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Metallurgical and Materials Transactions A

Published in:

01-11-2012

Characterization and In Vitro Corrosion Investigations of Thermal Sprayed Hydroxyapatite and Hydroxyapatite-Titania Coatings on Ti Alloy

Authors: Tejinder Pal Singh Sarao, Hazoor Singh Sidhu, Harpreet Singh

Published in: Metallurgical and Materials Transactions A | Issue 11/2012

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Abstract

In the current investigation, hydroxyapatite (HA) powder was mixed with titania (TiO₂) in 50:50 wt pct for depositing composite coatings on a Ti-alloy substrate using a thermal-spray coating technique. The coatings were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM)/energy-dispersive X-ray spectroscopy (EDS) analyses. The corrosion behavior of the coatings was studied by electrochemical corrosion testing in simulated human body fluid. After the corrosion testing, the samples were analyzed by XRD and SEM/EDS analyses. HA and TiO₂ (rutile) were the main phases observed in the developed coatings. Bulk HA coating was amorphous; however, the addition of TiO₂ effectively improved the crystallinity of HA in HA-TiO₂ coating. The SEM analysis confirmed the formation of a well-formed HA-TiO₂ composite coating. HA coating exhibited higher bond strength (67.8 MPa) compared with HA-TiO₂ composite coating (37.6 MPa). The electrochemical study showed a significant improvement in the corrosion resistance of the Ti alloy after the deposition of the coatings.

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Title: Characterization and In Vitro Corrosion Investigations of Thermal Sprayed Hydroxyapatite and Hydroxyapatite-Titania Coatings on Ti Alloy
Authors: Tejinder Pal Singh Sarao
Hazoor Singh Sidhu
Harpreet Singh
Publication date: 01-11-2012
Publisher: Springer US
Published in: Metallurgical and Materials Transactions A / Issue 11/2012
Print ISSN: 1073-5623
Electronic ISSN: 1543-1940
DOI: https://doi.org/10.1007/s11661-012-1175-8

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