Skip to main content
Top

2021 | OriginalPaper | Chapter

4. Atomic Structure and Microstructure Characterization

Authors : Jens Freudenberger, Martin Heilmaier, Ulrich Wendt

Published in: Springer Handbook of Mechanical Engineering

Publisher: Springer International Publishing

Activate our intelligent search to find suitable subject content or patents.

search-config
loading …

Abstract

This chapter is structured into two main parts. Part 1 describes the fundamentals of the atomic (ideal) structure and (real) microstructure arrangement of solid matter. The way in which (metallic) materials are generated from the melt and the resulting phase diagrams for common binary systems are elucidated in the first part of this chapter (Sect. 4.1). In order to understand materials properties, microstructural characterization has to be carried out on various length scales. Therefore, in the second part (Sect. 4.2), the most common preparation steps for microscopy methods used in materialography are given. Next, basic micromethods for the investigation of the local chemical composition and local crystalline structure are outlined. This includes methodologies for the quantification of the complex microstructures in engineering materials.

Dont have a licence yet? Then find out more about our products and how to get one now:

Springer Professional "Wirtschaft+Technik"

Online-Abonnement

Mit Springer Professional "Wirtschaft+Technik" erhalten Sie Zugriff auf:

  • über 102.000 Bücher
  • über 537 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Finance + Banking
  • Management + Führung
  • Marketing + Vertrieb
  • Maschinenbau + Werkstoffe
  • Versicherung + Risiko

Jetzt Wissensvorsprung sichern!

Springer Professional "Technik"

Online-Abonnement

Mit Springer Professional "Technik" erhalten Sie Zugriff auf:

  • über 67.000 Bücher
  • über 390 Zeitschriften

aus folgenden Fachgebieten:

  • Automobil + Motoren
  • Bauwesen + Immobilien
  • Business IT + Informatik
  • Elektrotechnik + Elektronik
  • Energie + Nachhaltigkeit
  • Maschinenbau + Werkstoffe




 

Jetzt Wissensvorsprung sichern!

Literature
go back to reference R.W. Cahn, P. Haasen, E.J. Kramer: Materials science and technology. In: Glasses and Amorphous Materials, Vol. 9, ed. by J. Zarzycki (Wiley-VCH, Weinheim 2005) R.W. Cahn, P. Haasen, E.J. Kramer: Materials science and technology. In: Glasses and Amorphous Materials, Vol. 9, ed. by J. Zarzycki (Wiley-VCH, Weinheim 2005)
go back to reference A. Inoue, T. Zhang, T. Masumoto: Production of amorphous cylinder and sheet of La55Al25Ni20 alloy by a metallic mold casting method, Mater. Trans. 31, 425–428 (1990)CrossRef A. Inoue, T. Zhang, T. Masumoto: Production of amorphous cylinder and sheet of La55Al25Ni20 alloy by a metallic mold casting method, Mater. Trans. 31, 425–428 (1990)CrossRef
go back to reference A. Peker, W.L. Johnson: A highly processable metallic glass: Zr41.2Ti13.8Cu12.5Ni10.0Be22.5, Appl. Phys. Lett. 63, 2342 (1993)CrossRef A. Peker, W.L. Johnson: A highly processable metallic glass: Zr41.2Ti13.8Cu12.5Ni10.0Be22.5, Appl. Phys. Lett. 63, 2342 (1993)CrossRef
go back to reference A. Leonhard, L.Q. Xing, M. Heilmaier, A. Gebert, J. Eckert, L. Schultz: Effect of crystalline precipitations on the mechanical behavior of bulk glass forming Zr-based alloys, Nanostruct. Mater. 10, 805–817 (1998)CrossRef A. Leonhard, L.Q. Xing, M. Heilmaier, A. Gebert, J. Eckert, L. Schultz: Effect of crystalline precipitations on the mechanical behavior of bulk glass forming Zr-based alloys, Nanostruct. Mater. 10, 805–817 (1998)CrossRef
go back to reference A. Inoue: Stabilization of metallic supercooled liquid and bulk amorphous alloys, Acta Mater 48, 279–306 (2000)CrossRef A. Inoue: Stabilization of metallic supercooled liquid and bulk amorphous alloys, Acta Mater 48, 279–306 (2000)CrossRef
go back to reference C. Kittel: Introduction to Solid State Physics, 8th edn. (Wiley, Chichester 2004)MATH C. Kittel: Introduction to Solid State Physics, 8th edn. (Wiley, Chichester 2004)MATH
go back to reference R.W. Cahn, P. Haasen: Physical Metallurgy, 4th edn. (North Holland, Amsterdam 1996) R.W. Cahn, P. Haasen: Physical Metallurgy, 4th edn. (North Holland, Amsterdam 1996)
go back to reference R. Tilley: Crystals and Crystal Structures (Wiley, Chichester 2006) R. Tilley: Crystals and Crystal Structures (Wiley, Chichester 2006)
go back to reference D.A. Porter, K.E. Easterling: Phase Transformations in Metals and Alloys, 2nd edn. (Chapman Hall, London 1997) D.A. Porter, K.E. Easterling: Phase Transformations in Metals and Alloys, 2nd edn. (Chapman Hall, London 1997)
go back to reference D.B. Williams, C.B. Carter: Transmission Electron Microscopy (Plenum, New York 1996)CrossRef D.B. Williams, C.B. Carter: Transmission Electron Microscopy (Plenum, New York 1996)CrossRef
go back to reference G.E. Dieter: Mechanical Metallurgy, SI Metric Edition (McGraw-Hill, London 1988) G.E. Dieter: Mechanical Metallurgy, SI Metric Edition (McGraw-Hill, London 1988)
go back to reference E.O. Hall: The deformation and aging of mild steel: III Discussion of results, Proc. R. Soc. B 64, 747–752 (1951) E.O. Hall: The deformation and aging of mild steel: III Discussion of results, Proc. R. Soc. B 64, 747–752 (1951)
go back to reference N.J. Petch: The cleavage strength of polycrystals, J. Iron Steel Inst. 174, 25 (1953) N.J. Petch: The cleavage strength of polycrystals, J. Iron Steel Inst. 174, 25 (1953)
go back to reference J. Gurland: Correlation between yield strength and microstructure of some carbon steels. In: Stereology and Quantitative Metallography, ed. by G. Pellissier, S. Purdy (ASTM International, West Conshohocken 1972) pp. 108–118CrossRef J. Gurland: Correlation between yield strength and microstructure of some carbon steels. In: Stereology and Quantitative Metallography, ed. by G. Pellissier, S. Purdy (ASTM International, West Conshohocken 1972) pp. 108–118CrossRef
go back to reference B. Reppich: Particle strengthening. In: Plastic Deformation and Fracture of Materials, Materials Science and Technology, Vol. 6, ed. by R.W. Cahn, P. Haasen, E.J. Kramer (Wiley-VCH, Weinheim 1993) pp. 312–357 B. Reppich: Particle strengthening. In: Plastic Deformation and Fracture of Materials, Materials Science and Technology, Vol. 6, ed. by R.W. Cahn, P. Haasen, E.J. Kramer (Wiley-VCH, Weinheim 1993) pp. 312–357
go back to reference R.J. Silbey, R.A. Alberty, M.G. Bawendi: Physical Chemistry, 4th edn. (Wiley, Hoboken 2005) R.J. Silbey, R.A. Alberty, M.G. Bawendi: Physical Chemistry, 4th edn. (Wiley, Hoboken 2005)
go back to reference H.E. Exner, M. Rettenmayr, C. Müller: Komplexe Grenzflächengeometrien bei Phasenumwandlungen, Prakt. Metallogr. 41, 443–458 (2004)CrossRef H.E. Exner, M. Rettenmayr, C. Müller: Komplexe Grenzflächengeometrien bei Phasenumwandlungen, Prakt. Metallogr. 41, 443–458 (2004)CrossRef
go back to reference V.K. Pecharsky, P. Zavalij: Fundamentals of Powder Diffraction and Structural Characterization of Materials (Kluwer, Dordrecht 2003) V.K. Pecharsky, P. Zavalij: Fundamentals of Powder Diffraction and Structural Characterization of Materials (Kluwer, Dordrecht 2003)
go back to reference D.J. Dyson: X-ray and Electron Diffraction Studies in Materials Science (Maney, London 2004) D.J. Dyson: X-ray and Electron Diffraction Studies in Materials Science (Maney, London 2004)
go back to reference F.H. Chung, D.K. Smith: Industrial Applications of X-ray Diffraction (Dekker, New York 1999) F.H. Chung, D.K. Smith: Industrial Applications of X-ray Diffraction (Dekker, New York 1999)
go back to reference M. Howes, T. Inoue, G.E. Totten: Handbook of Residual Stress and Deformation of Steel (ASM International, Materials Park 2002) M. Howes, T. Inoue, G.E. Totten: Handbook of Residual Stress and Deformation of Steel (ASM International, Materials Park 2002)
go back to reference V. Randle, O. Engler: Introduction to Texture Analysis (Gordon Breach, Amsterdam 2000)CrossRef V. Randle, O. Engler: Introduction to Texture Analysis (Gordon Breach, Amsterdam 2000)CrossRef
go back to reference H.J. Bunge: Texture Analysis in Materials Science, Mathematical Methods (Butterworth-Heinemann, London 1982) H.J. Bunge: Texture Analysis in Materials Science, Mathematical Methods (Butterworth-Heinemann, London 1982)
go back to reference G.F. Vander Voort: ASM Handbook: Metallography and Microstructures (ASM International, Materials Park 2004)CrossRef G.F. Vander Voort: ASM Handbook: Metallography and Microstructures (ASM International, Materials Park 2004)CrossRef
go back to reference B. Bousfield: Surface Preparation and Microscopy of Materials (Wiley, Chichester 1992)CrossRef B. Bousfield: Surface Preparation and Microscopy of Materials (Wiley, Chichester 1992)CrossRef
go back to reference G. Petzow, V. Carle: Metallographic Etching (ASM International, Materials Park 1999) G. Petzow, V. Carle: Metallographic Etching (ASM International, Materials Park 1999)
go back to reference H.G. Michler: Electron Microscopy of Polymers (Springer, Berlin, Heidelberg 2008) H.G. Michler: Electron Microscopy of Polymers (Springer, Berlin, Heidelberg 2008)
go back to reference L. Reimer: Scanning Electron Microscopy. Physics of Image Formation and Microanalysis (Springer, Berlin 1998)CrossRef L. Reimer: Scanning Electron Microscopy. Physics of Image Formation and Microanalysis (Springer, Berlin 1998)CrossRef
go back to reference J.I. Goldstein, D.E. Newbury, P. Echlin, D.C. Joy, C. Fiori, E. Lifshin: Scanning Electron Microscopy and X-ray Microanalysis (Plenum, New York 1992)CrossRef J.I. Goldstein, D.E. Newbury, P. Echlin, D.C. Joy, C. Fiori, E. Lifshin: Scanning Electron Microscopy and X-ray Microanalysis (Plenum, New York 1992)CrossRef
go back to reference W. Hauffe: Production of microstructures by ion beam sputtering. In: Sputtering by Particle Bombardment III, Topics in Applied Physics, Vol. 64, ed. by R. Behrisch, K. Wittmaack (Springer, Berlin, Heidelberg 1991) pp. 305–338CrossRef W. Hauffe: Production of microstructures by ion beam sputtering. In: Sputtering by Particle Bombardment III, Topics in Applied Physics, Vol. 64, ed. by R. Behrisch, K. Wittmaack (Springer, Berlin, Heidelberg 1991) pp. 305–338CrossRef
go back to reference L.A. Giannuzzi, F.A. Stevie: Introduction to Focused Ion Beams (Springer, New York 2004) L.A. Giannuzzi, F.A. Stevie: Introduction to Focused Ion Beams (Springer, New York 2004)
go back to reference B.W. Kempshall, S.M. Schwarz, B.I. Prenitzer, L.A. Giannuzzi, R.B. Irwin, F.A. Stevie: Ion channeling effects on the focused ion beam milling of Cu, J. Vac. Sci. Technol. B 19, 749–754 (2001)CrossRef B.W. Kempshall, S.M. Schwarz, B.I. Prenitzer, L.A. Giannuzzi, R.B. Irwin, F.A. Stevie: Ion channeling effects on the focused ion beam milling of Cu, J. Vac. Sci. Technol. B 19, 749–754 (2001)CrossRef
go back to reference L. Reimer: Transmission Electron Microscopy. Physics of Image Formation and Microanalysis (Springer, Berlin 2006) L. Reimer: Transmission Electron Microscopy. Physics of Image Formation and Microanalysis (Springer, Berlin 2006)
go back to reference C.C. Ahn, M.M. Disko, B. Fultz: Transmission Electron Energy Loss Spectrometry in Materials Science and the EELS Atlas (Wiley-VCH, Weinheim 2004)CrossRef C.C. Ahn, M.M. Disko, B. Fultz: Transmission Electron Energy Loss Spectrometry in Materials Science and the EELS Atlas (Wiley-VCH, Weinheim 2004)CrossRef
go back to reference J.P. Eberhart: Structural and Chemical Analysis of Materials (Wiley, Chichester 1991) J.P. Eberhart: Structural and Chemical Analysis of Materials (Wiley, Chichester 1991)
go back to reference V.D. Scott, G. Love, S.J.B. Reed: Quantitative Electron Probe Microanalysis (Ellis Horwood, New York 1995) V.D. Scott, G. Love, S.J.B. Reed: Quantitative Electron Probe Microanalysis (Ellis Horwood, New York 1995)
go back to reference A.J. Schwartz, M. Kumar, B.L. Adams: Electron Backscatter Diffraction in Materials Science (Kluwer, New York 2000)CrossRef A.J. Schwartz, M. Kumar, B.L. Adams: Electron Backscatter Diffraction in Materials Science (Kluwer, New York 2000)CrossRef
go back to reference D.J. Dingley, K.Z. Baba-Kishi, V. Randle: Atlas of Backscattering Kikuchi Diffraction Patterns (IOP, Bristol 1995) D.J. Dingley, K.Z. Baba-Kishi, V. Randle: Atlas of Backscattering Kikuchi Diffraction Patterns (IOP, Bristol 1995)
go back to reference D. Katrakova, F. Mücklich: Specimen preparation for electron backscatter diffraction. Part I: Metals, Prakt. Metallogr. 38, 547–565 (2001)CrossRef D. Katrakova, F. Mücklich: Specimen preparation for electron backscatter diffraction. Part I: Metals, Prakt. Metallogr. 38, 547–565 (2001)CrossRef
go back to reference D. Katrakova, F. Mücklich: Specimen preparation for electron backscatter diffraction. Part II: Ceramics, Prakt. Metallogr. 39, 644–662 (2002)CrossRef D. Katrakova, F. Mücklich: Specimen preparation for electron backscatter diffraction. Part II: Ceramics, Prakt. Metallogr. 39, 644–662 (2002)CrossRef
go back to reference R.P. Goehner, J.R. Michael: Phase identification in a scanning electron microscope using backscattered electron Kikuchi patterns, J. Res. Natl. Inst. Stand. Technol. 101, 301–308 (1996)CrossRef R.P. Goehner, J.R. Michael: Phase identification in a scanning electron microscope using backscattered electron Kikuchi patterns, J. Res. Natl. Inst. Stand. Technol. 101, 301–308 (1996)CrossRef
go back to reference R.A. Schwarzer, A. Huot: The study of microstructure on a mesoscale by ACOM, Cryst. Res. Technol. 35, 851–862 (2000)CrossRef R.A. Schwarzer, A. Huot: The study of microstructure on a mesoscale by ACOM, Cryst. Res. Technol. 35, 851–862 (2000)CrossRef
go back to reference E.E. Underwood: Quantitative Stereology (Addison-Wesley, Reading 1970) E.E. Underwood: Quantitative Stereology (Addison-Wesley, Reading 1970)
go back to reference J. Ohser, F. Mücklich: Statistical Analysis of Microstructures in Materials Science (Wiley, Chichester 2000)MATH J. Ohser, F. Mücklich: Statistical Analysis of Microstructures in Materials Science (Wiley, Chichester 2000)MATH
go back to reference H.E. Exner: Quantitative description of microstructures by image analysis. In: Characterization of Materials (Part II), Materials Science and Technology, Vol. 2B, ed. by R.W. Cahn, P. Haasen, E.J. Kramer (VCH, Weinheim 1994) pp. 281–350 H.E. Exner: Quantitative description of microstructures by image analysis. In: Characterization of Materials (Part II), Materials Science and Technology, Vol. 2B, ed. by R.W. Cahn, P. Haasen, E.J. Kramer (VCH, Weinheim 1994) pp. 281–350
go back to reference E.E. Underwood: Quantitative metallography. In: Metallography and Microstructures, 9th edn., Metals Handbook, Vol. 9, ed. by K. Mills (ASM, Materials Park 1985) pp. 123–134 E.E. Underwood: Quantitative metallography. In: Metallography and Microstructures, 9th edn., Metals Handbook, Vol. 9, ed. by K. Mills (ASM, Materials Park 1985) pp. 123–134
go back to reference ISO: ISO 9042:1988: Steel – Manual Point Counting Method for Statistically Estimating the Volume Fraction of a Constituent with a Point Grid (ISO, Geneva 1988) ISO: ISO 9042:1988: Steel – Manual Point Counting Method for Statistically Estimating the Volume Fraction of a Constituent with a Point Grid (ISO, Geneva 1988)
go back to reference ISO: ISO 14250:2000 Steel – Metallographic Characterization of Duplex Grain Size and Distributions (ISO, Geneva 2000) ISO: ISO 14250:2000 Steel – Metallographic Characterization of Duplex Grain Size and Distributions (ISO, Geneva 2000)
go back to reference ASTM: ASTM E1245-03: Standard Practice for Determining the Inclusion or Second-Phase Constituent Content of Metals by Automatic Image Analysis (ASTM International, West Conshohocken 2003) ASTM: ASTM E1245-03: Standard Practice for Determining the Inclusion or Second-Phase Constituent Content of Metals by Automatic Image Analysis (ASTM International, West Conshohocken 2003)
go back to reference ISO: ISO 945:1975: Cast Iron – Designation of Microstructure of Graphite (ISO, Geneva 1975) ISO: ISO 945:1975: Cast Iron – Designation of Microstructure of Graphite (ISO, Geneva 1975)
go back to reference ISO: ISO 2624:1990: Copper and Copper Alloys – Estimation of Average Grain Size (ISO, Geneva 1990) ISO: ISO 2624:1990: Copper and Copper Alloys – Estimation of Average Grain Size (ISO, Geneva 1990)
go back to reference ASTM: ASTM E112-96(2004): Standard Test Methods for Determining Average Grain Size (ASTM International, West Conshohocken 2004) ASTM: ASTM E112-96(2004): Standard Test Methods for Determining Average Grain Size (ASTM International, West Conshohocken 2004)
go back to reference ISO: ISO 643-2003: Steels – Micrographic Determination of the Apparent Grain Size (ISO, Geneva 2003) ISO: ISO 643-2003: Steels – Micrographic Determination of the Apparent Grain Size (ISO, Geneva 2003)
Metadata
Title
Atomic Structure and Microstructure Characterization
Authors
Jens Freudenberger
Martin Heilmaier
Ulrich Wendt
Copyright Year
2021
Publisher
Springer International Publishing
DOI
https://doi.org/10.1007/978-3-030-47035-7_4

Premium Partners