Skip to main content
Disciplines
Automotive Business IT + Informatics Construction + Real Estate Electrical Engineering + Electronics Energy + Sustainability Insurance + Risk Finance + Banking Management + Leadership Marketing + Sales Mechanical Engineering + Materials
Events
DE
EN
Books
Journals
Topic Page
Marketing
Start single access now
Access for companies
EXTENDED SEARCH
Log in
Top
Published in:
Cover of the book

2018 | OriginalPaper | Chapter

Thermal Decomposition and Stabilization Studies of ADN with AN Impurities in the Presence of Catalysts

Authors : Pratim Kumar, Rajiv Kumar, Puran Chandra Joshi

Published in: Proceedings of the International Conference on Modern Research in Aerospace Engineering

Publisher: Springer Singapore

Log in

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

In the present study, Ammonium Dinitramide (ADN) was synthesized by the nitration of Potassium Sulfamate (PS) salt with mixed acids of nitric/sulfuric acid in the ratio of 4:1 at −40 °C. The synthesized ADN was then characterized by using various analytical instruments. The preliminary result obtained has confirmed that the obtained ADN has AN impurities in its crystals. The next attempt was to stabilize synthesized ADN by adding 2% of catalysts by weight. Catalysts used in the present work are Cupric (II) Oxide (CuO), Ammonium Metavandate (NH4VO3), and Copper Chromite (Cu2Cr2O5). Evaporative crystallization method was used to prepare ADN + Catalysts samples. Simultaneous Thermal Analyzer (STA) was used to study the thermal characteristics of prepared samples by using DSC/TG-DTG techniques. All the three catalysts were found to be effective in stabilization of ADN, however NH4VO3 was found to be most effective.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

inform now

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

inform now

Springer Professional "Wirtschaft"

Online-Abonnement

Mit Springer Professional "Wirtschaft" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 340 Zeitschriften

aus folgenden Fachgebieten:

  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Versicherung + Risiko




Jetzt Wissensvorsprung sichern!

inform now
next chapter Experimental Investigation of Flame Speed of Fuel–Air Mixture for Varying Air/Fuel Ratio
Literature
1.
Sutton GP (2001) Rocket propulsion elements seventh edition. Wiley New York, Chapter 12, pp. 474–517
2.
Jacobs PWM, Whitehead HM (1969) Decomposition and combustion of ammonium perchlorate. Chem Rev 69(4):551–590CrossRef
3.
Talawar MB, Sivabalan R, Mukundan T, Muthurajan H, Sikder AK, Gandhe BR, Rao AS (2009) Environmentally compatible next generation green energetic materials (GEMs). J Hazard Mater 161:589–607CrossRef
4.
Sinditskii VP, Egorshev VY, Levshenkov AI, Serushkin VV (2006) Combustion of ammonium dinitramide, Part 1: burning behavior. J Propuls Pow 22(4):769–776
5.
Sinditskii VP, Egorshev VY, Levshenkov AI, Serushkin VV (2006) Combustion of ammonium dinitramide, Part 2: combustion mechanism. J Propuls Pow 22( 4):P777–784
6.
Vandel AP, Lobanova AA, Loginova VS (2009) Application of dinitramide salts (Review). Russ J Appl Chem 89(10):1763–1768CrossRef
7.
Ostmark H, Bemm U, Langlet A, Sanden R, Wingborg N (2000) The properties of ammonium dinitramide (ADN): part 1, basic properties, and spectroscopic data. J Energ Mater 18(2):123–138CrossRef
8.
Heintz T, Pontius H, Aniol J, Birke C, Leisinger K, Reinhard W (2009) Ammonium dinitramide (ADN)-prilling, coating, and characterization. Propellants Explos Pyrotech 34:231–238CrossRef
9.
Mishra IB, Russell TP (2002) Thermal stability of ammonium dinitramide. Thermochim Acta 384:47–56CrossRef
10.
Golofit T, Maksimowski P, Biernacki A (2013) Optimization of potassium dinitramide preparation. Propellants Explos Pyrotech 38:261–265CrossRef
11.
Wingborg N, de Flon J, Johnson C, Whitelow W (2008) Green propellants based on ADN, space propulsion, 5–8 May’, Heraklion, Crete, Greece. ESA, 3AF, SNPE
12.
Larsson A, Wingborg W, Green propellants based on ammonium dinitramide, Swedish Defence Research Academy, Sweden, Advances in Spacecraft Technology
13.
Oommen C, Jain SR (1999) Ammonium nitrate: a promising rocket propellant oxidizer. J Hazard Mater 67:253–281CrossRef
14.
Sudhakar AOR, Mathew S (2006) Thermal behavior of CuO doped phase stabilized ammonium nitrate. Thermochim Acta 451:5–9CrossRef
Metadata
Title
Thermal Decomposition and Stabilization Studies of ADN with AN Impurities in the Presence of Catalysts
Authors
Pratim Kumar
Rajiv Kumar
Puran Chandra Joshi
Copyright Year
2018
Publisher
Springer Singapore
Book
Proceedings of the International Conference on Modern Research in Aerospace Engineering

Print ISBN: 978-981-10-5848-6

Electronic ISBN: 978-981-10-5849-3

Copyright Year: 2018

DOI
https://doi.org/10.1007/978-981-10-5849-3_1

Premium Partner

    Image Credits