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Published in: Journal of Materials Engineering and Performance 7/2016

23-05-2016

Effect of Friction Stir Processing on Microstructure and Mechanical Properties of AZ91C Magnesium Cast Alloy Weld Zone

Authors: Behzad Hassani, Fathallah Karimzadeh, Mohammad Hossein Enayati, Soheil Sabooni, Rudolf Vallant

Published in: Journal of Materials Engineering and Performance | Issue 7/2016

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Abstract

In this study, friction stir processing (FSP) was applied to the GTAW (TIG)-welded AZ91C cast alloy to refine the microstructure and optimize the mechanical properties of the weld zone. Microstructural investigation of the samples was performed by optical microscopy and the phases in the microstructure were determined by x-ray diffraction (XRD). The microstructural evaluations showed that FSP destroys the coarse dendritic microstructure. Furthermore, it dissolves the secondary hard and brittle β-Mg17Al12 phase existing at grain boundaries of the TIG weld zone. The closure and decrease in amount of porosities along with the elimination of the cracks in the microstructure were observed. These changes were followed by a significant grain refinement to an average value of 11 µm. The results showed that the hardness values increased to the mean ones, respectively, for as-cast (63 Hv), TIG weld zone (67 Hv), and stir zone (79 Hv). The yield and ultimate strength were significantly enhanced after FSP. The fractography evaluations, by scanning electron microscopy (SEM), indicated to a transition from brittle to ductile fracture surface after applying FSP to the TIG weld zone.

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Literature
1.
go back to reference D. Sameer Kumar, C. Tara Sasanka, K. Ravindra, and K.N.S. Suman, Magnesium and Its Alloys in Automotive Applications: A Review, Am. J. Mater. Sci. Technol., 2015, 4, p 12–30 D. Sameer Kumar, C. Tara Sasanka, K. Ravindra, and K.N.S. Suman, Magnesium and Its Alloys in Automotive Applications: A Review, Am. J. Mater. Sci. Technol., 2015, 4, p 12–30
2.
go back to reference J. Wegrzyn, M. Mazur, A. Szymanski, and B. Balcerowska, Development of a Filler for Welding Magnesium Alloy GA8, Weld. Int., 1987, 2, p 146–150CrossRef J. Wegrzyn, M. Mazur, A. Szymanski, and B. Balcerowska, Development of a Filler for Welding Magnesium Alloy GA8, Weld. Int., 1987, 2, p 146–150CrossRef
3.
go back to reference Z.J. Lu, W.J. Evans, J.D. Parker, and S. Birley, Simulation of Microstructure and Liquation Cracking in 7017 Aluminium Alloy, Mater. Sci. Eng. A, 1996, 220, p 1–7CrossRef Z.J. Lu, W.J. Evans, J.D. Parker, and S. Birley, Simulation of Microstructure and Liquation Cracking in 7017 Aluminium Alloy, Mater. Sci. Eng. A, 1996, 220, p 1–7CrossRef
4.
go back to reference J. Sheng, G.Q. You, S.Y. Long, and F.S. Pan, Abnormal Macropore Formation During Double-Sided Gas Tungsten Arc Welding Of Magnesium AZ91D Alloy, Mater. Charact., 2008, 59, p 1059–1065CrossRef J. Sheng, G.Q. You, S.Y. Long, and F.S. Pan, Abnormal Macropore Formation During Double-Sided Gas Tungsten Arc Welding Of Magnesium AZ91D Alloy, Mater. Charact., 2008, 59, p 1059–1065CrossRef
5.
go back to reference A. Razal Rose, K. Manisekar, V. Balasubramanian, and S. Rajakumar, Prediction and Optimization of Pulsed Current Tungsten Inert Gas Welding Parameters to Attain Maximum Tensile Strength in AZ61A Magnesium Alloy, Mater. Des., 2012, 37, p 334–348CrossRef A. Razal Rose, K. Manisekar, V. Balasubramanian, and S. Rajakumar, Prediction and Optimization of Pulsed Current Tungsten Inert Gas Welding Parameters to Attain Maximum Tensile Strength in AZ61A Magnesium Alloy, Mater. Des., 2012, 37, p 334–348CrossRef
6.
go back to reference G. Padmanaban and V. Balasubramania, Optimization of Pulsed Current Gas Tungsten Arc Welding Process Parameters to Attain Maximum Tensile Strength in AZ31B Magnesium Alloy, Trans. Nonferrous Met. Soc. China, 2011, 21, p 467–476CrossRef G. Padmanaban and V. Balasubramania, Optimization of Pulsed Current Gas Tungsten Arc Welding Process Parameters to Attain Maximum Tensile Strength in AZ31B Magnesium Alloy, Trans. Nonferrous Met. Soc. China, 2011, 21, p 467–476CrossRef
7.
go back to reference C. Xu, G. Sheng, H. Wang, and X. Yuan, Reinforcement of Mg/Ti Joints Using Ultrasonic Assisted Tungsten Inert Gas Welding–Brazing Technology, Sci. Technol. Weld. Join., 2014, 19, p 703–707CrossRef C. Xu, G. Sheng, H. Wang, and X. Yuan, Reinforcement of Mg/Ti Joints Using Ultrasonic Assisted Tungsten Inert Gas Welding–Brazing Technology, Sci. Technol. Weld. Join., 2014, 19, p 703–707CrossRef
8.
go back to reference M. Marya and G.R. Edwards, Chloride Contributions in Flux Assisted GTA Welding of Magnesium Alloys, Weld. J., 2002, 81, p 292-s–298-s M. Marya and G.R. Edwards, Chloride Contributions in Flux Assisted GTA Welding of Magnesium Alloys, Weld. J., 2002, 81, p 292-s–298-s
9.
go back to reference W. Zhou, T.Z. Long, and C.K. Mark, Hot Cracking in Tungsten Inert Gas Welding of Magnesium Alloy AZ91D, Mater. Sci. Technol., 2007, 23, p 1294–1299CrossRef W. Zhou, T.Z. Long, and C.K. Mark, Hot Cracking in Tungsten Inert Gas Welding of Magnesium Alloy AZ91D, Mater. Sci. Technol., 2007, 23, p 1294–1299CrossRef
10.
go back to reference W. Tiejun and L. Zhiwen, A Continuum Damage Model for Weld Heat Affected Zone Under Low Cycle Fatigue Loading, Eng. Fract. Mech., 1990, 37, p 825–829CrossRef W. Tiejun and L. Zhiwen, A Continuum Damage Model for Weld Heat Affected Zone Under Low Cycle Fatigue Loading, Eng. Fract. Mech., 1990, 37, p 825–829CrossRef
11.
go back to reference F.Y. Zheng, Y.J. Wu, L.M. Peng, X.W. Li, P.H. Fu, and W.J. Ding, Microstructures and Mechanical Properties of Friction Stir Processed Mg-2.0Nd-0.3Zn-1.0Zr Magnesium Alloy, J. Magnes. Alloys, 2013, 1, p 122–127CrossRef F.Y. Zheng, Y.J. Wu, L.M. Peng, X.W. Li, P.H. Fu, and W.J. Ding, Microstructures and Mechanical Properties of Friction Stir Processed Mg-2.0Nd-0.3Zn-1.0Zr Magnesium Alloy, J. Magnes. Alloys, 2013, 1, p 122–127CrossRef
12.
go back to reference E. Cerri and P. Leo, Effect of Friction Stir Processing on Microstructure and Mechanical Properties of a HPDC Magnesium Alloy, Mater. Sci. Forum, 2014, 783–786, p 1735–1740CrossRef E. Cerri and P. Leo, Effect of Friction Stir Processing on Microstructure and Mechanical Properties of a HPDC Magnesium Alloy, Mater. Sci. Forum, 2014, 783–786, p 1735–1740CrossRef
13.
go back to reference F. Chai, D.T. Zhang, and Y.Y. Li, Effect of rotation speeds on microstructures and tensile properties of submerged friction stir processed AZ31 magnesium alloy, Mater. Res. Innov., 2014, 18, p S4-152–S4-156CrossRef F. Chai, D.T. Zhang, and Y.Y. Li, Effect of rotation speeds on microstructures and tensile properties of submerged friction stir processed AZ31 magnesium alloy, Mater. Res. Innov., 2014, 18, p S4-152–S4-156CrossRef
14.
go back to reference American Welding Society, Welding Handbook, 7th ed., vol. 4, AWS, Miami, FL, 1989 American Welding Society, Welding Handbook, 7th ed., vol. 4, AWS, Miami, FL, 1989
15.
go back to reference A.K. Dahle, Y.C. Lee, M.D. Nave, P.L. Schaffer, and D.H. St John, Development of the As-Cast Microstructure in Magnesium-Aluminium Alloys, J. Light Met., 2001, 1, p 61–72CrossRef A.K. Dahle, Y.C. Lee, M.D. Nave, P.L. Schaffer, and D.H. St John, Development of the As-Cast Microstructure in Magnesium-Aluminium Alloys, J. Light Met., 2001, 1, p 61–72CrossRef
16.
go back to reference D.X. Sun, D.Q. Sun, X.Y. Gu, and Z.Z. Xuan, Hot Cracking of Metal Inert Gas Arc Welded Magnesium Alloy AZ91D, ISIJ Int., 2009, 49, p 270–274CrossRef D.X. Sun, D.Q. Sun, X.Y. Gu, and Z.Z. Xuan, Hot Cracking of Metal Inert Gas Arc Welded Magnesium Alloy AZ91D, ISIJ Int., 2009, 49, p 270–274CrossRef
17.
go back to reference I.J. Polmear, Light Alloys: Metallurgy of the Light Metals, 2nd ed., Chapman and Hall, London, 1989, ISBN 0-340-49175-2 I.J. Polmear, Light Alloys: Metallurgy of the Light Metals, 2nd ed., Chapman and Hall, London, 1989, ISBN 0-340-49175-2
18.
go back to reference ASM Handbook Committee, Alloy Phase Diagrams, ASM International, Materials Park, OH, 1992 ASM Handbook Committee, Alloy Phase Diagrams, ASM International, Materials Park, OH, 1992
19.
go back to reference Sindo Kou and Welding Metallurgy, 2, Wiley, New York, 1987 Sindo Kou and Welding Metallurgy, 2, Wiley, New York, 1987
20.
go back to reference Q. Han, E.A. Kenik, S.R. Agnew, and S. Viswanathan, Solidification Behavior of Commercial Magnesium Alloys, Magnesium Technology 2001, J.N. Hryn, Ed., The Minerals, Metals and Materials Society (TMS), Warrendale, PA, 2001. Q. Han, E.A. Kenik, S.R. Agnew, and S. Viswanathan, Solidification Behavior of Commercial Magnesium Alloys, Magnesium Technology 2001, J.N. Hryn, Ed., The Minerals, Metals and Materials Society (TMS), Warrendale, PA, 2001.
21.
go back to reference G.C. Sih, Multiscale Fatigue Crack Initiation and Propagation of Engineering Materials, Structural Integrity and Microstructural Worthiness: Solid Mathematics and Its Applications, vol. 152, Springer, New York, 2008. G.C. Sih, Multiscale Fatigue Crack Initiation and Propagation of Engineering Materials, Structural Integrity and Microstructural Worthiness: Solid Mathematics and Its Applications, vol. 152, Springer, New York, 2008.
22.
go back to reference M.D. Nave, A.K. Dahle, and D.H. St. John, Magnesium Technology 2000, H.I. Kaplan, J.N. Hryn, and B.B. Clow, Ed., The Minerals, Metals and Materials Society (TMS), Warrendale, PA, 2000 M.D. Nave, A.K. Dahle, and D.H. St. John, Magnesium Technology 2000, H.I. Kaplan, J.N. Hryn, and B.B. Clow, Ed., The Minerals, Metals and Materials Society (TMS), Warrendale, PA, 2000
23.
go back to reference J.D.I. Shearouse and B.A. Mikucki, The Origin of Microporosity in Magnesium Alloy AZ91, SAE Trans. J. Mater. Manuf., 1994, 103, p 542–552 J.D.I. Shearouse and B.A. Mikucki, The Origin of Microporosity in Magnesium Alloy AZ91, SAE Trans. J. Mater. Manuf., 1994, 103, p 542–552
24.
go back to reference M. Hilpert and L. Wagner, Surface Treatment IV, C.A. Brebbiaand and J.M. Kenny, Ed., WIT Press, 1999, p 331 M. Hilpert and L. Wagner, Surface Treatment IV, C.A. Brebbiaand and J.M. Kenny, Ed., WIT Press, 1999, p 331
25.
go back to reference W.C. Zheng, S. Li, B. Tang, and D.B. Zeng, Microstructure and Properties of Mg-Al Binary Alloys, China Foundry, 2006, 3, p 270–274 W.C. Zheng, S. Li, B. Tang, and D.B. Zeng, Microstructure and Properties of Mg-Al Binary Alloys, China Foundry, 2006, 3, p 270–274
26.
go back to reference M.M. Avedesian, Magnesium and Magnesium Alloys, ASM International, Materials Park, OH, 1999 M.M. Avedesian, Magnesium and Magnesium Alloys, ASM International, Materials Park, OH, 1999
27.
go back to reference Alaknanda, R.S. Anand, and P. Kumar, Flaw Detection in Radiographic Weld Images Using Morphological Approach, NDT & E Int. 39, p 29–33 Alaknanda, R.S. Anand, and P. Kumar, Flaw Detection in Radiographic Weld Images Using Morphological Approach, NDT & E Int. 39, p 29–33
28.
go back to reference V. Jain, R.S. Mishra, and A.K. Gupta, Gouthama, Study of β-Precipitates and Their Effect on the Directional Yield Asymmetry of Friction Stir Processed and Aged AZ91C Alloy, Mater. Sci. Eng., A, 2013, 560, p 500–509CrossRef V. Jain, R.S. Mishra, and A.K. Gupta, Gouthama, Study of β-Precipitates and Their Effect on the Directional Yield Asymmetry of Friction Stir Processed and Aged AZ91C Alloy, Mater. Sci. Eng., A, 2013, 560, p 500–509CrossRef
29.
go back to reference A.H. Feng, B.L. Xiao, Z.Y. Ma, and R.S. Chen, Effect of Friction Stir Processing Procedures on Microstructure and Mechanical Properties of Mg-Al-Zn Casting, Effect of Friction Stir Processing Procedures on Microstructure and Mechanical Properties of Mg-Al-Zn Casting, Metall. Mater. Trans. A, 2009, 40, p 2447–2456CrossRef A.H. Feng, B.L. Xiao, Z.Y. Ma, and R.S. Chen, Effect of Friction Stir Processing Procedures on Microstructure and Mechanical Properties of Mg-Al-Zn Casting, Effect of Friction Stir Processing Procedures on Microstructure and Mechanical Properties of Mg-Al-Zn Casting, Metall. Mater. Trans. A, 2009, 40, p 2447–2456CrossRef
30.
go back to reference N. Afrin, D.L. Chen, X. Cao, and M. Jahazi, Strain Hardening Behavior of a Friction Stir Welded Magnesium Alloy, Scr. Mater., 2007, 57, p 1004–1007CrossRef N. Afrin, D.L. Chen, X. Cao, and M. Jahazi, Strain Hardening Behavior of a Friction Stir Welded Magnesium Alloy, Scr. Mater., 2007, 57, p 1004–1007CrossRef
31.
go back to reference ASM Speciality Handbook, Magnesium and Magnesium Alloys, ASM International, Materials Park, OH, 1999, p 1–314 ASM Speciality Handbook, Magnesium and Magnesium Alloys, ASM International, Materials Park, OH, 1999, p 1–314
32.
go back to reference W. Wen, W. Kuaishe, G. Qiang, and W. Nan, Effect of Friction Stir Processing on Microstructure and Mechanical Properties of Cast AZ31 Magnesium Alloy, Rare Met. Mater. Eng., 2012, 41, p 1522–1526CrossRef W. Wen, W. Kuaishe, G. Qiang, and W. Nan, Effect of Friction Stir Processing on Microstructure and Mechanical Properties of Cast AZ31 Magnesium Alloy, Rare Met. Mater. Eng., 2012, 41, p 1522–1526CrossRef
33.
go back to reference X.B. Liu, R.S. Chen, and E.H. Han, Effects of Ageing Treatment on Microstructures and Properties of Mg-Gd-Y-Zr Alloys With and Without Zn Additions, J. Alloys Compd., 2008, 465, p 232–238CrossRef X.B. Liu, R.S. Chen, and E.H. Han, Effects of Ageing Treatment on Microstructures and Properties of Mg-Gd-Y-Zr Alloys With and Without Zn Additions, J. Alloys Compd., 2008, 465, p 232–238CrossRef
34.
go back to reference W. Blum, P. Zhang, B. Watzinger, B.V. Grossmann, and H.G. Haldenwanger, Comparative Study of Creep of the Die-Cast Mg-Alloys AZ91, AS21, AS41, AM60 and AE42, Mater. Sci. Eng. A, 2001, 319–321, p 735–740CrossRef W. Blum, P. Zhang, B. Watzinger, B.V. Grossmann, and H.G. Haldenwanger, Comparative Study of Creep of the Die-Cast Mg-Alloys AZ91, AS21, AS41, AM60 and AE42, Mater. Sci. Eng. A, 2001, 319–321, p 735–740CrossRef
35.
go back to reference A. Fallahi, A. Ataee, and F. Biglari, Effects of Crystal Orientation on Stress Distribution Near the Triple Junction in a Tricrystal γ-TiAl, Mater. Sci. Eng. A, 2010, 527, p 4576–4581CrossRef A. Fallahi, A. Ataee, and F. Biglari, Effects of Crystal Orientation on Stress Distribution Near the Triple Junction in a Tricrystal γ-TiAl, Mater. Sci. Eng. A, 2010, 527, p 4576–4581CrossRef
Metadata
Title
Effect of Friction Stir Processing on Microstructure and Mechanical Properties of AZ91C Magnesium Cast Alloy Weld Zone
Authors
Behzad Hassani
Fathallah Karimzadeh
Mohammad Hossein Enayati
Soheil Sabooni
Rudolf Vallant
Publication date
23-05-2016
Publisher
Springer US
Published in
Journal of Materials Engineering and Performance / Issue 7/2016
Print ISSN: 1059-9495
Electronic ISSN: 1544-1024
DOI
https://doi.org/10.1007/s11665-016-2129-x

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