka, B., Schneider, H.: Aluminosilicate fiber/mullite matrix composites with favorable high-temperature properties. J. Eur. Ceram. Soc. 20, 619–623 (2000)CrossRef Kanka, B., Schneider, H.: Aluminosilicate fiber/mullite matrix composites with favorable high-temperature properties. J. Eur. Ceram. Soc. 20, 619–623 (2000)CrossRef
5.
go back to reference Mattoni, M.A., Yang, J.Y., Levi, C.G., Zok, F.W., Zawada, L.P.: Effects of combustor rig exposure on a porous-matrix oxide composite. Int. J. Appl. Ceram. Technol. 2, 133–140 (2005)CrossRef Mattoni, M.A., Yang, J.Y., Levi, C.G., Zok, F.W., Zawada, L.P.: Effects of combustor rig exposure on a porous-matrix oxide composite. Int. J. Appl. Ceram. Technol. 2, 133–140 (2005)CrossRef
6.
go back to reference Carelli, E.A.V., Fujita, H., Yang, J.Y., Zok, F.W.: Effects of thermal aging on the mechanical properties of a porous-matrix composite. J. Am. Ceram. Soc. 85, 595–602 (2002)CrossRef Carelli, E.A.V., Fujita, H., Yang, J.Y., Zok, F.W.: Effects of thermal aging on the mechanical properties of a porous-matrix composite. J. Am. Ceram. Soc. 85, 595–602 (2002)CrossRef
7.
go back to reference Keller, K.A., Mah, T., Parthasarathy, T.A., Boakye, E.E., Mogilevsky, P., Cinibulk, M.K.: Effectiveness of monazite coatings in oxide/oxide composites after long term exposure at high temperature. J. Am. Ceram. Soc. 86, 325–332 (2003)CrossRef Keller, K.A., Mah, T., Parthasarathy, T.A., Boakye, E.E., Mogilevsky, P., Cinibulk, M.K.: Effectiveness of monazite coatings in oxide/oxide composites after long term exposure at high temperature. J. Am. Ceram. Soc. 86, 325–332 (2003)CrossRef
8.
go back to reference Hackemann, S., Flucht, F., Braue, W.: Creep investigations of alumina- based all-oxide ceramic matrix composites. Composites A 41, 768–1776 (2010)CrossRef Hackemann, S., Flucht, F., Braue, W.: Creep investigations of alumina- based all-oxide ceramic matrix composites. Composites A 41, 768–1776 (2010)CrossRef
9.
go back to reference Zawada, L.P., Hay, R.S., Staehler, J., Lee, S.S.: Characterization and high temperature mechanical behavior of an oxide/oxide composite. J. Am. Ceram. Soc. 86, 981–990 (2003)CrossRef Zawada, L.P., Hay, R.S., Staehler, J., Lee, S.S.: Characterization and high temperature mechanical behavior of an oxide/oxide composite. J. Am. Ceram. Soc. 86, 981–990 (2003)CrossRef
10.
go back to reference Mehrman, J.M., Ruggles-Wrenn, M.B., Baek, S.S.: Influence of hold times on the elevated-temperature fatigue behavior of an oxide-oxide ceramic composite in air and in steam. Compos. Sci. Technol. 67, 1425–1438 (2007)CrossRef Mehrman, J.M., Ruggles-Wrenn, M.B., Baek, S.S.: Influence of hold times on the elevated-temperature fatigue behavior of an oxide-oxide ceramic composite in air and in steam. Compos. Sci. Technol. 67, 1425–1438 (2007)CrossRef
11.
go back to reference Ruggles-Wrenn, M., Braun, J.: Effects of steam environment on creep behavior of Nextel™720 alumina ceramic composite at elevated temperature. Mater. Sci. Eng. A 497, 101–110 (2008)CrossRef Ruggles-Wrenn, M., Braun, J.: Effects of steam environment on creep behavior of Nextel™720 alumina ceramic composite at elevated temperature. Mater. Sci. Eng. A 497, 101–110 (2008)CrossRef
12.
go back to reference Ruggles-Wrenn, M.B., Genelin, C.L.: Creep of Nextel™720/alumina-mullite ceramic composite at 1200°C in air, argon, and steam. Compos. Sci. Technol. 69, 663–669 (2009)CrossRef Ruggles-Wrenn, M.B., Genelin, C.L.: Creep of Nextel™720/alumina-mullite ceramic composite at 1200°C in air, argon, and steam. Compos. Sci. Technol. 69, 663–669 (2009)CrossRef
13.
go back to reference Ruggles-Wrenn, M.B., Koutsoukos, P., Baek, S.S.: Effects of environment on creep behavior of two oxide/oxide ceramic-matrix composites at 1200°C. J. Mater. Sci. 43, 6734–6746 (2008)CrossRef Ruggles-Wrenn, M.B., Koutsoukos, P., Baek, S.S.: Effects of environment on creep behavior of two oxide/oxide ceramic-matrix composites at 1200°C. J. Mater. Sci. 43, 6734–6746 (2008)CrossRef
14.
go back to reference Ruggles-Wrenn, M.B., Kutsal, T.: Effects of steam environment on creep behavior of Nextel™720/alumina-mullite ceramic composite at elevated temperature. Composites A 41, 1807–1816 (2010)CrossRef Ruggles-Wrenn, M.B., Kutsal, T.: Effects of steam environment on creep behavior of Nextel™720/alumina-mullite ceramic composite at elevated temperature. Composites A 41, 1807–1816 (2010)CrossRef
15.
go back to reference Ruggles-Wrenn, M.B., Ozer, M.: Creep behavior of Nextel™720/alumina-mullite ceramic composite with +/−45 fiber orientation at 1200°C. Mater. Sci. Eng. A 527, 5326–5334 (2010)CrossRef Ruggles-Wrenn, M.B., Ozer, M.: Creep behavior of Nextel™720/alumina-mullite ceramic composite with +/−45 fiber orientation at 1200°C. Mater. Sci. Eng. A 527, 5326–5334 (2010)CrossRef
16.
go back to reference Ruggles-Wrenn, M.B., Siegert, G.T., Back, S.S.: Creep behavior of Nextel™720/alumina ceramic composite with +/−45 fiber orientation at 1200°C. Compos. Sci. Technol. 68, 1588–1595 (2008)CrossRef Ruggles-Wrenn, M.B., Siegert, G.T., Back, S.S.: Creep behavior of Nextel™720/alumina ceramic composite with +/−45 fiber orientation at 1200°C. Compos. Sci. Technol. 68, 1588–1595 (2008)CrossRef
17.
go back to reference Ruggles-Wrenn, M.B., Szymczak, N.R.: Effects of steam environment on compressive creep behavior of Nextel™720/alumina ceramic composite at 1200°C. Composites A 39, 1829–1837 (2008)CrossRef Ruggles-Wrenn, M.B., Szymczak, N.R.: Effects of steam environment on compressive creep behavior of Nextel™720/alumina ceramic composite at 1200°C. Composites A 39, 1829–1837 (2008)CrossRef
18.
go back to reference Ruggles-Wrenn, M.B., Hetrick, G., Baek, S.S.: Effects of frequency and environment on fatigue behavior of an oxide-oxide ceramic composite at 1200°C. Int. J. Fatig. 30, 502–516 (2008)CrossRef Ruggles-Wrenn, M.B., Hetrick, G., Baek, S.S.: Effects of frequency and environment on fatigue behavior of an oxide-oxide ceramic composite at 1200°C. Int. J. Fatig. 30, 502–516 (2008)CrossRef
19.
go back to reference Armani, C.J., Ruggles-Wrenn, M.B., Hay, R.S., Fair, G.E.: Creep and microstructure of Nextel™ 720 fiber at elevated temperature in air and in steam. Acta Mater. 61, 6114–6124 (2013)CrossRef Armani, C.J., Ruggles-Wrenn, M.B., Hay, R.S., Fair, G.E.: Creep and microstructure of Nextel™ 720 fiber at elevated temperature in air and in steam. Acta Mater. 61, 6114–6124 (2013)CrossRef
20.
go back to reference Armani, C.J., Ruggles-Wrenn, M.B., Fair, G.E., Hay, R.S.: Creep of Nextel™ 610 fiber at 1100°C in air and steam. Int. J. Appl. Ceram. Technol. 10, 276–84 (2013)CrossRef Armani, C.J., Ruggles-Wrenn, M.B., Fair, G.E., Hay, R.S.: Creep of Nextel™ 610 fiber at 1100°C in air and steam. Int. J. Appl. Ceram. Technol. 10, 276–84 (2013)CrossRef
21.
go back to reference Hay, R.S., Armani, C.J., Ruggles-Wrenn, M.B., Fair, G.E.: Creep and microstructure evolution of Nextel™ 610 fiber in air and steam. J. Eur. Ceram. Soc. 34, 2413–2426 (2014)CrossRef Hay, R.S., Armani, C.J., Ruggles-Wrenn, M.B., Fair, G.E.: Creep and microstructure evolution of Nextel™ 610 fiber in air and steam. J. Eur. Ceram. Soc. 34, 2413–2426 (2014)CrossRef
22.
go back to reference Volkmann, E., Tushtev, K., Koch, D., Wilhelmi, C., Grathwohl, G., Rezwan, K.: Influence of fiber orientation and matrix processing on the tensile and creep performance of Nextel 610 reinforced polymer derived ceramic matrix composites. Mater. Sci. Eng. A 614, 171–179 (2014)CrossRef Volkmann, E., Tushtev, K., Koch, D., Wilhelmi, C., Grathwohl, G., Rezwan, K.: Influence of fiber orientation and matrix processing on the tensile and creep performance of Nextel 610 reinforced polymer derived ceramic matrix composites. Mater. Sci. Eng. A 614, 171–179 (2014)CrossRef
23.
go back to reference Volkmann, E., Dentel, A., Tushtev, K., Wilhelmi, C., Rezwan, K.: Influence of heat treatment and fiber orientation on the damage threshold and the fracture behavior of Nextel fiber-reinforced mullite-SiOC matrix composites analyzed by acoustic emission monitoring. J. Mater. Sci. 49, 7890–7899 (2014)CrossRef Volkmann, E., Dentel, A., Tushtev, K., Wilhelmi, C., Rezwan, K.: Influence of heat treatment and fiber orientation on the damage threshold and the fracture behavior of Nextel fiber-reinforced mullite-SiOC matrix composites analyzed by acoustic emission monitoring. J. Mater. Sci. 49, 7890–7899 (2014)CrossRef
24.
go back to reference Volkmann, E., Lima Evangelista, L., Tushtev, K., Koch, D., Wilhelmi, C., Rezwan, K.: Oxidation-induced microstructural changes of a polymer derived Nextel™ 610 ceramic composite and impact on the mechanical performance. J. Mater. Sci. 49, 710–719 (2014)CrossRef Volkmann, E., Lima Evangelista, L., Tushtev, K., Koch, D., Wilhelmi, C., Rezwan, K.: Oxidation-induced microstructural changes of a polymer derived Nextel™ 610 ceramic composite and impact on the mechanical performance. J. Mater. Sci. 49, 710–719 (2014)CrossRef
25.
go back to reference Lee, S., Zawada, L., Staehler, J., Folsom, C.: Mechanical behavior and high-temperature performance of a woven NicalonTM/Si-N-C ceramic-matrix composite. J. Am. Ceram. Soc. 81, 1797–811 (1998)CrossRef Lee, S., Zawada, L., Staehler, J., Folsom, C.: Mechanical behavior and high-temperature performance of a woven NicalonTM/Si-N-C ceramic-matrix composite. J. Am. Ceram. Soc. 81, 1797–811 (1998)CrossRef
26.
go back to reference Jurf, R.A., Butner, S.C.: Advances in oxide-oxide CMC. J. Engineering Gas Turbines Power, Trans. ASME 122, 202–205 (2000)CrossRef Jurf, R.A., Butner, S.C.: Advances in oxide-oxide CMC. J. Engineering Gas Turbines Power, Trans. ASME 122, 202–205 (2000)CrossRef
27.
go back to reference Ruggles-Wrenn, M.B., Jones, T.: Tension-compression fatigue behavior of a SiC/SiC ceramic matrix composite at 1200°C in air and in steam. Int. J. Fatig. 47, 154–160 (2013)CrossRef Ruggles-Wrenn, M.B., Jones, T.: Tension-compression fatigue behavior of a SiC/SiC ceramic matrix composite at 1200°C in air and in steam. Int. J. Fatig. 47, 154–160 (2013)CrossRef
28.
go back to reference Wilson, D.M., Visser, L.R.: High performance oxide fibers for metal and ceramic composites. Comp. A 32, 1143–1153 (2001)CrossRef Wilson, D.M., Visser, L.R.: High performance oxide fibers for metal and ceramic composites. Comp. A 32, 1143–1153 (2001)CrossRef
29.
go back to reference Wilson, D.M., Lieder, S.L., Luenegurg, D.C.: Microstructure and high-temperature properties of Nextel 720 fibers. Ceram. Eng. Sci. Proc. 16(5), 1005–1014 (1995)CrossRef Wilson, D.M., Lieder, S.L., Luenegurg, D.C.: Microstructure and high-temperature properties of Nextel 720 fibers. Ceram. Eng. Sci. Proc. 16(5), 1005–1014 (1995)CrossRef
30.
go back to reference Wannaparhun, S., Seal, S.: A combined spectroscopic and thermodynamic investigation of Nextel-720/alumina ceramic matrix composite in air and water vapor at 1100°C. J. Am. Ceram. Soc. 86, 1628–30 (2003)CrossRef Wannaparhun, S., Seal, S.: A combined spectroscopic and thermodynamic investigation of Nextel-720/alumina ceramic matrix composite in air and water vapor at 1100°C. J. Am. Ceram. Soc. 86, 1628–30 (2003)CrossRef
Metadata
Title
Tension-Compression Fatigue of a Nextel™720/alumina Composite at 1200 °C in Air and in Steam
Authors
R. L. Lanser
M. B. Ruggles-Wrenn
Publication date
01-08-2016
Publisher
Springer Netherlands
Published in
Applied Composite Materials / Issue 4/2016
Print ISSN: 0929-189X
Electronic ISSN: 1573-4897
DOI
https://doi.org/10.1007/s10443-016-9481-8

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