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Erschienen in: Metallurgical and Materials Transactions A 11/2012

01.11.2012

Characterization and In Vitro Corrosion Investigations of Thermal Sprayed Hydroxyapatite and Hydroxyapatite-Titania Coatings on Ti Alloy

verfasst von: Tejinder Pal Singh Sarao, Hazoor Singh Sidhu, Harpreet Singh

Erschienen in: Metallurgical and Materials Transactions A | Ausgabe 11/2012

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Abstract

In the current investigation, hydroxyapatite (HA) powder was mixed with titania (TiO2) in 50:50 wt pct for depositing composite coatings on a Ti-alloy substrate using a thermal-spray coating technique. The coatings were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM)/energy-dispersive X-ray spectroscopy (EDS) analyses. The corrosion behavior of the coatings was studied by electrochemical corrosion testing in simulated human body fluid. After the corrosion testing, the samples were analyzed by XRD and SEM/EDS analyses. HA and TiO2 (rutile) were the main phases observed in the developed coatings. Bulk HA coating was amorphous; however, the addition of TiO2 effectively improved the crystallinity of HA in HA-TiO2 coating. The SEM analysis confirmed the formation of a well-formed HA-TiO2 composite coating. HA coating exhibited higher bond strength (67.8 MPa) compared with HA-TiO2 composite coating (37.6 MPa). The electrochemical study showed a significant improvement in the corrosion resistance of the Ti alloy after the deposition of the coatings.

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Metadaten
Titel
Characterization and In Vitro Corrosion Investigations of Thermal Sprayed Hydroxyapatite and Hydroxyapatite-Titania Coatings on Ti Alloy
verfasst von
Tejinder Pal Singh Sarao
Hazoor Singh Sidhu
Harpreet Singh
Publikationsdatum
01.11.2012
Verlag
Springer US
Erschienen in
Metallurgical and Materials Transactions A / Ausgabe 11/2012
Print ISSN: 1073-5623
Elektronische ISSN: 1543-1940
DOI
https://doi.org/10.1007/s11661-012-1175-8

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