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Journal of Materials Science: Materials in Electronics
Published in: Journal of Materials Science: Materials in Electronics 24/2019

12-11-2019

Effect of different MnO2 phases (β-, γ-, and ε-) on the microstructure and piezoelectric properties of Pb(Zr1/2Ti1/2)O3–Pb(Zn1/3Nb2/3)O3–Pb(Ni1/3Nb2/3)O3 ceramics for energy harvesting

Authors: Junting Liu, Leilei Li, Zhennan Liu, Wanli Wu, Yujian Wang, Jie Xu, Feng Gao

Published in: Journal of Materials Science: Materials in Electronics | Issue 24/2019

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Abstract

This study reports 0.83Pb(Zr1/2Ti1/2)O3–0.11Pb(Zn1/3Nb2/3)O3–0.06Pb(Ni1/3Nb2/3)O3 (PZNNT) ceramics doped with MnO2 were obtained through the conventional solid-state reaction method. The effects of MnO2 additive with different phases (β-, γ-, and ε-) on the microstructure and piezoelectric properties of PZNNT ceramics were discussed under the same condition. On the basis of X-ray photoelectron spectroscopy (XPS), the results clearly showed that Mn ions in different crystal forms of MnO2 could convert from Mn4+ ions to diverse valence states (Mn2+, Mn3+) and produce different oxygen vacancies. Furthermore, the relevant electric properties of samples increased as follows: PZNNT/β-MnO2 < PZNNT/ε-MnO2 < PZNNT/γ-MnO2. The optimal electric properties could be obtained by adding 1.5 mol% γ-MnO2, the energy conversion factor (d33 × g33), the mechanical quality factor (Qm), the electromechanical coupling factor (kp), and the Curie temperature (Tc) which were 9859 × 10−15 m2/N, 357, 0.556, and 315 °C, respectively. It indicates that γ-MnO2-modified PZNNT ceramics are potential candidate materials for piezoelectric energy harvesting.
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Metadata
Title
Effect of different MnO2 phases (β-, γ-, and ε-) on the microstructure and piezoelectric properties of Pb(Zr1/2Ti1/2)O3–Pb(Zn1/3Nb2/3)O3–Pb(Ni1/3Nb2/3)O3 ceramics for energy harvesting
Authors
Junting Liu
Leilei Li
Zhennan Liu
Wanli Wu
Yujian Wang
Jie Xu
Feng Gao
Publication date
12-11-2019
Publisher
Springer US
Published in
Journal of Materials Science: Materials in Electronics / Issue 24/2019
Print ISSN: 0957-4522
Electronic ISSN: 1573-482X
DOI
https://doi.org/10.1007/s10854-019-02504-5

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